| Literature DB >> 21177139 |
V Kanagarajan1, M R Ezhilarasi, M Gopalakrishnan.
Abstract
An array of novel 1,1'-(5,5'-(1,4-phenylene)bis(3-aryl-1H-pyrazole-5,1(4H,5H)-diyl))diethanones, a bis acetylated pyrazoles derivatives are synthesized in 'one-pot' by ultrasound irradiation method and are characterized by melting point, elemental analysis, MS, FT-IR, one-dimensional NMR (1H and 13C) and two-dimensional NOESY spectra. The methylene and methane protons of pyrazoles moiety splits signal as ABX pattern in the proton NMR spectra and the key nOe correlations are confirmed by NOESY spectrum. Copyright ÂEntities:
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Year: 2010 PMID: 21177139 DOI: 10.1016/j.saa.2010.11.038
Source DB: PubMed Journal: Spectrochim Acta A Mol Biomol Spectrosc ISSN: 1386-1425 Impact factor: 4.098