Literature DB >> 19559899

Identification of reaction compounds in micrometric layers from gothic paintings using combined SR-XRD and SR-FTIR.

Nati Salvadó1, Salvador Butí, James Nicholson, Hermann Emerich, Ana Labrador, Trinitat Pradell.   

Abstract

Synchrotron radiation X-ray diffraction (micro-SR-XRD) and Fourier transform infrared spectroscopy (micro-SR-FTIR) are used in the non-destructive identification of reaction and aging compounds from micrometric ancient painting layers. The combination of the micrometer size and non-destructive nature of the techniques together with the high resolution and brilliance of the synchrotron radiation has proved to be a procedure most advantageous for the study of reaction, aging and degradation processes. Copper, lead and calcium carboxylates and oxalates are determined in the chromatic, preparation and alteration layers from 15th century egg tempera and oil paintings. Their nature and crystallinity have been assessed. Some hypothesis about the mechanisms of development of both carboxylates and oxalates are presented.

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Year:  2009        PMID: 19559899     DOI: 10.1016/j.talanta.2009.04.005

Source DB:  PubMed          Journal:  Talanta        ISSN: 0039-9140            Impact factor:   6.057


  7 in total

1.  Identification of different copper green pigments in Renaissance paintings by cluster-TOF-SIMS imaging analysis.

Authors:  Pascale Richardin; Vincent Mazel; Philippe Walter; Olivier Laprévote; Alain Brunelle
Journal:  J Am Soc Mass Spectrom       Date:  2011-06-01       Impact factor: 3.109

Review 2.  A Critical Review on the Analysis of Metal Soaps in Oil Paintings.

Authors:  Francesca Caterina Izzo; Matilde Kratter; Austin Nevin; Elisabetta Zendri
Journal:  ChemistryOpen       Date:  2021-09       Impact factor: 2.630

3.  Mass Spectrometric and Synchrotron Radiation based techniques for the identification and distribution of painting materials in samples from paints of Josep Maria Sert.

Authors:  Anna Lluveras-Tenorio; Alessia Andreotti; Ilaria Bonaduce; Sarah Boularand; Marine Cotte; Josep Roqué; Maria Perla Colombini; Marius Vendrell-Saz
Journal:  Chem Cent J       Date:  2012-05-22       Impact factor: 4.215

4.  Novel optical photothermal infrared (O-PTIR) spectroscopy for the noninvasive characterization of heritage glass-metal objects.

Authors:  Andrea Marchetti; Victoria Beltran; Gert Nuyts; Ferenc Borondics; Steven De Meyer; Marina Van Bos; Jakub Jaroszewicz; Elke Otten; Marjolijn Debulpaep; Karolien De Wael
Journal:  Sci Adv       Date:  2022-03-04       Impact factor: 14.136

5.  Characterizing paint technologies and recipes in Levantine and Schematic rock art: El Carche site as a case study (Jalance, Spain).

Authors:  Annalisa Chieli; Marius Vendrell; Clodoaldo Roldán; Pilar Giráldez; Ines Domingo
Journal:  PLoS One       Date:  2022-08-15       Impact factor: 3.752

6.  Radiocarbon dating of lead white: novel application in the study of polychrome sculpture.

Authors:  Sara Sá; Laura Hendriks; Isabel Pombo Cardoso; Irka Hajdas
Journal:  Sci Rep       Date:  2021-06-24       Impact factor: 4.379

7.  Insights into the composition of ancient Egyptian red and black inks on papyri achieved by synchrotron-based microanalyses.

Authors:  Thomas Christiansen; Marine Cotte; Wout de Nolf; Elouan Mouro; Juan Reyes-Herrera; Steven de Meyer; Frederik Vanmeert; Nati Salvadó; Victor Gonzalez; Poul Erik Lindelof; Kell Mortensen; Kim Ryholt; Koen Janssens; Sine Larsen
Journal:  Proc Natl Acad Sci U S A       Date:  2020-10-26       Impact factor: 11.205

  7 in total

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