Literature DB >> 15893899

Quantitative NMR spectroscopy--applications in drug analysis.

U Holzgrabe1, R Deubner, C Schollmayer, B Waibel.   

Abstract

NMR spectroscopy being a primary ratio method of measurement is highly suitable to evaluate the quality of drugs. NMR spectroscopy can be used for the identification of a drug substance, the identification and quantification of impurities arising from the synthesis pathway and degradation, or residual solvents as well as the determination of the content in the assay. This review gives an overview of the application of quantitative NMR spectroscopy in International Pharmacopoeias and for licensing purposes.

Mesh：

Substances：

Year:  2005        PMID： 15893899     DOI： 10.1016/j.jpba.2005.01.050

Source DB:  PubMed          Journal:  J Pharm Biomed Anal        ISSN： 0731-7085            Impact factor:   3.935


  13 in total

1.  Liquid chromatography with absorbance detection and with isotope-dilution mass spectrometry for determination of isoflavones in soy standard reference materials.

Authors:  Melissa M Phillips; Mary Bedner; Manuela Reitz; Carolyn Q Burdette; Michael A Nelson; James H Yen; Lane C Sander; Catherine A Rimmer
Journal:  Anal Bioanal Chem       Date:  2016-11-10       Impact factor: 4.142

Review 2.  Quantitative 1H NMR. Development and potential of an analytical method: an update.

Authors:  Guido F Pauli; Tanja Gödecke; Birgit U Jaki; David C Lankin
Journal:  J Nat Prod       Date:  2012-04-06       Impact factor: 4.050

3.  Real-Time Analysis of Tenofovir Release Kinetics Using Quantitative Phosphorus (31P) Nuclear Magnetic Resonance Spectroscopy.

Authors:  Vivek Agrahari; Jianing Meng; Sudhaunshu S Purohit; Nathan A Oyler; Bi-Botti C Youan
Journal:  J Pharm Sci       Date:  2017-04-13       Impact factor: 3.534

4.  2D-Cosy NMR Spectroscopy as a Quantitative Tool in Biological Matrix: Application to Cyclodextrins.

Authors:  Gilles Dufour; Brigitte Evrard; Pascal de Tullio
Journal:  AAPS J       Date:  2015-08-25       Impact factor: 4.009

5.  Chemical purity using quantitative 1H-nuclear magnetic resonance: a hierarchical Bayesian approach for traceable calibrations.

Authors:  Blaza Toman; Michael A Nelson; Katrice A Lippa
Journal:  Metrologia       Date:  2016-09-28       Impact factor: 3.157

6.  A New Realization of SI for Organic Chemical Measurement: NIST PS1 Primary Standard for Quantitative NMR (Benzoic Acid).

Authors:  M A Nelson; J F Waters; B Toman; B E Lang; A Rück; K Breitruck; M Obkircher; A Windust; K A Lippa
Journal:  Anal Chem       Date:  2018-08-16       Impact factor: 8.008

7.  Method development in quantitative NMR towards metrologically traceable organic certified reference materials used as (31)P qNMR standards.

Authors:  Michael Weber; Christine Hellriegel; Alexander Rueck; Juerg Wuethrich; Peter Jenks; Markus Obkircher
Journal:  Anal Bioanal Chem       Date:  2014-11-22       Impact factor: 4.142

8.  Quantitative proton nuclear magnetic resonance method for simultaneous analysis of fluticasone propionate and azelastine hydrochloride in nasal spray formulation.

Authors:  Amal A El-Masry; Dalia R El-Wasseef; Manal Eid; Ihsan A Shehata; Abdallah M Zeid
Journal:  R Soc Open Sci       Date:  2021-07-14       Impact factor: 2.963

Review 9.  Recommendations and Standardization of Biomarker Quantification Using NMR-Based Metabolomics with Particular Focus on Urinary Analysis.

Authors:  Abdul-Hamid Emwas; Raja Roy; Ryan T McKay; Danielle Ryan; Lorraine Brennan; Leonardo Tenori; Claudio Luchinat; Xin Gao; Ana Carolina Zeri; G A Nagana Gowda; Daniel Raftery; Christoph Steinbeck; Reza M Salek; David S Wishart
Journal:  J Proteome Res       Date:  2016-01-20       Impact factor: 4.466

10.  Quantitative Nuclear Magnetic Resonance Spectroscopy Based on PULCON Methodology: Application to Quantification of Invaluable Marine Toxin, Okadaic Acid.

Authors:  Ryuichi Watanabe; Chika Sugai; Taichi Yamazaki; Ryoji Matsushima; Hajime Uchida; Masahiro Matsumiya; Akiko Takatsu; Toshiyuki Suzuki
Journal:  Toxins (Basel)       Date:  2016-10-13       Impact factor: 4.546
View more

北京卡尤迪生物科技股份有限公司 © 2022-2023.