Literature DB >> 20877783

Preparation of arylsulfonyl chlorides by chlorosulfonylation of in situ generated diazonium salts using a continuous flow reactor.

Laia Malet-Sanz1, Julia Madrzak, Steven V Ley, Ian R Baxendale.   

Abstract

A new flow procedure for the preparation of arylsulfonyl chlorides from aniline starting materials is described. The reaction conditions are mild, requiring no added acid and are amenable to continuous flow processing, in a safe, easily scalable and less labour intensive way than the corresponding batch method.

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Year:  2010        PMID： 20877783     DOI： 10.1039/c0ob00450b

Source DB:  PubMed          Journal:  Org Biomol Chem        ISSN： 1477-0520            Impact factor:   3.876


  8 in total

1.  The flow synthesis of heterocycles for natural product and medicinal chemistry applications.

Authors:  Marcus Baumann; Ian R Baxendale; Steven V Ley
Journal:  Mol Divers       Date:  2010-10-20       Impact factor: 2.943

2.  Synthesis of aryl sulfonamides via palladium-catalyzed chlorosulfonylation of arylboronic acids.

Authors:  J Robb DeBergh; Nootaree Niljianskul; Stephen L Buchwald
Journal:  J Am Chem Soc       Date:  2013-07-12       Impact factor: 15.419

3.  Synthesis of diverse pyrazole-4-sulfonyl chlorides starting from 2-(benzylthio)malonaldehyde.

Authors:  Pavlo A Sokolyuk; Ivan S Kondratov; Olexiy V Gavrylenko; Andrey A Tolmachov
Journal:  Mol Divers       Date:  2015-09-12       Impact factor: 2.943

4.  Continuous-flow catalytic asymmetric hydrogenations: Reaction optimization using FTIR inline analysis.

Authors:  Magnus Rueping; Teerawut Bootwicha; Erli Sugiono
Journal:  Beilstein J Org Chem       Date:  2012-02-23       Impact factor: 2.883

5.  One Amine-3 Tasks: Reductive Coupling of Imines with Olefins in Batch and Flow.

Authors:  Quentin Lefebvre; Riccardo Porta; Anthony Millet; Jiaqi Jia; Magnus Rueping
Journal:  Chemistry       Date:  2020-01-21       Impact factor: 5.236

6.  Scalable, Chemoselective Nickel Electrocatalytic Sulfinylation of Aryl Halides with SO2.

Authors:  Terry Shing-Bong Lou; Yu Kawamata; Tamara Ewing; Guillermo A Correa-Otero; Michael R Collins; Phil S Baran
Journal:  Angew Chem Int Ed Engl       Date:  2022-08-03       Impact factor: 16.823

7.  Metal- and Reagent-Free Electrochemical Synthesis of Alkyl Arylsulfonates in a Multi-Component Reaction.

Authors:  Stephan P Blum; Dieter Schollmeyer; Maris Turks; Siegfried R Waldvogel
Journal:  Chemistry       Date:  2020-06-22       Impact factor: 5.236

8.  Exploring Flow Procedures for Diazonium Formation.

Authors:  Te Hu; Ian R Baxendale; Marcus Baumann
Journal:  Molecules       Date:  2016-07-14       Impact factor: 4.411
  8 in total

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