| Literature DB >> 36079289 |
Qiang Leng1,2, Qingliang Chang1,2, Yuantian Sun1,2, Biao Zhang1,2, Jianzhuang Qin1,2.
Abstract
Gangue paste material is mainly composed of coal gangue with particle size, which is mixed with cement. Fly ash and additives can be added to change its performance. In this paper, the influence of each component on the mechanical properties of gangue paste material was studied by an orthogonal experiment. The conversion relationship among various indexes of mechanical properties of gangue paste material and the response surface prediction model were discussed. The results show that the mechanical properties of gangue paste materials are positively correlated with the content of cement, the content of fly ash and the mass concentration, which increase with the increase of the three factors, and show the primary and secondary relationship of the content of cement > the content of fly ash > the mass concentration. A response surface prediction model of mechanical property parameters is established, which includes the first order term of the influencing factors of gangue paste material and the first order interaction term between any two factors. In the response surface prediction model of uniaxial compressive strength, splitting tensile strength, cohesion and elastic modulus, the goodness of fit test coefficients are 0.998, 0.957, 0.970 and 0.997, respectively, which proves that the model has good goodness of fit. The research results provide basic parameters for paste filling mining practice, and also provide the basis for numerical simulation of filling body value.Entities:
Keywords: gangue paste material; mechanical properties; response surface
Year: 2022 PMID: 36079289 PMCID: PMC9457201 DOI: 10.3390/ma15175904
Source DB: PubMed Journal: Materials (Basel) ISSN: 1996-1944 Impact factor: 3.748
Main components and contents of fly ash.
| Component | SiO2 | Al2O3 | CaO | Fe2O3 | C |
|---|---|---|---|---|---|
| Content | 48.8% | 20.3% | 2.2% | 6.2% | 9.9% |
Figure 1The raw materials.
Physical properties of SL cement.
| Consistency of Clean Pulp | Volume Stability | Fineness/% | Setting Time/h:min | |
|---|---|---|---|---|
| Initial Setting | Final Coagulation | |||
| 23 | Stable | 4.00 | 2:00 | 5:00 |
Mechanical properties of SL cement.
| Flexural Strength/MPa | UCS/MPa | Flexural Compression Ratio | ||||||
|---|---|---|---|---|---|---|---|---|
| 3 d | 7 d | 28 d | 3 d | 7 d | 28 d | 3 d | 7 d | 28 d |
| 6.76 | 6.85 | 7.03 | 37.3 | 40.9 | 43.1 | 0.10 | 0.17 | 0.16 |
Figure 2Grain size distribution of gangue in Gaohe coal mine.
Level table of orthogonal factors.
| Level of Orthogonal | Influence Factor | ||
|---|---|---|---|
| Mass Concentration | Cement Content | Fly Ash | |
| Level 1 | 83 | 125 | 0 |
| Level 2 | 84 | 175 | 50 |
| Level 3 | 85 | 225 | 100 |
Orthogonal test scheme.
| No. | Mass Concentration | Cement Content | Fly Ash | PA (kg/m3) | HA (kg/m3) | Slump (mm) | Expansion Degree |
|---|---|---|---|---|---|---|---|
| GH-1 | 83 | 125 | 0 | 3 | 5 | 240 | 500 |
| GH-2 | 83 | 175 | 50 | 3 | 5 | 260 | 580 |
| GH-3 | 83 | 225 | 100 | 3 | 5 | 265 | 620 |
| GH-4 | 84 | 125 | 50 | 3 | 5 | 255 | 590 |
| GH-5 | 84 | 175 | 100 | 3 | 5 | 265 | 550 |
| GH-6 | 84 | 225 | 0 | 3 | 5 | 268 | 610 |
| GH-7 | 85 | 125 | 100 | 3 | 5 | 255 | 595 |
| GH-8 | 85 | 175 | 0 | 3 | 5 | 250 | 510 |
| GH-9 | 85 | 225 | 50 | 3 | 5 | 236 | 410 |
Figure 3The prepared samples.
Parameters and application of test piece.
| Size | Quantity | Function |
|---|---|---|
| 100 mm × 100 mm × 100 mm | There are 6 for each ratio, and 54 specimens in total | 27 for cube compression test; 27 for splitting tensile test |
| 50 mm × 100 mm cylindrical | There are 3 for each ratio, and 27 specimens in total | Determination of elastic modulus and Poisson’s ratio |
Figure 4Failure mode of gangue paste material under uniaxial compression. (a) Failure mode of cube specimen under compression. (b) Failure mode of cylindrical specimen under compression.
Test values of mechanical parameters of gangue paste materials.
| No. | UCS (MPa) | Splitting Tensile Strength (MPa) | Cohesion | Friction Angle | Elastic Modulus | Poisson’s Ratio |
|---|---|---|---|---|---|---|
| GH-1 | 3.00 | 0.60 | 0.55 | 25.1 | 318.20 | 0.12 |
| GH-2 | 6.37 | 1.18 | 0.93 | 25.9 | 618.64 | 0.16 |
| GH-3 | 9.33 | 1.51 | 1.40 | 25.9 | 1028.23 | 0.10 |
| GH-4 | 3.89 | 0.72 | 0.76 | 18.0 | 542.06 | 0.22 |
| GH-5 | 7.41 | 1.19 | 1.06 | 28.1 | 924.58 | 0.10 |
| GH-6 | 8.37 | 1.25 | 1.19 | 26.3 | 778.57 | 0.20 |
| GH-7 | 5.07 | 1.00 | 0.79 | 24.3 | 573.54 | 0.21 |
| GH-8 | 6.54 | 1.12 | 1.00 | 26.1 | 707.08 | 0.17 |
| GH-9 | 10.16 | 1.61 | 1.72 | 23.1 | 1218.87 | 0.10 |
Range analysis of factors influencing mechanical properties of gangue paste materials.
| Index | UCS | Splitting Tensile Strength | Cohesion | ||||||
|---|---|---|---|---|---|---|---|---|---|
| Mass Concentration | Cement Content | Fly Ash Content | Mass Concentration | Cement Content | Fly Ash Content | Mass Concentration | Cement Content | Fly Ash Content | |
|
| 6.23 | 3.99 | 5.97 | 1.10 | 0.77 | 0.99 | 0.96 | 0.70 | 0.91 |
|
| 6.56 | 6.77 | 6.81 | 1.09 | 1.16 | 1.17 | 1.00 | 1.00 | 1.14 |
|
| 7.26 | 9.29 | 7.27 | 1.24 | 1.46 | 1.23 | 1.17 | 1.44 | 1.08 |
|
| 1.03 | 5.30 | 1.30 | 0.15 | 0.69 | 0.24 | 0.21 | 0.74 | 0.23 |
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| 25.6 | 22.5 | 25.8 | 655.02 | 477.93 | 601.28 | 0.13 | 0.18 | 0.16 |
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| 24.1 | 26.7 | 22.3 | 748.40 | 750.10 | 793.19 | 0.17 | 0.14 | 0.16 |
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| 24.5 | 25.1 | 26.1 | 833.16 | 1008.56 | 842.12 | 0.16 | 0.13 | 0.14 |
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| 1.5 | 4.2 | 3.8 | 178.14 | 530.63 | 240.84 | 0.04 | 0.05 | 0.02 |
Variance analysis of factors influencing mechanical properties of gangue paste materials.
| Sources of Volatility | UCS (MPa) | Splitting Tensile Strength (MPa) | Cohesion (MPa) | ||||||
|---|---|---|---|---|---|---|---|---|---|
| Sum of Squares of Deviations (SS) | F Value | Critical Test Value (Fa) | Sum of Squares of Deviations (SS) | F Value | Critical Test Value (Fa) | Sum of Squares of Deviations (SS) | F Value | Critical Test Value (Fa) | |
| Mass concentration | 1.642 | 11.95 | F0.05 (2, 8) = 4.46 | 0.059 | 54.63 | F0.05 (2, 8) = 4.46 | 0.074 | 2.48 | F0.05 (2, 8) = 4.46 |
| Cement content | 42.172 | 307.03 | F0.01 (2, 8) = 8.65 | 0.705 | 647.53 | F0.01 (2, 8) = 8.65 | 0.824 | 27.70 | F0.01 (2, 8) = 8.65 |
| Fly ash content | 2.605 | 18.96 | F0.1 (2, 8) = 3.11 | 0.096 | 87.82 | F0.1 (2, 8) = 3.11 | 0.082 | 2.74 | F0.1 (2, 8) = 3.11 |
| Error, c | 0.137 | 0.011 | 0.030 | ||||||
| Sum | 46.556 | 0.861 | 1.010 | ||||||
| Sources of Volatility | Friction Angle (°) | Elastic Modulus (MPa) | Poisson’s Ratio | ||||||
| Sum of Squares of Deviations (SS) | F Value | Critical Test Value (Fa) | Sum of Squares of Deviations (SS) | F Value | Critical Test Value (Fa) | Sum of Squares of Deviations (SS) | F Value | Critical Test Value (Fa) | |
| Mass concentration | 3.669 | 0.40 | F0.05 (2, 8) = 4.46 | 47,638 | 1.16 | F0.05 (2, 8) = 4.46 | 0.003 | 0.32 | F0.05 (2, 8) = 4.46 |
| Cement content | 27.416 | 3.01 | F0.01 (2, 8) = 8.65 | 422,436 | 10.30 | F0.01 (2, 8) = 8.65 | 0.004 | 0.39 | F0.01 (2, 8) = 8.65 |
| Fly ash content | 26.509 | 2.91 | F0.1 (2, 8) = 3.11 | 97,223 | 2.37 | F0.1 (2, 8) = 3.11 | 0.001 | 0.12 | F0.1 (2, 8) = 3.11 |
| Error, c | 9.109 | 40,995 | 0.011 | ||||||
| Sum | 66.702 | 608,292 | 0.020 | ||||||
Figure 5Relationship between cube compressive strength and splitting tensile strength.
Figure 6Relationship between cube compressive strength and cohesion.
Figure 7Relationship between cube compressive strength and elastic modulus.
Figure 8Response surface of different factors to each index.
Variance analysis of prediction model for mechanical properties of gangue paste materials.
| Variation | UCS (MPa) | Splitting Tensile Strength (MPa) | Cohesion | ||||||
|---|---|---|---|---|---|---|---|---|---|
| Sum of Squares | R2 | Sum of Squares | R2 | Sum of Squares | R2 | ||||
| Model | 46.450 | 0.007 | 0.998 | 0.820 | 0.122 | 0.957 | 0.980 | 0.087 | 0.970 |
| x1 | 0.750 | 0.062 | 0.020 | 0.405 | 0.055 | 0.197 | |||
| x2 | 18.200 | 0.003 | 0.310 | 0.054 | 0.370 | 0.039 | |||
| x3 | 1.640 | 0.030 | 0.043 | 0.265 | 0.047 | 0.218 | |||
| x1x2 | 0.091 | 0.314 | 1.93 × 10−4 | 0.928 | 0.011 | 0.477 | |||
| x1x3 | 1.371 × 10−3 | 0.885 | 2.143 × 10−5 | 0.976 | 1.167 × 10−4 | 0.938 | |||
| x2x3 | 2.288 × 10−3 | 0.853 | 9.524 × 10−4 | 0.841 | 7.202 × 10−3 | 0.560 | |||
| Residual | 0.100 | 0.037 | 0.030 | ||||||
| Net error | 46.560 | 0.860 | 1.010 | ||||||
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| Model | 65.150 | 0.604 | 0.735 | 6.062 × 105 | 0.011 | 0.997 | 0.017 | 0.329 | 0.875 |
| x1 | 3.460 | 0.642 | 27,749.060 | 0.036 | 2.881 × 10−4 | 0.677 | |||
| x2 | 30.520 | 0.249 | 1.448 × 105 | 0.007 | 3.086 × 10−3 | 0.255 | |||
| x3 | 50.270 | 0.175 | 91,202.260 | 0.012 | 1.61 × 10−3 | 0.372 | |||
| x1x2 | 37.720 | 0.215 | 20,315.680 | 0.049 | 6.095 × 10−4 | 0.555 | |||
| x1x3 | 20.440 | 0.318 | 4318.630 | 0.182 | 4.024 × 10−4 | 0.626 | |||
| x2x3 | 13.710 | 0.393 | 881.740 | 0.459 | 3.438 × 10−3 | 0.237 | |||
| Residual | 23.550 | 2127.330 | 2.467 × 10−3 | ||||||
| Net error | 88.700 | 6.083 × 105 | 0.020 | ||||||