Literature DB >> 10329239

NMR probe for the simultaneous acquisition of multiple samples.

G Fisher1, C Petucci, E MacNamara, D Raftery.   

Abstract

A dual channel probe for the simultaneous acquisition of NMR data from multiple samples has been developed. This multiplex probe consists of two noninteracting sample coils that are each capable of detecting NMR signals at the same resonant frequency with good sensitivity and resolution. 13C free induction decays for the two samples, methanol (13C, 99%) and carbon tetrachloride (13C, 99%), were acquired simultaneously at 75.44 MHz using a single transmitter pulse and separate NMR receivers. S/N measurements are comparable to those observed using single coils. No evidence of cross talk is evident in the spectra even after considerable signal averaging. The probe demonstrates the feasibility of significant parallelism in NMR, which will be of interest in situations where high throughput analysis is desired. Copyright 1999 Academic Press.

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Year:  1999        PMID: 10329239     DOI: 10.1006/jmre.1999.1725

Source DB:  PubMed          Journal:  J Magn Reson        ISSN: 1090-7807            Impact factor:   2.229


  4 in total

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2.  Multiplexed NMR: an automated CapNMR dual-sample probe.

Authors:  James A Norcross; Craig T Milling; Dean L Olson; Duanxiang Xu; Anthony Audrieth; Robert Albrecht; Ke Ruan; John Likos; Claude Jones; Timothy L Peck
Journal:  Anal Chem       Date:  2010-09-01       Impact factor: 6.986

3.  Automated microflow NMR: routine analysis of five-microliter samples.

Authors:  Ariane Jansma; Tiffany Chuan; Robert W Albrecht; Dean L Olson; Timothy L Peck; Bernhard H Geierstanger
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4.  Design and construction of a versatile dual volume heteronuclear double resonance microcoil NMR probe.

Authors:  Ravi Kc; Ian D Henry; Gregory H J Park; Daniel Raftery
Journal:  J Magn Reson       Date:  2008-12-25       Impact factor: 2.229

  4 in total

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