| Literature DB >> 9873547 |
J J Parlow1, M L Vazquez, D L Flynn.
Abstract
A polymer-bound calcium sulfonate resin is prepared and used to sequester tetrabutylammonium fluoride. The simultaneous use of the calcium sulfonate resin with a sulfonic acid resin is used for the quenching and purification of desilylating reactions involving tetrabutylammonium fluoride as the reagent. Employment of this resin workup technique eliminates the need for a liquid-phase extractive protocol allowing the procedure to be easily automated.Entities:
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Year: 1998 PMID: 9873547 DOI: 10.1016/s0960-894x(98)00432-6
Source DB: PubMed Journal: Bioorg Med Chem Lett ISSN: 0960-894X Impact factor: 2.823