| Literature DB >> 18498194 |
Maria J Petersson1, Ian D Jenkins, Wendy A Loughlin.
Abstract
The structure of a polymer-supported version of the Hendrickson "POP" reagent, prepared by the reaction of polymer-supported triphenylphosphine oxide 1 with triflic anhydride, is established as an equilibrium mixture of polymer-supported triphenylphosphine ditriflate 3 (delta 79.4 ppm) and polymer-supported phosphonium anhydride 4 (delta 73.3 ppm). The (31)P NMR chemical shift reported previously for 3 is shown to be incorrect.Entities:
Mesh:
Substances:
Year: 2008 PMID: 18498194 DOI: 10.1021/jo800447v
Source DB: PubMed Journal: J Org Chem ISSN: 0022-3263 Impact factor: 4.354