Literature DB >> 12086828

Polymer-assisted Horner-Emmons olefination using PASSflow reactors: pure products without purification.

Wladimir Solodenko1, Ulrich Kunz, Gerhard Jas, Andreas Kirschning.   

Abstract

A PASSflow protocol for the Horner-Emmons olefination of aldehydes using polymer-bound hydroxide ions in flowthrough reactors is presented which allows preparation of alkenes in very high yield with minimal purification.

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Year:  2002        PMID： 12086828     DOI： 10.1016/s0960-894x(02)00265-2

Source DB:  PubMed          Journal:  Bioorg Med Chem Lett        ISSN： 0960-894X            Impact factor:   2.823


  5 in total

1.  The flow synthesis of heterocycles for natural product and medicinal chemistry applications.

Authors:  Marcus Baumann; Ian R Baxendale; Steven V Ley
Journal:  Mol Divers       Date:  2010-10-20       Impact factor: 2.943

2.  2-Pyridinealdoxime, a new ligand for a Pd-precatalyst: application in solid-phase-assisted Suzuki-Miyaura reaction.

Authors:  Wladimir Solodenko; Christoph Brochwitz; Rudolf Wartchow; Md Abul Hashem; Kamal M Dawood; Michel Vaultier; Andreas Kirschning
Journal:  Mol Divers       Date:  2005       Impact factor: 2.943

3.  Synthesis of 9-fluorenylidenes and 9,10-phenanthrenes through palladium-catalyzed aryne annulation by o-halostyrenes and o-halo allylic benzenes.

Authors:  Shilpa A Worlikar; Richard C Larock
Journal:  J Org Chem       Date:  2009-12-04       Impact factor: 4.354

4.  Polyionic polymers--heterogeneous media for metal nanoparticles as catalyst in Suzuki-Miyaura and Heck-Mizoroki reactions under flow conditions.

Authors:  Klaas Mennecke; Andreas Kirschning
Journal:  Beilstein J Org Chem       Date:  2009-05-08       Impact factor: 2.883

5.  Palladium-catalyzed synthesis of 9-fluorenylidenes through aryne annulation.

Authors:  Shilpa A Worlikar; Richard C Larock
Journal:  Org Lett       Date:  2009-06-04       Impact factor: 6.005
  5 in total

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