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Literature DB >> 12010025

Seeking higher resolution and sensitivity for NMR of quadrupolar nuclei at ultrahigh magnetic fields.

Zhehong Gan¹, Peter Gor'kov, Timothy A Cross, Ago Samoson, Dominique Massiot.

Abstract

We report the acquisition of solid-state NMR spectra of quadrupolar nuclei obtained at very high magnetic fields (25 and 40 T), thus improving spectral sensitivity and resolution. For an example compound, the MAS spectrum obtained at 40 T is nearly free from the second-order quadrupolar broadening and can be interpreted quantitatively in a very simple manner.

Year: 2002 PMID： 12010025 DOI： 10.1021/ja025849p

Source DB: PubMed Journal: J Am Chem Soc ISSN： 0002-7863 Impact factor: 15.419

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Cited

9 in total

Review 1. Chemical shift tensor - the heart of NMR: Insights into biological aspects of proteins.

Authors: Hazime Saitô; Isao Ando; Ayyalusamy Ramamoorthy
Journal: Prog Nucl Magn Reson Spectrosc Date: 2010-05-07 Impact factor: 9.795

2. Single Scan 2D NMR Spectroscopy on a 25 T Bitter Magnet.

Authors: Boaz Shapira; Kiran Shetty; William W Brey; Zhehong Gan; Lucio Frydman
Journal: Chem Phys Lett Date: 2007-07-16 Impact factor: 2.328

3. Field-stepped ultra-wideline NMR at up to 36 T: On the inequivalence between field and frequency stepping.

Authors: Ivan Hung; Adam R Altenhof; Robert W Schurko; David L Bryce; Oc Hee Han; Zhehong Gan
Journal: Magn Reson Chem Date: 2020-12-29 Impact factor: 2.447

4. Achieving 1 ppm field homogeneity above 24 T: Application of differential mapping for shimming Keck and the Series Connected Hybrid magnets at the NHMFL.

Authors: Ilya M Litvak; Adrian Griffin; Joana Paulino; Wenping Mao; Peter Gor'kov; Kiran K Shetty; William W Brey
Journal: J Magn Reson Date: 2019-03-05 Impact factor: 2.229

5. NMR spectroscopy up to 35.2T using a series-connected hybrid magnet.

Authors: Zhehong Gan; Ivan Hung; Xiaoling Wang; Joana Paulino; Gang Wu; Ilya M Litvak; Peter L Gor'kov; William W Brey; Pietro Lendi; Jeffrey L Schiano; Mark D Bird; Iain R Dixon; Jack Toth; Gregory S Boebinger; Timothy A Cross
Journal: J Magn Reson Date: 2017-08-24 Impact factor: 2.229

Review 9. Solid State NMR Spectroscopy a Valuable Technique for Structural Insights of Advanced Thin Film Materials: A Review.

Authors: Mustapha El Hariri El Nokab; Khaled O Sebakhy
Journal: Nanomaterials (Basel) Date: 2021-06-04 Impact factor: 5.076

9 in total

Seeking higher resolution and sensitivity for NMR of quadrupolar nuclei at ultrahigh magnetic fields.

Review 1. Chemical shift tensor - the heart of NMR: Insights into biological aspects of proteins.

2. Single Scan 2D NMR Spectroscopy on a 25 T Bitter Magnet.

3. Field-stepped ultra-wideline NMR at up to 36 T: On the inequivalence between field and frequency stepping.

4. Achieving 1 ppm field homogeneity above 24 T: Application of differential mapping for shimming Keck and the Series Connected Hybrid magnets at the NHMFL.

5. NMR spectroscopy up to 35.2T using a series-connected hybrid magnet.

6. ¹⁴N overtone nuclear magnetic resonance of rotating solids.

7. Mapping the oxygen structure of γ-Al₂O₃ by high-field solid-state NMR spectroscopy.

Review 8. A Practical Review of NMR Lineshapes for Spin-1/2 and Quadrupolar Nuclei in Disordered Materials.

Review 9. Solid State NMR Spectroscopy a Valuable Technique for Structural Insights of Advanced Thin Film Materials: A Review.

Seeking higher resolution and sensitivity for NMR of quadrupolar nuclei at ultrahigh magnetic fields.

Review 1. Chemical shift tensor - the heart of NMR: Insights into biological aspects of proteins.

2. Single Scan 2D NMR Spectroscopy on a 25 T Bitter Magnet.

3. Field-stepped ultra-wideline NMR at up to 36 T: On the inequivalence between field and frequency stepping.

4. Achieving 1 ppm field homogeneity above 24 T: Application of differential mapping for shimming Keck and the Series Connected Hybrid magnets at the NHMFL.

5. NMR spectroscopy up to 35.2T using a series-connected hybrid magnet.

6. 14N overtone nuclear magnetic resonance of rotating solids.

7. Mapping the oxygen structure of γ-Al2O3 by high-field solid-state NMR spectroscopy.

Review 8. A Practical Review of NMR Lineshapes for Spin-1/2 and Quadrupolar Nuclei in Disordered Materials.

Review 9. Solid State NMR Spectroscopy a Valuable Technique for Structural Insights of Advanced Thin Film Materials: A Review.

4. Achieving 1 ppm field homogeneity above 24 T: Application of differential mapping for shimming Keck and the Series Connected Hybrid magnets at the NHMFL.

6. ¹⁴N overtone nuclear magnetic resonance of rotating solids.

7. Mapping the oxygen structure of γ-Al₂O₃ by high-field solid-state NMR spectroscopy.