Literature DB >> 35787581

Serial macromolecular crystallography at ALBA Synchrotron Light Source. Erratum.

Jose M Martin-Garcia1, Sabine Botha2, Hao Hu2, Rebecca Jernigan1, Albert Castellví3, Stella Lisova2, Fernando Gil4, Barbara Calisto4, Isidro Crespo4, Shatabdi Roy-Chowdhury1, Alice Grieco5, Gihan Ketawala1, Uwe Weierstall1, John Spence1, Petra Fromme1, Nadia Zatsepin1, Dirk Roeland Boer4, Xavi Carpena4.   

Abstract

A revised version of Table 2 of Martin-Garcia et al. [J. Synchrotron Rad. (2022). 29, 896-907] is provided. open access.

Entities:  

Keywords:  ALBA; LCP; XALOC; microcrystal; serial synchrotron crystallography; viscous jet

Year:  2022        PMID: 35787581      PMCID: PMC9255580          DOI: 10.1107/S1600577522005185

Source DB:  PubMed          Journal:  J Synchrotron Radiat        ISSN: 0909-0495            Impact factor:   2.557


The PDB code for phycocyanin given in Table 2 ▸ in the paper by Martin-Garcia et al. (2022 ▸) was incorrectly given as 7s4z. The correct code is 7s50. The full correct table is shown below.
Table 2

Data refinement statistics (values in parentheses are for the high-resolution shell)

 LysozymeProteinase KPhycocyaninα-Spectrin-SH3Insulin
Resolution range (Å)35.35–2.1 (2.16–2.10)44.21–1.9 (1.95–1.9)43.4–2.1 (2.16–2.1)32.6–2.1 (2.16–2.1)24.35–1.71
Completeness (%)100 (100)100 (100)99.2 (90.0)99.1 (88.1)99.7 (96.0)
No. of reflections, working set6723 (479)19879 (1431)22830 (1530)4110 (264)8163 (584)
No. of reflections, test set741 (59)1071 (79)1185 (78)503 (33)908 (56)
Rwork (%)17.916.530.519.424.0
Rfree (%)23.219.634.723.925.8
No. of atoms     
Protein100120682488462808
Ions12203
Ligands0413800
Water178943515
Total101921632671467826
R.m.s. deviations     
Bonds (Å)0.0100.0110.0050.0120.006
Angles (°)1.5821.5961.1621.8261.271
Average B-factors (Å2)     
Protein46.930.453.962.133.0
Ions64.533.092.8035.1
Ligands055.357.600
Water40.035.147.459.734.2
Ramachandran plot     
Favoured (%)96.196.097.698.294.7
Allowed (%)3.93.62.11.84.3
PDB code 7s4w 7s4z 7s50 7s4r 7s4y
  1 in total

1.  Serial macromolecular crystallography at ALBA Synchrotron Light Source.

Authors:  Jose M Martin-Garcia; Sabine Botha; Hao Hu; Rebecca Jernigan; Albert Castellví; Stella Lisova; Fernando Gil; Barbara Calisto; Isidro Crespo; Shatabdi Roy-Chowdhury; Alice Grieco; Gihan Ketawala; Uwe Weierstall; John Spence; Petra Fromme; Nadia Zatsepin; Dirk Roeland Boer; Xavi Carpena
Journal:  J Synchrotron Radiat       Date:  2022-04-04       Impact factor: 2.557

  1 in total

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