Wei Wang1, Weizhen Li2, Shuang Xu2. 1. College of Chemistry and Chemical Engineering, Yulin University, Yulin 719000, Shaanxi, P. R. China. 2. Oil Production Plant No. 1, Petrochina Changqing Oilfeld Company, Yan'an, 716000, Shaanxi, P. R. China.
Abstract
Pore structure characteristics of tight sandstones, including pore types, connectivity, and morphological features, provides a basis for selecting the "sweet spot" in tight sandstone reservoirs. A variety of research methods, high-pressure mercury intrusion porosimetry, cast thin sections, scanning electron microscopy, and fractal theory were integrated to explore these parameters of tight sandstones from the Chang 7 member of the Triassic Yanchang Formation in the Ordos Basin, China. Results indicate that tight sandstones are defined by three pore types with distinct fractal dimensions and corresponding pore structure, which are combined pores, isolated grain pores, and clay-dominated pores. The pore spaces of the three types gradually evolve from the microscale to the nanoscale. Combined pores were formed by dissolution pores connected to the surrounding pores and have been distinguished by their irregular shape. Their connected paths are multidirectional, resulting in better connectivity. Isolated grain pores have a small number of poorly connected paths, which causes weak connectivity. Clay-dominated pores have narrow and complex connected paths, resulting in poor connectivity. From the combined pore to the clay-dominated pore, the fractal dimensions of pore spaces decrease, indicating that the heterogeneity of pore spaces is gradually weakened whereas the heterogeneity of the flow characteristics is gradually enhanced. On the basis of the proportions of the three pore types, the tight sandstones can be genetically classified into a combined pore type, an isolated grain pore type, and a clay-dominated pore type. The differences in pore space and heterogeneity affect the distribution of tight oil; therefore, sand bodies located near the source rock, characterized by strong dissolution and dominated by the combined pore type, are favorable zones for tight sandstone reservoirs.
Pore structure characteristics of tight sandstones, including pore types, connectivity, and morphological features, provides a basis for selecting the "sweet spot" in tight sandstone reservoirs. A variety of research methods, high-pressure mercury intrusion porosimetry, cast thin sections, scanning electron microscopy, and fractal theory were integrated to explore these parameters of tight sandstones from the Chang 7 member of the Triassic Yanchang Formation in the Ordos Basin, China. Results indicate that tight sandstones are defined by three pore types with distinct fractal dimensions and corresponding pore structure, which are combined pores, isolated grain pores, and clay-dominated pores. The pore spaces of the three types gradually evolve from the microscale to the nanoscale. Combined pores were formed by dissolution pores connected to the surrounding pores and have been distinguished by their irregular shape. Their connected paths are multidirectional, resulting in better connectivity. Isolated grain pores have a small number of poorly connected paths, which causes weak connectivity. Clay-dominated pores have narrow and complex connected paths, resulting in poor connectivity. From the combined pore to the clay-dominated pore, the fractal dimensions of pore spaces decrease, indicating that the heterogeneity of pore spaces is gradually weakened whereas the heterogeneity of the flow characteristics is gradually enhanced. On the basis of the proportions of the three pore types, the tight sandstones can be genetically classified into a combined pore type, an isolated grain pore type, and a clay-dominated pore type. The differences in pore space and heterogeneity affect the distribution of tight oil; therefore, sand bodies located near the source rock, characterized by strong dissolution and dominated by the combined pore type, are favorable zones for tight sandstone reservoirs.
With the development of
exploration technologies and the depletion
of conventional oil reserves, tight sandstone reservoirs have become
the focus of global oil and gas exploration.[1−3] The main factors
influencing a well’s performance in tight sandstone are the
pore structures and the connectivity.[4,5] Because tight
sandstone is affected by diagenesis, its pore structure is characterized
by a complex and irregular pore shape, various connectivities, and
strong heterogeneity, thus the identification of reservoir space types
and heterogeneity and the quantification of their contribution to
the storage capacity are the bases for predicting the enrichment and
development of tight sandstone reservoirs.[6−8]Pore structures
of tight sandstone have been measured by many methods,
and the parameters of the pore throat, such as the pore radius, pore
size distribution, and sorting coefficient, were obtained. Although
these parameters clarified the pore structure of tight sandstone,
they ignored the evolution of the reservoir pore space and the corresponding
change in heterogeneity and did not quantify the contribution of different
types of reservoir space to the physical properties. The study of
reservoir space evolution (including pore type and size) is not only
helpful for evaluating the storage and connectivity of tight reservoirs
but also can effectively guide the prediction of favorable areas for
tight sandstone reservoirs. However, traditional experimental methods
and parameters are not able to comprehensively measure the heterogeneity
and pore structure.[9,10] Therefore, a more modern approach
is necessary to understand the microscopic pore structure, specifically
by combining the theoretical methods with the experimental ones.During the past few years, several techniques have been used to
characterize the pore structure of tight sandstone, including X-ray-computed
tomography, nuclear magnetic resonance, rate-controlled porosimetry,
low-pressure gas adsorption (LPGA), and small-angle and ultrasmall-angle
neutron scattering (SANS/USANS).[10−15] Although these methods play an important role in exploring the pore
structures, all of these techniques have limitations to the experimental
method or are too expensive for routine use.[16−20] However, high-pressure mercury intrusion porosimetry
(HMIP) can identify microscale and nanoscale pores and is widely used
to measure the pore size distribution in rocks because of its high
injection pressure.[21]Fractal theory
is an effective method of nonlinear mathematics
that can characterize intricate phenomena, and it is used to explicate
system characteristics of irregular, unstable, and complex structures.[22−24] The fractal dimension (D) is the expression of
fractal characteristics and contributes to the quantitative measurement
of the irregularity of pore structures.[25−28] It build a link between morphological
features and physical properties. Many scholars have successfully
applied fractal theory to investigate the pore structure of coal and
sandstone.[29,30] The increase in the fractal dimension
indicates rough surfaces and complex structure of the pore space,
and the decreasing in the fractal dimension indicates a regular shape
and a smooth pore surface.[19,31,32] The fractal dimension is an important symbol to characterize the
pore structure. The fractal dimension can demonstrate the mercury
filling process of particle samples and depict the features of the
pore structure.[33] Different values of the
fractal dimension correspond to specific stages of the mercury intrusion
process and can be used to distinguish among intergranular voids,
intragranular voids, and matrix compressibility during pore filling.[34,35] Hence, the fractal dimension is a significant parameter for evaluating
the heterogeneity and complexity of the pore structure, and it is
used to identify pore types with distinct morphological features in
tight sandstones. Because of differences in testing principles and
pore models, there are some differences in the fractal dimensions
calculated with different techniques.[26,36]In this
study, we used HMIP, cast thin sections, scanning electron
microscopy (SEM), and fractal methods to investigate the pore space
evolution, heterogeneity, and effect on physical properties of tight
sandstone from the Triassic Yanchang Formation in the Ordos Basin,
China. Pore types and corresponding pore structures in the tight sandstones
have been identified. The contributions of different pore types to
the physical properties were quantified. The pore structure and connectivity
characteristics of different tight sandstone types were discussed.
The obtained results provide insights regarding oil migration and
distribution in tight sandstone.
Materials
and Methods
Sampling and Sample Preparation
For
this study, tight sandstone samples were collected from the Chang
7 Member of the Triassic Yanchang Formation in the Ordos Basin, China
(Figure A). The Chang
7 subsection is a semideep and deep lake deposit with tight sandstone
that developed adjacent to the source rocks (Figure B).[37] The acid
fluid from the source rock migrated into the Chang 7 tight sandstone,
resulting in the extensive dissolution of the tight sandstone.[38]
Figure 1
Geological and lithological features of the Ordos Basin.
(a) Location
and tectonic units of the research area and (b) stratigraphic column
of the Chang 7 member.
Geological and lithological features of the Ordos Basin.
(a) Location
and tectonic units of the research area and (b) stratigraphic column
of the Chang 7 member.Ten 2.5-cm-diameter cylindrical
core plugs were drilled parallel
to the bedding surface of the tight sandstone. Residuals were removed
from all of the samples, after which they were dried under vacuum
at 105 °C for 24 h. Each core plug was then analyzed using helium
porosity and nitrogen permeability tests and then divided into three
parts for thin-section, SEM, and HMIP analyses to determine the microscopic
and fractal characteristics of the pore space of the tight sandstones.
Experimental Methods
Thin-Section
Analysis
Thin sections
were impregnated with red epoxy resins and then analyzed to determine
their petrological characteristics and pore origin. Petrographic images
were captured using a Leica DLC-420 microscope camera system.
Scanning Electron Microscopy (SEM)
An FEI Quanta 400
FEG SEM was used to examine the pore structure
of broken fragments from samples with fresh surfaces. Samples were
coated with gold and used for secondary electron imaging (SE), backscattering
electron imaging (BSE), and energy-dispersive spectroscopy (EDS) mineral
identification. The accelerating voltage and SEM resolution were 30
kV and 1.2 nm, respectively.
The HMIP is a pore-size measurement technique that
uses the penetration of a nonwetting liquid (in this case, mercury)
to measure the size and volume of pores in porous solids (in this
case, sandstone). When mercury is injected into the porous sample,
capillary pressure prevents the mercury from invading the pore space.
Therefore, the injection pressure is required to overcome the capillary
resistance, and each injection pressure of mercury corresponds to
the capillary pressure of the pore with the corresponding size. The
volume of mercury represents the volume of the connected pore space.An Autopore 9420 mercury porosimeter was used to perform HMIP on
the collected samples. Using a maximum displacement pressure of 200
MPa, the HMIP analysis determined the capillary pressure curves of
the sandstone samples during mercury intrusion. After reaching the
maximum pressure, the displacement pressure is gradually decreased
to allow for mercury extrusion from the samples. The intrusion and
extrusion mercury curves are obtained on the basis of pressure data
and corresponding mercury saturation.Because the pore size
and pore connectivity control the capillary
pressure, the capillary pressure curve can reflect the pore structure.
The pore diameter was evaluated using the Washburn equation as seen
in eq , with an air/mercury
surface tension of 480 dyn/cm and a contact angle of 140°. These
HMIP measurements can identify pore sizes larger than 3.6 nmwhere Pc is the capillary pressure in MPa, θ is the contact
angle in degrees, σ is the air/mercury surface tension in N/m,
and r is the pore radius in μm.
Fractal Method
If the pore space
has fractal characteristics, then the number of pores (N(r)) with a radius greater than r can be mathematically expressed according to fractal theory as the
function[22,39,40]where r is the pore radius
and D is the fractal dimension. For mercury porosimetry, eq can be inferred as followswhere VHg is the mercury intrusion saturation corresponding to the
capillary pressure (Pc). We combined eqs and 4 to obtain the fractal dimension, D (eq ), as followswhere K is the line slope
for plotting the double logarithm of dVHg/dPc versus Pc.
Results and Discussion
Petrophysical
Characteristics
Table shows the mineral
compositions of the samples. The tight sandstone of the Chang 7 subsection
is dominated by feldspathic lithic sandstone (Figure A). The rock components mainly consist of
feldspar and quartz, followed by rock fragments. The cement is mainly
authigenic clay minerals (chlorite, kaolinite, and illite) and carbonate
(Figure B,C).
Table 1
Petrophysical Properties of the Eight
Tight Sandstone Samples
samples
well name
lithology
depth (m)
porosity (%)
permeability (× 10–3 μm2)
G1
H57
fine-grained feldspathic sandstone
2358
11.1
0.27
G2
CH54
fine-grained feldspathic sandstone
2229
10.8
0.21
G3
CH36
fine-grained feldspathic sandstone
2348
9.4
0.18
G4
H198
fine-grained feldspathic sandstone
2350
11.1
0.21
G5
A8
fine-grained feldspathic sandstone
2164
10.5
0.17
G6
A9
fine-grained feldspathic sandstone
2223
10.3
0.19
G7
G25
fine-grained feldspathic sandstone
2542
9.5
0.20
G8
CH79
fine-grained feldspathic sandstone
2342
9.2
0.13
Figure 2
Microscopic characteristics and pore types of
the tight sandstone
samples. (A) Feldspathic lithic sandstone in sample G1. (B) Pore-filling
kaolinite in sample G3. (C) Pore-bridging illite in sample G4. (D)
Intergranular pores and dissolution pores in sample G5. (E) Combined
pores formed by dissolution pores connected to surrounding pores in
sample G2. (F) Clay-dominated pores of chlorite in sample G10.
Microscopic characteristics and pore types of
the tight sandstone
samples. (A) Feldspathic lithic sandstone in sample G1. (B) Pore-filling
kaolinite in sample G3. (C) Pore-bridging illite in sample G4. (D)
Intergranular pores and dissolution pores in sample G5. (E) Combined
pores formed by dissolution pores connected to surrounding pores in
sample G2. (F) Clay-dominated pores of chlorite in sample G10.On the basis of the origin of the Chang 7 tight
sandstone, its
pores are predominately intergranular, dissolution, and clay. Intergranular
pores are formed by primary pores that remain after compaction and
cementing of the clastic particles, and they are polygon-shaped with
straight edges (Figure D). Dissolution pores form as a result of the corrosion by acidic
fluid within the particles, and they have an ink bottle shape (Figure D). Dissolution pores
can connect with the surrounding pores to form combined pores with
irregular shapes and large radii (Figure E). Authentic clay that occurs in the intergranular
pores and dissolution pores form clay-dominated pores[41] (Figure F).The porosity values of the samples range from 7.2 to 11.5%,
with
an average of 9.9%. The permeability values of the samples range from
0.13 × 10–3 to 0.27 × 10–3 μm2, with an average of 0.20 × 10–3 μm2 (Table ). An increase in porosity has a corresponding increase in
permeability (Figure ). This correlation between porosity and permeability indicates good
pore connectivity, and a few microfractures also exist in the tight
sandstone.
Figure 3
Porosity values versus permeability values of samples.
Porosity values versus permeability values of samples.
Characteristics of Mercury Curves from HMIP
The HMIP is an effective method for obtaining pore connectivity,
which directly influences the fluid flow in porous materials.[42]Figure shows the HMIP curves of the eight samples. The mercury intrusion
saturation increased rapidly when the pressure was low. This indicates
that a large amount of mercury enters the large pores and that the
connectivity of the large pores is good. As the pressure is further
increased (Pc > 40 MPa), the mercury
intrusion
saturation increases slowly, indicating that the connectivity of the
small pores is poor. The characteristics of the mercury curves indicate
that there was significant variation in the pore structure of the
tight sandstone.
Figure 4
Intrusion and extrusion mercury curves of HMIP.
Intrusion and extrusion mercury curves of HMIP.The pore sizes of the sample can be calculated
and the pore size
distribution (PSD) can be obtained by combining the mercury intrusion
curves. The pore size distributions of the tight sandstone in this
study mainly range from 3.6 nm to 0.6 μm (Figure ), and the pore distribution ranges from
the microscale to the nanoscale. The PSD curves show evident fluctuations,
which means that the pore throat distribution is highly heterogeneous.
Figure 5
Pore size
distribution based on HMIP.
Pore size
distribution based on HMIP.
Pore Type Identification Based on Fractal
Dimensions
Fractal dimensions can be used to characterize
the heterogeneity of space. The larger the fractal dimensions, the
more heterogeneous the space.[43] Fractal
dimensions can specifically be used to distinguish the pore space
of the tight sandstones.The log(dVp/dP)–log(P) plots that have been obtained
from the HMIP curves of the eight samples have two obvious turning
points, which divided the plots into three stages (Figure ). Fractal dimensions D1, D2, and D3 are derived
from three stages with all p values being less than
0.05 (Table ), indicating
that the pores of the Chang 7 samples have three types of fractal
features which can be identified by calculating the principle fractal
dimensions. The related values of the fractal dimensions are shown
in Table .
Figure 6
Plots of log(dVp/dP) versus log(P) and
the linear fitting results for the three stages.
(A–H) Samples G1–G8, respectively.
Table 2
Fractal Dimension Value and Related
Parameters for Three Stages of MICP
D
K
P value
samples
D1a
D2b
D3c
K1d
K2e
K3f
P1g
P2h
P3i
G1
5.5635
2.3897
1.9333
1.5635
–1.6103
–2.0667
0.0017
0.0001
0.0450
G2
7.3749
2.8372
1.8713
3.3749
–1.1628
–2.1287
0.0094
0.0001
0.0001
G3
6.6017
2.5354
1.8366
2.6017
–1.4646
–2.1634
0.0007
0.0001
0.0001
G4
5.3937
2.7591
1.7831
1.3937
–1.2409
–2.2169
0.0050
0.0001
0.0146
G5
6.4147
2.8054
1.6038
2.4147
–1.1946
–2.3962
0.0220
0.0001
0.0006
G6
5.4113
2.6618
1.9802
1.4113
–1.3382
–2.0198
0.0043
0.0001
0.0047
G7
6.4210
2.8177
1.5796
2.4210
–1.1823
–2.4204
0.0347
0.0001
0.0050
G8
4.9335
2.8785
1.6002
0.9335
–1.1215
–2.3998
0.0030
0.0001
0.0005
Fractal dimension of stage A.
Fractal dimension of stage B.
Fractal dimension of stage C.
Slope of the fitted line of stage
A.
Slope of the fitted line
of stage
B.
Slope of the fitted line
of stage
C.
P value
in the
linear regression analysis of stage A.
P value in the
linear regression analysis of stage B.
P value in the
linear regression analysis of stage C.
Plots of log(dVp/dP) versus log(P) and
the linear fitting results for the three stages.
(A–H) Samples G1–G8, respectively.Fractal dimension of stage A.Fractal dimension of stage B.Fractal dimension of stage C.Slope of the fitted line of stage
A.Slope of the fitted line
of stage
B.Slope of the fitted line
of stage
C.P value
in the
linear regression analysis of stage A.P value in the
linear regression analysis of stage B.P value in the
linear regression analysis of stage C.The D1 value of the samples ranges
from 4.9335
to 7.3749 with an average of 6.0143, with D1 being
larger than 3. Any D > 3 has no geometrical meaning
for pore spaces in fractal theory.[44] According
to previous studies, D > 3 can be attributed to
many
factors, such as compression and rupture of the matrix, microfracturing,
and oversimplification of the pore space and skin effect.[18,21,45]For the Chang 7 tight sandstone,
the pressure corresponding to
stage A is low, the microfractures are not developed, and the P values of the linear regression analysis corresponding
to stage A are less than 0.05. This indicates that pores with large
reservoir spaces are present and that the strong heterogeneity can
be represented by the fractal characteristics.On the basis
of the thin section and SEM analyses, we found that
the dissolution pores connect with the surrounding pores, forming
combined pores with a large, complex storage space (Figure A). The radius of the combined
pores is large, and the fluid can easily flow into these large combined
pore spaces, resulting in a rapid increase in mercury saturation at
low pressures, and high values of log(dVp/dP)/log(P). Stage A corresponds to mercury
filling the combined pores, which have irregular bottleneck shapes
and are significantly heterogeneous, resulting in high fractal dimensions
(D > 3.0).
Figure 7
Schematic diagrams of pore connectivity.
(A) Connectivity and pore
structure of combined pores (CP) and isolated grain pores (IGP) in
sample G2. (B) Clay-dominated pores within the intergranular space
of chlorite aggregations in sample G4. (C) Clay-dominated pores within
the intergranular space of kaolinite aggregations in sample G3.
Schematic diagrams of pore connectivity.
(A) Connectivity and pore
structure of combined pores (CP) and isolated grain pores (IGP) in
sample G2. (B) Clay-dominated pores within the intergranular space
of chlorite aggregations in sample G4. (C) Clay-dominated pores within
the intergranular space of kaolinite aggregations in sample G3.D2 of the samples ranges from
2.3897 to 2.8785
with an average of 2.7106. Fractal dimensions of between 2 and 3 represent
the dissolution pores due to their volume-filling shapes.[46] Diagenesis caused heavy deformation of the intergranular
pores of the Chang 7 tight sandstone (Figure A). These pores show heterogeneity and fractal
dimensions similar to those of dissolution pores.The intergranular
pores and the isolated dissolution pores have
a few connection paths, and these two pore types can be identified
as isolated grain pores as a result of their poor connectivity. Stage
B therefore corresponds to filling isolated grain pores, which have
medium heterogeneity and fractal dimensions, with mercury.D3 of the samples ranges from 1.5796 to 1.9302,
with an average of 1.7735. D3 values of between 1
and 2 indicate that mercury is invading the intergranular voids during
stage C.[46] The corresponding pressure of
stage C is greater than 11 MPa, whereas the size of corresponding
stage C is less than 0.06 nm, which is associated with clay-dominated
pores. 1 < D3 < 2 indicates limited compressibility
of the clay in the tight sandstone.[42] The
clay-dominated pores originate from the intergranular space of clay
aggregations with regular shapes (Figure B,C). The radii of the clay-dominated pores
are small, and fluid flows into the pores only under high pressure.
Stage C therefore corresponds to the mercury filling of clay-dominated
pores, which have simple intergranular fill shapes, poor heterogeneity,
and low fractal dimensions.The reservoir space of tight sandstone
is defined by combined pores,
isolated grain pores, and clay-dominated pores (Figure ). The fractal dimensions decrease from combined
pores to clay-dominated pores, indicates that the heterogeneity of
the pore space decreases from the microscale to the nanoscale.
Figure 8
Schematic diagram
of the pore types of the tight sandstone: (A)
combined pore, (B) isolated grain pore, and (C) clay-dominated pore.
Schematic diagram
of the pore types of the tight sandstone: (A)
combined pore, (B) isolated grain pore, and (C) clay-dominated pore.The fractal characteristics of HMIP results show
three distinct
fractal dimensions (D1, D2, and D3), mainly ranging from 1.8 to 6.5 and corresponding to
different pore types. These results are obviously different from the
fractal dimensions calculated with SANS/USANS and LPGA results (ranging
mostly between 2.6 and 2.8).[14,19,27] The differences in fractal dimensions from HMIP, LPGA, and SANS/USANS
techniques may be partially attributed to the following: (1) LPGA
and SANS/USANS obtain only a narrow range of pore structure, mostly
concerning nanoscale pores.[16] The small
range of pores shows only one fractal metric. (2) Mercury can enter
only the connected pores, and the accessibility at lower relative
pressures to the complex pore by probe molecules (N2 and
CO2) is limited.[47] (3) Different
pore geometry is assumed in the analysis data from different techniques.[16,48]
Effect of Pores on Physical Properties
Effect of Pores on Porosity
The
proportion of different pore types among the total reservoir spaces
can be used to calculate the mercury saturation in each type of pore
relative to the total mercury saturation (Table and Figure ). The proportions of combined pores, isolated grain
pores, and clay-dominated pores range from 18.23 to 43.83% (average
27.22%), 39.52 to 58.02% (average 46.28%), and 3.74 to 426.91% (average
15.24%), respectively, and proportions of three types of pores show
variability between samples. Combined pores and isolated grain pores
form the two main pore types in the sandstone samples of this study,
of which isolated grain pores are the majority.
Table 3
Petrophysical Properties Related to
Various Types of Pores in Eight Tight Sandstone Samples
proportion
of porosity (%)
contribution
to permeability (%)
porosity
permeability contribution ratio
samples
combined pores
isolated pores
clay-dominated pores
combined pores
isolated pores
clay-dominated pores
combined pores
isolated pores
clay-dominated pores
G1
43.83
39.64
3.74
92.85
7.14
0.01
2.118
0.180
0.003
G2
24.35
47.99
17.88
86.34
13.65
0.01
3.546
0.284
0.001
G3
32.66
40.89
17.21
85.27
14.72
0.01
2.611
0.360
0.001
G4
22.12
58.02
10.03
86.33
13.66
0.01
3.903
0.235
0.001
G5
26.81
46.75
16.99
84.73
15.26
0.01
3.160
0.326
0.001
G6
23.57
50.71
9.98
83.54
16.45
0.01
3.544
0.324
0.001
G7
26.19
46.72
19.17
83.43
16.56
0.01
3.186
0.354
0.001
G8
18.23
39.52
26.91
91.25
8.74
0.01
5.005
0.221
0.001
Figure 9
Tight sandstone sample
pore type histogram based on HMIP.
Tight sandstone sample
pore type histogram based on HMIP.
Effect of Pores on Permeability
The bundle
of tubes model can be used to calculate the contributions
of the different pore throats to the permeability (K)[100]where is the increment of the total mercury intrusion
corresponding to pore throats with a radius of r.On the basis of the distribution
ranges of three pore types, the contributions of the different pore
types to the permeability were calculated and are shown in Table . Combined pores contribute
83.43–92.85% (average 86.71%) to the permeability, indicating
that the main pore type contributing to permeability is combined pores.
The contribution of isolated grain pores to permeability ranges from
7.14 to 16.56% (average 13.27%), while the contribution of clay-dominated
pores is 0.11%, indicating that the contribution of isolated grain
pores and clay-dominated pores to the permeability is low.The
porosity permeability contribution ratio (PPCR) is the ratio
of the contribution of permeability to the proportion of the porosity
and can reflect the connectivity of pores. The PPCR values of the
combined pores, dissolution pores, and clay-dominated pores range
from 2.118 to 5.005 (average 3.384), 0.180 to 0.360 (average 0.286),
and 0.001 to 0.003 (average 0.001), respectively (Table ). The storage capacity and
connectivity decrease from combined pores to clay-dominated pores,
which is inconsistent with the heterogeneity of the pore space.
Effect of Diagenesis on the Pore Structure
and Connectivity Characteristics of the Pores
Diagenesis
has an important influence on the morphological structure and connectivity
of pores, which are in turn closely related to the fractal dimensions
and the connectivity of the tight sandstone.[49] Compaction reduces the intergranular space and causes the clastic
particles to be in close contact with each other. Intergranular pores,
therefore, develop in isolation and connect with other pores via a
narrow necking throat (Figure A).
Figure 10
Typical pores that occur in the tight sandstones samples.
(A) Intergranular
pores with closed connection paths in sample G6. (B) Dissolution pores
in the interior of clastic particles in sample G8. (C) Combined pores
in sample G2. (D) Clay-dominated pores of clay aggregates in sample
G3.
Typical pores that occur in the tight sandstones samples.
(A) Intergranular
pores with closed connection paths in sample G6. (B) Dissolution pores
in the interior of clastic particles in sample G8. (C) Combined pores
in sample G2. (D) Clay-dominated pores of clay aggregates in sample
G3.Dissolution is the main diagenesis
that increases the storage space
in tight sandstone. Dissolution mainly occurs in the interior of particles
to form dissolution pores (Figure B). The dissolution pores mainly connect with the dissolution
pore-shrinking throats, thus the connection paths of the intergranular
pores and dissolution pores are relatively isolated.With increased
dissolution, most of the particles dissolved and
the dissolution pores started to extend outward and connect with surrounding
pore spaces to form combined pores with large storage spaces. Multiple
and broad connection paths of combined pores occur in the samples
(Figure C).Aggregates of authigenic clay minerals fill the pores and segment
the primary intergranular pores into clay-dominated pores, which connect
with cluster throats (Figure D).In summary, combined pores formed via dissolution
pores connecting
with the surrounding pores. The pore spaces of the combined pores
is large and extremely irregular, and the connectivity of these pores
is good. Isolated grain pores include intergranular pores and dissolution
pores. Their pore spaces are slightly irregular and they have moderate
connectivity. Clay-dominated pores originated from the intergranular
space between clay aggregates. Their pore spaces are regular and homogeneous,
and their connectivity is poor. A clear correlation exists between
connectivity and pore type. The connected path reveals the mismatch
of heterogeneity of pore spaces and connectivity.
Pore Structures and Flow Characteristics of
Tight Sandstone
The storage capacity, connectivity, and heterogeneity
of the reservoir space have an important impact on the accumulation
and development of tight sandstone reservoirs.On the basis
of the proportions of the three pore types in the tight sandstone,
the tight sandstone can be genetically classified into a combined
pore type, an isolated grain pore type, and a clay-dominated pore
type. The pore structures and flow characteristics of the various
types of tight sandstone are distinct. These three genetic classifications
are discussed below.Combined pore type (samples G1). This
tight sandstone type was strongly affected by dissolution. The combined
pore content is high (more than 30%), while the isolated pore content
is relatively low, with the clay-dominated pore content being the
lowest (Figure A).
This tight sandstone has a large storage space (with a porosity higher
than 11%) and a strong connectivity (with a permeability larger than
0.25 × 10–3 μm2). The speed
of mercury intrusion into this sandstone type is fast, indicating
that the fluid can quickly enter the pore spaces of this tight sandstone
type (Figure B).
Figure 11
Classification and flow characteristics of the tight sandstone,
where G1, G4, and G8 represent the combined pore (CP) type, the isolated
grain pore (IGP) type, and the clay-dominated pore (CDP) type, respectively.
(1) Comparison of different pore contents. (2) Comparison of the mercury
intrusion saturation. (3) Schematic diagrams of flow characteristics
in the different tight sandstone types.
Classification and flow characteristics of the tight sandstone,
where G1, G4, and G8 represent the combined pore (CP) type, the isolated
grain pore (IGP) type, and the clay-dominated pore (CDP) type, respectively.
(1) Comparison of different pore contents. (2) Comparison of the mercury
intrusion saturation. (3) Schematic diagrams of flow characteristics
in the different tight sandstone types.Because of the multidirectional connected paths, the heterogeneity
of the seepage process is low (Figure C). The oil uniformly migrated through these
multiple paths and into the pore spaces and was well distributed within
the pore spaces of the tight sandstone, leading to large areas with
high oil saturation within the sand bodies.[50]Isolated pore type (samples G2–G7).
This tight sandstone was affected by compaction and cementation, which
led to a higher isolated pore content compared to the other pore types.
This tight sandstone has moderate storage space (with an average porosity
of 10.1%), and a moderate connectivity (with an average permeability
of 0.19 × 10–3 μm2). The initial
speed of mercury intrusion was slow but increased rapidly as the pressure
increased (Figure ). This means that fluid first migrated into a small number of combined
pores, after which it migrated into a large number of isolated grain
pores.The flow characteristics of these
tight sandstones are controlled
by the isolated grain pores, which have fewer connected paths (Figure ). In this tight
sandstone type, the oil migrated via a few obvious and dominant flow
paths, and the oil intrusion and saturation of the isolated pore type
of tight sandstone is moderate.Clay-dominated pore type (sample G8).
These tight sands are predominately affected by clay cementation and
have a high clay content (larger than 20%). The clay fills the pores
and lowers the availability of combined pores and isolated grain pores
(Tables and 3 and Figure A). The storage space of this tight sandstone type
is low (porosity 7.2%), and the connectivity is poor (permeability
0.12 × 10–3 μm[2]), indicating that clay minerals occupy the intergranular space and
separate the connected paths. The initial speed at which the fluid
entered this sandstone is slow, indicating that a large amount of
fluid filled the clay-dominated pores (Figure B).The clay-dominated
pores are mainly connected with combined pores
because of a lack of isolated grain pores and form a short-radial-flow
characteristic (Figure C). The movement of the oil front is not uniform, and the
oil and gas are mainly located in the clay-dominated pores, resulting
in a small area within the sand bodies that have a low saturation.Combined pores greatly improve the storage and connectivity of
the tight sandstones. The combined pores predominantly form by dissolution
via the acids from the hydrocarbon source rocks. The sand bodies that
are close to the hydrocarbon source rock are therefore favorable tight
sandstone reservoir areas. In areas located far from the hydrocarbon
source rock, the tight sandstone dominated by isolated grain pores
should be the favorable area for a tight reservoir. This research
is useful for the exploration and development of tight sandstone reservoirs.
Conclusions
In this article, thin sections,
SEM, HMIP, and fractal theory were
used to examine the pore structure, connectivity, and fractal characteristics
of eight tight sandstone samples of the Upper Triassic Yanchang Formation
from the Ordos Basin. The following conclusions are relevant:Diagenesis
causes the evolution of
reservoir space size from the microscale to the nanoscale. Accordingly,
a relevant pore type evolved from combined pores and isolated grain
pores to clay-dominated pores, with each corresponding to a distinct
pore structure. The changes in the type and size of reservoir spaces
not only cause the differences in storage capacity and connectivity
but also lead to the fractal features of pore spaces evolving from
high (D1 > 3) to low (1 < D3
< 3) values.From
the combined pore to the clay-dominated
pore, the storage capacity and connectivity decrease and the heterogeneity
of pore spaces is gradually weakened, whereas that of the flow process
is gradually enhanced. The connected paths reveal the mismatch of
the heterogeneity of the pore space and flow characteristics.The tight sandstone can
be classified
into three pore types: the combined pore type, the isolated grain
pore type, and the clay-dominated pore type, with each having distinct
pore structures and flow characteristics. All of these changes in
reservoir spaces influence the distribution of tight oil. The sandstone
dominated by the combined pore type has a uniform flow process and
large areas available for oil ingress, which results in high saturated
sand bodies. The sand bodies that are located close to the hydrocarbon
source rock are therefore favorable tight sandstone reservoirs. In
areas located far from the hydrocarbon source rock, the tight sandstone
dominated by isolated grain pores should be the favorable area for
the tight reservoir.