Literature DB >> 11014596

Radiation damping compensation of selective pulses in water-protein exchange spectroscopy.

B Cutting1, J H Chen, D Moskau, G Bodenhausen.   

Abstract

The observation of nuclear Overhauser effects (NOEs) between bound water and biological macromolecules such as proteins and nucleic acids can be improved by inverting the water resonance selectively while compensating for radiation damping effects. The efficiency of inversion, the offset profiles, and the appearance of 2D NOE-NOESY spectra can be improved in comparison with earlier methods.

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Year:  2000        PMID: 11014596     DOI: 10.1023/a:1008303322609

Source DB:  PubMed          Journal:  J Biomol NMR        ISSN: 0925-2738            Impact factor:   2.835


  12 in total

1.  Evaluation of slaved pulses to study protein hydration.

Authors:  O Bornet; F Guerlesquin; M Piotto
Journal:  J Magn Reson       Date:  1999-05       Impact factor: 2.229

2.  Amplification of radiation damping in a 600-MHz NMR spectrometer: Application to the study of water-protein interactions.

Authors:  D Abergel; A Louis-Joseph; J Y Lallemand
Journal:  J Biomol NMR       Date:  1996-07       Impact factor: 2.835

3.  Suppression of radiation damping during selective excitation of the water signal: The WANTED sequence.

Authors:  A Böckmann; E Guittet
Journal:  J Biomol NMR       Date:  1996-07       Impact factor: 2.835

4.  Protein hydration in aqueous solution.

Authors:  G Otting; E Liepinsh; K Wüthrich
Journal:  Science       Date:  1991-11-15       Impact factor: 47.728

5.  Homonuclear 1D and 2D NMR Experiments for the Observation of Solvent-Solute Interactions

Authors: 
Journal:  J Magn Reson B       Date:  1996-09

6.  The initiation of radiation damping by noise.

Authors:  A Sodickson; W E Maas; D G Cory
Journal:  J Magn Reson B       Date:  1996-03

Review 7.  Hydrogen exchange and structural dynamics of proteins and nucleic acids.

Authors:  S W Englander; N R Kallenbach
Journal:  Q Rev Biophys       Date:  1983-11       Impact factor: 5.318

8.  Water-macromolecule interactions by NMR: a quadrature-free constant-time approach and its application to CI2.

Authors:  G Melacini; R Boelens; R Kaptein
Journal:  J Biomol NMR       Date:  1999-11       Impact factor: 2.835

9.  Water-protein NOEs: Optimized scheme for selective water excitation.

Authors:  E Liepinsh; G Otting
Journal:  J Biomol NMR       Date:  1999-01       Impact factor: 2.835

10.  Quantitative Determination of Cross-Relaxation Rates in NMR Using Selective Pulses to Inhibit Spin Diffusion

Authors: 
Journal:  J Magn Reson B       Date:  1996-04
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  2 in total

1.  SWET for secure water suppression on probes with high quality factor.

Authors:  Peter S C Wu; Gottfried Otting
Journal:  J Biomol NMR       Date:  2005-07       Impact factor: 2.835

2.  Radiation damping in modern NMR experiments: progress and challenges.

Authors:  V V Krishnan; Nagarajan Murali
Journal:  Prog Nucl Magn Reson Spectrosc       Date:  2012-06-15       Impact factor: 9.795

  2 in total

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