Literature DB >> 967675

An improved synthetic route to the beta-hydroxyethyl esters of 5'-nucleotides.

W S Zieliński.   

Abstract

A simple method is described for the preparation of the beta-hydroxyethyl esters of nucleoside 5'-phosphates by treatment of the appropriate 2',3'-isopropylidene nucleoside with 2-chloro-2-oxo-1,3-dioxaphospholane. Unambigous structural assignments were based on 13C nmr spectroscopy. Chemical shifts and 13C-31P spin-spin coupling constants are discussed.

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Year:  1976        PMID： 967675      PMCID： PMC343035          DOI： 10.1093/nar/3.7.1769

Source DB:  PubMed          Journal:  Nucleic Acids Res        ISSN： 0305-1048            Impact factor:   16.971


  1 in total

1.  A conformational study of adenylyl-(3',5')-adenosine and adenylyl-(2',5')-adenosine in aqueous solution by carbon-13 magnetic resonance spectroscopy.

Authors:  T Schleich; B P Cross; I C Smith
Journal:  Nucleic Acids Res       Date:  1976-02       Impact factor: 16.971
  1 in total

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