| Literature DB >> 12583741 |
Xiaolei Gao1, Masakazu Nakadai, Barry B Snider.
Abstract
[structure: see text] The structure of waol A has been revised from 1 to 6, the vinylogue of TAN-2483 A (5). Aldol reaction of 10b(c) with 2,4-hexadienal (11) affords 9b(c), which is subjected to iodoetherification with bis(sym-collidine)IPF(6) to provide 8b(c). Treatment with Et(3)N in CH(2)Cl(2) completes three-step syntheses of TAN-2483A (5) and waol A (6).Entities:
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Year: 2003 PMID： 12583741 DOI： 10.1021/ol0273405
Source DB: PubMed Journal: Org Lett ISSN： 1523-7052 Impact factor: 6.005