Literature DB >> 6860411

High performance liquid chromatographic determination of malondialdehyde in vegetable oils.

T Hirayama, N Yamada, M Nohara, S Fukui.   

Abstract

A simple high performance liquid chromatographic (HPLC) method has been developed for determining malondialdehyde (MDA) in vegetable oils. MDA was reacted with dansyl hydrazine in an acidic medium, and the product, 1-dansyl-pyrazole, was determined by HPLC, using a Zorbax sil column with mixed mobile phase of n-hexane-methylene chloride. MDA can be determined as 1-dansyl-pyrazole by fluorometric detection at a level of 0.01 ppm in vegetable oils.

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Year:  1983        PMID: 6860411

Source DB:  PubMed          Journal:  J Assoc Off Anal Chem        ISSN: 0004-5756


  2 in total

1.  Gas chromatographic analysis of free and bound malonaldehyde in rat liver homogenates.

Authors:  T Ichinose; M G Miller; T Shibamoto
Journal:  Lipids       Date:  1989-10       Impact factor: 1.880

2.  Analysis of free malondialdehyde in photoirradiated corn oil and beef fat via a pyrazole derivative.

Authors:  K Umano; K J Dennis; T Shibamoto
Journal:  Lipids       Date:  1988-08       Impact factor: 1.880

  2 in total

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