Literature DB >> 22356786

40 keV atomic resolution TEM.

David C Bell1, Christopher J Russo, Dmitry V Kolmykov.   

Abstract

Here we present the first atomic resolution TEM imaging at 40 keV using an aberration-corrected, monochromated source TEM. Low-voltage High-Resolution Electron Microscopy (LVHREM) has several advantages, including increased cross-sections for inelastic and elastic scattering, increased contrast per electron and improved spectroscopy efficiency, decreased delocalization effects and reduced knock-on damage. Together, these often improve the contrast to damage ratio obtained on a large class of samples. Third-order aberration correction now allows us to operate the TEM at low energies while retaining atomic resolution, which was previously impossible. At low voltage the major limitation to resolution becomes the chromatic aberration limit. We show that using a source monochromator we are able to reduce the effect of chromatic aberration and achieve a usable high-resolution limit at 40 keV to less than 1Å. We show various materials' examples of the application of the technique to image graphene and silicon, and compare atomic resolution images with electron multislice simulations.
Copyright © 2012 Elsevier B.V. All rights reserved.

Entities:  

Year:  2011        PMID: 22356786     DOI: 10.1016/j.ultramic.2011.12.001

Source DB:  PubMed          Journal:  Ultramicroscopy        ISSN: 0304-3991            Impact factor:   2.689


  5 in total

1.  In Situ Time-dependent Dielectric Breakdown in the Transmission Electron Microscope: A Possibility to Understand the Failure Mechanism in Microelectronic Devices.

Authors:  Zhongquan Liao; Martin Gall; Kong Boon Yeap; Christoph Sander; André Clausner; Uwe Mühle; Jürgen Gluch; Yvonne Standke; Oliver Aubel; Armand Beyer; Meike Hauschildt; Ehrenfried Zschech
Journal:  J Vis Exp       Date:  2015-06-26       Impact factor: 1.355

2.  Benefits and Limitations of Low-kV Macromolecular Imaging of Frozen-Hydrated Biological Samples.

Authors:  Endre Majorovits; Isabel Angert; Ute Kaiser; Rasmus R Schröder
Journal:  Biophys J       Date:  2016-02-23       Impact factor: 4.033

3.  Optimal acceleration voltage for near-atomic resolution imaging of layer-stacked 2D polymer thin films.

Authors:  Baokun Liang; Yingying Zhang; Christopher Leist; Zhaowei Ou; Miroslav Položij; Zhiyong Wang; David Mücke; Renhao Dong; Zhikun Zheng; Thomas Heine; Xinliang Feng; Ute Kaiser; Haoyuan Qi
Journal:  Nat Commun       Date:  2022-07-08       Impact factor: 17.694

4.  CryoEM at 100 keV: a demonstration and prospects.

Authors:  K Naydenova; G McMullan; M J Peet; Y Lee; P C Edwards; S Chen; E Leahy; S Scotcher; R Henderson; C J Russo
Journal:  IUCrJ       Date:  2019-10-11       Impact factor: 4.769

5.  Monolayer Graphitic Carbon Nitride as Metal-Free Catalyst with Enhanced Performance in Photo- and Electro-Catalysis.

Authors:  Huiyan Piao; Goeun Choi; Xiaoyan Jin; Seong-Ju Hwang; Young Jae Song; Sung-Pyo Cho; Jin-Ho Choy
Journal:  Nanomicro Lett       Date:  2022-02-03
  5 in total

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