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Literature DB >> 19907786

Synthesis of a photo-caged aminooxy alkane thiol.

Rock J Mancini¹, Ronald C Li, Zachary P Tolstyka, Heather D Maynard.

Abstract

A photo-caged aminooxy alkane thiol synthesized in 7 steps and 15% overall yield was used to form a self-assembled monolayer (SAM). Photo-deprotection on the surface was confirmed by FT-IR spectroscopy and contact angle goniometry. Conjugation of a small molecule ketone, ethyl levulinate, further confirmed the presence of aminooxy groups on the surface.

Entities: CellLine Chemical Disease Species

Mesh：

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Year: 2009 PMID： 19907786 PMCID： PMC3086890 DOI： 10.1039/b904195h

Source DB: PubMed Journal: Org Biomol Chem ISSN： 1477-0520 Impact factor: 3.876

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Authors: Shahrul A Alang Ahmad; Lu Shin Wong; Ehtsham ul-Haq; Jamie K Hobbs; Graham J Leggett; Jason Micklefield
Journal: J Am Chem Soc Date: 2009-02-04 Impact factor: 15.419

Synthesis of a photo-caged aminooxy alkane thiol.

Review 1. Engineering cellular microenvironments to improve cell-based drug testing.

Review 2. Semisynthesis of proteins by expressed protein ligation.

3. Dynamic interfaces between cells and surfaces: electroactive substrates that sequentially release and attach cells.

4. A modular approach for the construction and modification of glyco-SAMs utilizing 1,3-dipolar cycloaddition.

Review 5. Chemoselective ligation reactions with proteins, oligosaccharides and cells.

6. Global analysis of protein activities using proteome chips.

7. Dual-surface modification of the tobacco mosaic virus.

8. Molecular printboards: monolayers of beta-cyclodextrins on silicon oxide surfaces.

9. Micrometer- and nanometer-scale photopatterning using 2-nitrophenylpropyloxycarbonyl-protected aminosiloxane monolayers.

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