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Literature DB >> 23606410

Novel process windows for enabling, accelerating, and uplifting flow chemistry.

Volker Hessel¹, Dana Kralisch, Norbert Kockmann, Timothy Noël, Qi Wang.

Abstract

Novel Process Windows make use of process conditions that are far from conventional practices. This involves the use of high temperatures, high pressures, high concentrations (solvent-free), new chemical transformations, explosive conditions, and process simplification and integration to boost synthetic chemistry on both the laboratory and production scale. Such harsh reaction conditions can be safely reached in microstructured reactors due to their excellent transport intensification properties. This Review discusses the different routes towards Novel Process Windows and provides several examples for each route grouped into different classes of chemical and process-design intensification.

Mesh：

Year: 2013 PMID： 23606410 DOI： 10.1002/cssc.201200766

Source DB: PubMed Journal: ChemSusChem ISSN： 1864-5631 Impact factor: 8.928

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Cited

27 in total

1. A high gas fraction, reduced power, syngas bioprocessing method demonstrated with a Clostridium ljungdahlii OTA1 paper biocomposite.

Authors: Mark J Schulte; Jeff Wiltgen; John Ritter; Charles B Mooney; Michael C Flickinger
Journal: Biotechnol Bioeng Date: 2016-03-28 Impact factor: 4.530

Review 2. Technological Innovations in Photochemistry for Organic Synthesis: Flow Chemistry, High-Throughput Experimentation, Scale-up, and Photoelectrochemistry.

Authors: Laura Buglioni; Fabian Raymenants; Aidan Slattery; Stefan D A Zondag; Timothy Noël
Journal: Chem Rev Date: 2021-08-10 Impact factor: 60.622

3. Development of an Intermittent-Flow Enantioselective Aza-Henry Reaction Using an Arylnitromethane and Homogeneous Brønsted Acid-Base Catalyst with Recycle.

Authors: Sergey V Tsukanov; Martin D Johnson; Scott A May; Morgan Rosemeyer; Michael A Watkins; Stanley P Kolis; Matthew H Yates; Jeffrey N Johnston
Journal: Org Process Res Dev Date: 2016-02-01 Impact factor: 3.317

4. Biocatalysis in Continuous-Flow Microfluidic Reactors.

Authors: Marco P Cardoso Marques; Alvaro Lorente-Arevalo; Juan M Bolivar
Journal: Adv Biochem Eng Biotechnol Date: 2022 Impact factor: 2.768

Review 5. The synthesis of active pharmaceutical ingredients (APIs) using continuous flow chemistry.

Authors: Marcus Baumann; Ian R Baxendale
Journal: Beilstein J Org Chem Date: 2015-07-17 Impact factor: 2.883

6. Flow synthesis of phenylserine using threonine aldolase immobilized on Eupergit support.

Authors: Jagdish D Tibhe; Hui Fu; Timothy Noël; Qi Wang; Jan Meuldijk; Volker Hessel
Journal: Beilstein J Org Chem Date: 2013-10-22 Impact factor: 2.883

Review 7. Machine-Assisted Organic Synthesis.

Authors: Steven V Ley; Daniel E Fitzpatrick; Rebecca M Myers; Claudio Battilocchio; Richard J Ingham
Journal: Angew Chem Int Ed Engl Date: 2015-07-16 Impact factor: 15.336

Novel process windows for enabling, accelerating, and uplifting flow chemistry.

1. A high gas fraction, reduced power, syngas bioprocessing method demonstrated with a Clostridium ljungdahlii OTA1 paper biocomposite.

Review 2. Technological Innovations in Photochemistry for Organic Synthesis: Flow Chemistry, High-Throughput Experimentation, Scale-up, and Photoelectrochemistry.

3. Development of an Intermittent-Flow Enantioselective Aza-Henry Reaction Using an Arylnitromethane and Homogeneous Brønsted Acid-Base Catalyst with Recycle.

4. Biocatalysis in Continuous-Flow Microfluidic Reactors.

Review 5. The synthesis of active pharmaceutical ingredients (APIs) using continuous flow chemistry.

6. Flow synthesis of phenylserine using threonine aldolase immobilized on Eupergit support.

Review 7. Machine-Assisted Organic Synthesis.

Review 8. Enabling Technologies for the Future of Chemical Synthesis.

Review 9. Microflow High-p,T Intensification of Vitamin D₃ Synthesis Using an Ultraviolet Lamp.

Review 10. Strategic Application of Residence-Time Control in Continuous-Flow Reactors.

Novel process windows for enabling, accelerating, and uplifting flow chemistry.

1. A high gas fraction, reduced power, syngas bioprocessing method demonstrated with a Clostridium ljungdahlii OTA1 paper biocomposite.

Review 2. Technological Innovations in Photochemistry for Organic Synthesis: Flow Chemistry, High-Throughput Experimentation, Scale-up, and Photoelectrochemistry.

3. Development of an Intermittent-Flow Enantioselective Aza-Henry Reaction Using an Arylnitromethane and Homogeneous Brønsted Acid-Base Catalyst with Recycle.

4. Biocatalysis in Continuous-Flow Microfluidic Reactors.

Review 5. The synthesis of active pharmaceutical ingredients (APIs) using continuous flow chemistry.

6. Flow synthesis of phenylserine using threonine aldolase immobilized on Eupergit support.

Review 7. Machine-Assisted Organic Synthesis.

Review 8. Enabling Technologies for the Future of Chemical Synthesis.

Review 9. Microflow High-p,T Intensification of Vitamin D3 Synthesis Using an Ultraviolet Lamp.

Review 10. Strategic Application of Residence-Time Control in Continuous-Flow Reactors.

Review 9. Microflow High-p,T Intensification of Vitamin D₃ Synthesis Using an Ultraviolet Lamp.