Literature DB >> 5637426

Bis(trimethylsilyl)acetamide in the silylation of lipolysis products for gas-liquid chromatography.

W H Tallent, R Kleiman.   

Abstract

When bis(trimethylsilyl)acetamide is used to silylate lipolysates for gas-liquid chromatography, the pyridine solution containing the sample and silylating agent can be injected directly onto the column. Conversion of free fatty acids to methyl esters before silylation is unnecessary, since silyl esters elute as sharp gas-liquid chromatographic peaks.

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Year:  1968        PMID： 5637426

Source DB:  PubMed          Journal:  J Lipid Res        ISSN： 0022-2275            Impact factor:   5.922


  7 in total

1.  Quantitative determination of glycerol, mono- and diglycerides by gas liquid chromatography.

Authors:  J Blum; W R Koehler
Journal:  Lipids       Date:  1970-07       Impact factor: 1.880

2.  New sources of 9-d-hydroxy-cis-12-octadecenoic acid.

Authors:  R G Powell; R Kleiman; C R Smith
Journal:  Lipids       Date:  1969-11       Impact factor: 1.880

3.  Glyceride structure of Erlangea tomentosa seed oil, a new source of vernolic acid.

Authors:  B E Phillips; C R Smith; J W Hagemann
Journal:  Lipids       Date:  1969-11       Impact factor: 1.880

4.  Gas-liquid chromatography of monoglycerides and diglycerides.

Authors:  R Watts; R Dils
Journal:  Biochem J       Date:  1968-12       Impact factor: 3.857

5.  Retarded hydrolysis by pancreatic lipase of seed oils with trans-3 unsaturation.

Authors:  R Kleiman; F R Earle; W H Tallent; I A Wolff
Journal:  Lipids       Date:  1970-06       Impact factor: 1.880

6.  Structure and intraglyceride distribution of coriolic acid.

Authors:  W H Tallent; J Harris; G F Spencer; I A Wolff
Journal:  Lipids       Date:  1968-09       Impact factor: 1.880

7.  Gas chromatographic resolution of homologous monoacyl and monoalkylglycerols.

Authors:  J J Myher; A Kuksis
Journal:  Lipids       Date:  1974-06       Impact factor: 1.880
  7 in total

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