| Literature DB >> 8885326 |
M S García Falcón1, S González Amigo, M A Lage Yusty, M J López de Alda Villaizán, J Simal Lozano.
Abstract
We developed a method for the determination of low levels of the carcinogen benzo[a]pyrene (BaP) in lipid-soluble liquid smoke (LSLS). The method consists of partitioning the LSLS (2 g) between n-hexane and DMSO, purification of the DMSO extracts on Sep-Pak C18 Plus and then Silica Plus cartridges, and determination of the BaP in the isolated extract by HPLC with fluorescence detection. Detection and quantification limits were 0.049 microgram/l (0.024 microgram/kg of LSLS) and 0.089 microgram/l (0.045 mg/kg), respectively. Recovery (87%) and CV% (< or = 1.5) were satisfactory.Entities:
Mesh：
Substances：
Year: 1996 PMID： 8885326 DOI： 10.1080/02652039609374473
Source DB: PubMed Journal: Food Addit Contam ISSN： 0265-203X