Literature DB >> 19191469

Producing and quantifying enriched para-H2.

Brian A Tom1, Siddhartha Bhasker, Yuki Miyamoto, Takamasa Momose, Benjamin J McCall.   

Abstract

The production of enriched para-H(2) is useful for many scientific applications, but the technology for producing and measuring para-H(2) is not yet widespread. In this note and in the accompanying auxiliary material, we describe the design, construction, and use of a versatile standalone converter that is capable of producing para-H(2) enrichments of up to > or = 99.99% at continuous flow rates of up to 0.4 SLM. We also discuss para-H(2) storage and back conversion rates, and improvements to three techniques (thermal conductance, NMR, and solid hydrogen impurity spectroscopy) used to quantify the para-H(2) enrichment.

Entities:  

Year:  2009        PMID: 19191469     DOI: 10.1063/1.3072881

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  7 in total

1.  A pulsed injection parahydrogen generator and techniques for quantifying enrichment.

Authors:  Bibo Feng; Aaron M Coffey; Raul D Colon; Eduard Y Chekmenev; Kevin W Waddell
Journal:  J Magn Reson       Date:  2011-12-02       Impact factor: 2.229

2.  Clinical-Scale Production of Nearly Pure (>98.5%) Parahydrogen and Quantification by Benchtop NMR Spectroscopy.

Authors:  Shiraz Nantogma; Baptiste Joalland; Ken Wilkens; Eduard Y Chekmenev
Journal:  Anal Chem       Date:  2021-02-04       Impact factor: 6.986

3.  Low-Cost High-Pressure Clinical-Scale 50% Parahydrogen Generator Using Liquid Nitrogen at 77 K.

Authors:  Benjamin Chapman; Baptiste Joalland; Collier Meersman; Jessica Ettedgui; Rolf E Swenson; Murali C Krishna; Panayiotis Nikolaou; Kirill V Kovtunov; Oleg G Salnikov; Igor V Koptyug; Max E Gemeinhardt; Boyd M Goodson; Roman V Shchepin; Eduard Y Chekmenev
Journal:  Anal Chem       Date:  2021-06-08       Impact factor: 8.008

4.  SABRE hyperpolarization enables high-sensitivity 1H and 13C benchtop NMR spectroscopy.

Authors:  Peter M Richardson; Andrew J Parrott; Olga Semenova; Alison Nordon; Simon B Duckett; Meghan E Halse
Journal:  Analyst       Date:  2018-07-09       Impact factor: 4.616

5.  Reaction Monitoring Using SABRE-Hyperpolarized Benchtop (1 T) NMR Spectroscopy.

Authors:  Olga Semenova; Peter M Richardson; Andrew J Parrott; Alison Nordon; Meghan E Halse; Simon B Duckett
Journal:  Anal Chem       Date:  2019-05-02       Impact factor: 6.986

Review 6.  Parahydrogen-Induced Hyperpolarization of Gases.

Authors:  Kirill V Kovtunov; Igor V Koptyug; Marianna Fekete; Simon B Duckett; Thomas Theis; Baptiste Joalland; Eduard Y Chekmenev
Journal:  Angew Chem Int Ed Engl       Date:  2020-08-11       Impact factor: 16.823

7.  Quantification of hyperpolarisation efficiency in SABRE and SABRE-Relay enhanced NMR spectroscopy.

Authors:  Peter M Richardson; Richard O John; Andrew J Parrott; Peter J Rayner; Wissam Iali; Alison Nordon; Meghan E Halse; Simon B Duckett
Journal:  Phys Chem Chem Phys       Date:  2018-10-10       Impact factor: 3.676

  7 in total

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