Literature DB >> 15861489

1H and 13C NMR identification of unexpected 3,4-dihydroquinoxalines in the syntheses of 1,5-benzodiazepine derivatives.

E M Tjiou1, E G Lhoussaine, D Virieux, A Fruchier.   

Abstract

The reaction between o-phenylenediamines, dehydroacetic acid and aromatic aldehydes is shown to give not only the expected 1,5-benzodiazepine derivative but also a 3,4-dihydroquinoxaline, the structure of which was determined by its 1H and 13C 1D and 2D NMR spectra. Copyright 2005 John Wiley & Sons, Ltd

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Year:  2005        PMID: 15861489     DOI: 10.1002/mrc.1593

Source DB:  PubMed          Journal:  Magn Reson Chem        ISSN: 0749-1581            Impact factor:   2.447


  2 in total

1.  Conformation and tautomerizm of the 2-methyl-4-pyridin-2'-yl-1,5-benzodiazepine molecule. An ab initio study.

Authors:  Nurten Tezer
Journal:  J Mol Model       Date:  2007-10-23       Impact factor: 1.810

2.  Crystal structure and Hirshfeld surface analysis of 3,4-dihydro-2-(2,4-dioxo-6-methylpyran-3-ylidene)-4-(4-pyridin-4-yl)-1,5-benzodiazepine.

Authors:  Lhoussaine El Ghayati; Youssef Ramli; Tuncer Hökelek; Mohamed Labd Taha; Joel T Mague; El Mokhtar Essassi
Journal:  Acta Crystallogr E Crystallogr Commun       Date:  2019-01-01
  2 in total

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