Literature DB >> 21202052

2-(1H-1,2,3-Benzotriazol-1-yl)-N'-cyclo-pentyl-ideneacetohydrazide.

Ning-Ning Ji, Zhi-Qiang Shi.   

Abstract

The title compound, C(13)H(15)N(5)O, was synthesized by the reaction of 2-(1H-1,2,3-benzotriazol-1-yl)acetohydrazide with cyclo-penta-none. In the cyclopentane ring, two C atoms and their attached H atoms are disordered over two positions; the site occupancy factors are ca 0.63 and 0.37. In the crystal structure, mol-ecules are linked into infinite chains directed along the b axis by N-H⋯O hydrogen bonds. In addition, there are weak C-H⋯O and C-H⋯N hydrogen bonds, as well as C-H⋯π-ring inter-actions in the structure.

Entities:  

Year:  2008        PMID: 21202052      PMCID: PMC2961015          DOI: 10.1107/S1600536808005631

Source DB:  PubMed          Journal:  Acta Crystallogr Sect E Struct Rep Online        ISSN: 1600-5368


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  4 in total
  2 in total

1.  2-(1H-Benzotriazol-1-yl)acetohydrazide.

Authors:  Yan-Xia Zhang; Zhi-Qiang Shi
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2009-06-10

2.  Ethyl 2-(1H-1,2,3-benzotriazol-1-yl)acetate.

Authors:  Xiao-Xia Li; Zhong Chen
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2010-12-15
  2 in total

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