Literature DB >> 9441876

Sensitivity- and gradient-enhanced heteronuclear coupled/decoupled HSQC-TOCSY experiments for measuring long-range heteronuclear coupling constants.

K E Kövér1, V J Hruby, D Uhrín.   

Abstract

A pulsed field gradient version of the sensitivity-enhanced 2D HSQC-TOCSY experiment is proposed for measurement of long-range heteronuclear coupling constants. The coupling constants are obtained by computer-aided analysis of mixed-phase multiplets with and without the heteronuclear splitting. Generation of pure phase data is not required. Since large 1JXH and JHH couplings are used for coherence transfer, small nJXH can be measured accurately, which could be difficult to obtain from purely heteronuclear polarization transfer experiments. Copyright 1997 Academic Press.

Mesh:

Year:  1997        PMID: 9441876     DOI: 10.1006/jmre.1997.1265

Source DB:  PubMed          Journal:  J Magn Reson        ISSN: 1090-7807            Impact factor:   2.229


  9 in total

1.  Rational design of cell-permeable cyclic peptides containing a d-Pro-l-Pro motif.

Authors:  Jin Wen; Hui Liao; Kye Stachowski; Jordan P Hempfling; Ziqing Qian; Chunhua Yuan; Mark P Foster; Dehua Pei
Journal:  Bioorg Med Chem       Date:  2020-08-18       Impact factor: 3.641

2.  NMR structure analysis of uniformly 13C-labeled carbohydrates.

Authors:  Carolina Fontana; Helena Kovacs; Göran Widmalm
Journal:  J Biomol NMR       Date:  2014-04-26       Impact factor: 2.835

3.  Structural analysis of the core region of O-lipopolysaccharide of Porphyromonas gingivalis from mutants defective in O-antigen ligase and O-antigen polymerase.

Authors:  Nikolay A Paramonov; Joseph Aduse-Opoku; Ahmed Hashim; Minnie Rangarajan; Michael A Curtis
Journal:  J Bacteriol       Date:  2009-06-12       Impact factor: 3.490

4.  Identification of the linkage between A-polysaccharide and the core in the A-lipopolysaccharide of Porphyromonas gingivalis W50.

Authors:  Nikolay Paramonov; Joseph Aduse-Opoku; Ahmed Hashim; Minnie Rangarajan; Michael A Curtis
Journal:  J Bacteriol       Date:  2015-03-02       Impact factor: 3.490

5.  Aplisulfamines, new sulfoxide-containing metabolites from an aplidium tunicate: absolute stereochemistry at chiral sulfur and carbon atoms assigned through an original combination of spectroscopic and computational methods.

Authors:  Anna Aiello; Ernesto Fattorusso; Concetta Imperatore; Paolo Luciano; Marialuisa Menna; Rocco Vitalone
Journal:  Mar Drugs       Date:  2012-01-04       Impact factor: 6.085

6.  Precise measurement of long-range heteronuclear coupling constants by a novel broadband proton-proton-decoupled CPMG-HSQMBC method.

Authors:  István Timári; Tünde Z Illyés; Ralph W Adams; Mathias Nilsson; László Szilágyi; Gareth A Morris; Katalin E Kövér
Journal:  Chemistry       Date:  2015-01-08       Impact factor: 5.236

7.  A sodium channel inhibitor ISTX-I with a novel structure provides a new hint at the evolutionary link between two toxin folds.

Authors:  Mingqiang Rong; Jiangxin Liu; Meilin Zhang; Gan Wang; Gang Zhao; Guodong Wang; Yaping Zhang; Kaifeng Hu; Ren Lai
Journal:  Sci Rep       Date:  2016-07-13       Impact factor: 4.379

8.  Identification and Characterization of ShSPI, a Kazal-Type Elastase Inhibitor from the Venom of Scolopendra Hainanum.

Authors:  Ning Luan; Qiyu Zhao; Zilei Duan; Mengyao Ji; Meichen Xing; Tengyu Zhu; James Mwangi; Mingqiang Rong; Jiangxin Liu; Ren Lai
Journal:  Toxins (Basel)       Date:  2019-12-05       Impact factor: 4.546

Review 9.  Metabolic profiling as a tool for prioritizing antimicrobial compounds.

Authors:  Changsheng Wu; Young Hae Choi; Gilles P van Wezel
Journal:  J Ind Microbiol Biotechnol       Date:  2015-09-03       Impact factor: 3.346

  9 in total

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