Literature DB >> 7128594

The application of 13C-NMR spectroscopy to study lipid A from Yersinia pseudotuberculosis lipopolysaccharide.

I N Krasikova, V I Gorbach, V V Isakov, T F Solov'eva, Y S Ovodov.   

Abstract

The use of 13C-NMR spectroscopy in the establishment of lipid A backbone structure from lipopolysaccharide of Yersinia pseudotuberculosis has been described. The 13C-NMR spectra of degraded lipid A and its N-acetate were obtained. The assignment of signals was made by comparison with the chemical shifts for 13C-NMR spectra of glucosaminitol, N-acetyl-glucosaminitol and their beta-1,4 and beta-1,6 disaccharides. It was shown that lipid A backbone of the lipopolysaccharide in question consists of beta-1,6-linked glucosamine disaccharide.

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Year:  1982        PMID: 7128594     DOI: 10.1111/j.1432-1033.1982.tb06786.x

Source DB:  PubMed          Journal:  Eur J Biochem        ISSN: 0014-2956


  2 in total

1.  Structure, serological specificity, and synthesis of artificial glycoconjugates representing the genus-specific lipopolysaccharide epitope of Chlamydia spp.

Authors:  O Holst; L Brade; P Kosma; H Brade
Journal:  J Bacteriol       Date:  1991-03       Impact factor: 3.490

2.  Aminopolyols from Carbohydrates: Amination of Sugars and Sugar-Derived Tetrahydrofurans with Transaminases.

Authors:  Fabiana Subrizi; Laure Benhamou; John M Ward; Tom D Sheppard; Helen C Hailes
Journal:  Angew Chem Int Ed Engl       Date:  2019-02-14       Impact factor: 15.336

  2 in total

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