| Literature DB >> 17962769 |
Gernot A Eller1, Wolfgang Holzer.
Abstract
Novel 3-acetyl-2-aminothiophenes were prepared from cyanoacetone and 1,4-dithianyl-2,5-diols using a modified Gewald reaction. The syntheses of the corresponding acetamides, as well as that of 3-acetyl-2-amino-5-nitrothiophene - an interesting building-block for thiophene azo dyes - are reported. Detailed spectroscopic investigations ((1)H-NMR, (13)C-NMR, MS, IR) of the obtained compounds are presented.Entities:
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Year: 2006 PMID: 17962769 PMCID: PMC6148543 DOI: 10.3390/11050371
Source DB: PubMed Journal: Molecules ISSN: 1420-3049 Impact factor: 4.411