The fracture of composite coal-rock under load is the process of energy conversion. As the dissipative energy composition, there is a correlation between the infrared radiation energy and the coal-rock states. Based on theories of theoretical mechanics, modern quantum mechanics, thermodynamics, and other disciplines, first, this paper explained the causes of infrared radiation energy in the process of coal-rock fracture by using the microanalysis method. After that, the mathematical model of dissipation energy-infrared radiation energy coupling was deduced and established, and the experimental analysis was carried out under different loading conditions. The analysis shows that the conversion of mechanical energy and internal energy in the process of loading caused constant collisions between molecules in coal-rock, which led to a temperature rise. After entering the excited state, molecules have to transition to a lower energy level, which generates infrared radiation. The experimental results show that there was a strong correlation between energy characteristic parameters, which is consistent with the established relationship. In addition, the energy conversion and dissipated energy changes in the loading process had stages. Before the elastic-plastic stage, the dissipated energy obtained by coal-rock energy conversion was less, but it increased rapidly in the later stage, which eventually led to the fracture of coal-rock. In the early elastic-plastic period, infrared radiation energy was the main component of the dissipated energy and its variation trend was consistent with the dissipated energy. After that, the infrared radiation energy remained stable, but the dissipation energy still increased. At this time, infrared radiant energy was no longer the main component of dissipated energy. And the infrared radiation energy dropped rapidly before coal-rock fracture, which had certain precursory characteristics. The coupling mechanism of dissipated energy-infrared radiation energy can be used to explain the failure reason of composite coal-rock under different loading conditions from the perspective of energy, which will provide a new idea for assisting the prediction of coal-rock dynamic disasters.
The fracture of composite coal-rock under load is the process of energy conversion. As the dissipative energy composition, there is a correlation between the infrared radiation energy and the coal-rock states. Based on theories of theoretical mechanics, modern quantum mechanics, thermodynamics, and other disciplines, first, this paper explained the causes of infrared radiation energy in the process of coal-rock fracture by using the microanalysis method. After that, the mathematical model of dissipation energy-infrared radiation energy coupling was deduced and established, and the experimental analysis was carried out under different loading conditions. The analysis shows that the conversion of mechanical energy and internal energy in the process of loading caused constant collisions between molecules in coal-rock, which led to a temperature rise. After entering the excited state, molecules have to transition to a lower energy level, which generates infrared radiation. The experimental results show that there was a strong correlation between energy characteristic parameters, which is consistent with the established relationship. In addition, the energy conversion and dissipated energy changes in the loading process had stages. Before the elastic-plastic stage, the dissipated energy obtained by coal-rock energy conversion was less, but it increased rapidly in the later stage, which eventually led to the fracture of coal-rock. In the early elastic-plastic period, infrared radiation energy was the main component of the dissipated energy and its variation trend was consistent with the dissipated energy. After that, the infrared radiation energy remained stable, but the dissipation energy still increased. At this time, infrared radiant energy was no longer the main component of dissipated energy. And the infrared radiation energy dropped rapidly before coal-rock fracture, which had certain precursory characteristics. The coupling mechanism of dissipated energy-infrared radiation energy can be used to explain the failure reason of composite coal-rock under different loading conditions from the perspective of energy, which will provide a new idea for assisting the prediction of coal-rock dynamic disasters.
With the deep mining of coal seam, the problems of coal-rock dynamic
disaster prevention and control such as rockburst have been paid more
attention.[1−5] In this context, researchers have studied various problems arising
in the process of rockburst, for example, the internal or external
causes of rockburst,[6,7] the risk assessment of rockburst
accident,[8−10] the law of coal-rock cracking,[11] the law of impact signal transmission,[12] etc. In these research fields, coal-rock dynamic disaster
prediction plays an important role, which is directly related to the
safety of life and property. As a result, many researchers hope to
find a method of disaster prediction by studying the characteristics
of coal-rock in the process of fracture.At present, most of
the existing research results in this field
are merely on the variation law or coupling relationship of observable
physical parameters: Li X. et al.[13−15] used numerical
simulation to study the coupling mechanism of the temperature, stress,
and electromagnetic field of composite coal-rock in the process of
loading; verified the simulation conclusion based on experiments;
and established the multi-physical field coupling model of composite
coal and rock and the triaxial failure criterion under different unloading
conditions. Liu X. et al.[16] studied the variation law of electromagnetic radiation in the process
of uniaxial compression of coal-rock and established the relationship
between the Hurst index and deformation, and the research results
have a positive significance for rockburst prediction. Zheng K.H. et al.[17] modeled the failure
process of coal-rock under a dynamic impact load based on the finite
element and discrete element models of images. They considered that
the spatial distribution and loading direction of samples had an impact
on material strength and failure mode, and verified that XCT image
modeling was an effective analysis method. Guo J.Y. et al.[18] studied the difference between acoustic
emission and failure of coal-rock based on a uniaxial compression
experiment, believed that acoustic emission characteristics could
better describe the failure characteristics of coal-rock, and proposed
a failure warning value of 100–150. Li L. et al.[19] studied the fracture evolution law
of single fracture prefabricated fractures in Longmaxi shale using
a CCD camera and acoustic emission monitoring equipment. The study
showed that there was a strong correlation between the acoustic emission
and rock fracture state, so this law could be used to judge the rock
state. Although existing researches can reveal the failure law of
coal-rock to a certain extent, there are still some limitations in
the nature of coal-rock fracture and prediction of its fracture.The fracture of coal-rock under load is a thermodynamic process,
and its deformation state is related to internal and external energy
transformation.[20−23] To master the relationship between the failure law of composite
coal-energy transformation, researchers from various countries have
made some achievements in recent years: Duan M.K. et al.[24] conducted an experimental analysis
on the permeability characteristics, acoustic emission characteristics,
and energy dissipation of coal-rock during cyclic loading, and the
results showed that the dissipated energy increases with the loading
process in a quadratic function relationship and is positively correlated
with the deformation trend. Li X.L. et al.[25] established the elastic–plastic brittle
rockburst model of coal-rock and introduced the concept of volume
energy potential function to effectively analyze the characteristics
of microseismic and electromagnetic radiation. Xue Y. et al.[26] carried out theoretical analysis and
FLAC simulation on the mechanism of coal pillar rockburst and classified
the rockburst risk by using energy density characteristics. The study
found that elastic strain energy would release suddenly when rockburst
disaster occurred. Mohammadali S. et al.[27] studied the elastic strain energy of rock, combined
the energy and accumulation degree, and analyzed the two methods by
numerical simulation, which can effectively predict the rockburst
trend. Yang L. et al.[28] conducted uniaxial compression and cyclic loading and unloading
tests on two-layer coal-rock mass, studied the evolution law of each
energy in the process of loading, and preliminarily discussed the
energy driving mechanism of failure of coal-rock mass. Li B.B. et al.[29] studied the damage of
coal-rock under mechanical–thermal coupling based on triaxial
compression experiments at different temperatures and found that energy
evolution had stage characteristics and that dissipated energy was
the main cause of damage. Through experiments or theoretical analysis
by some researchers, it can be known that the dissipated energy is
closely related to the fracture state of coal-rock, and it is feasible
to predict coal-rock’s deformation trend from the perspective
of energy. As a general term for many energies, dissipative energy
is very difficult to obtain directly. To solve this problem, most
researchers calculate the elastic strain energy and total energy to
indirectly obtain the dissipated energy and the energy state of coal-rock.
This method has certain theoretical significance, but it is difficult
in engineering applications. The reason is that the calculation of
elastic strain energy must rely on the mechanical parameters, so it
is inevitable to use a large number of contact sensors, which does
not meet the application requirements of the engineering field. To
sum up, it is of great significance to find a method of obtaining
the dissipative energy state without contact, which will help to further
establish the relationship between energy and coal-rock’s state
and finally realize the application of the energy theory in reality.Infrared radiation energy is a kind of energy that can be obtained
by a noncontact method, and it is closely related to the internal
state of the measured object. As a result, infrared radiation analysis
technology has been widely used in various fields requiring noncontact
measurement, for example, vital signs monitoring,[30,31] power equipment damage monitoring,[32,33] celestial
movement,[34] medical diagnosis assistance,[35] geological survey,[36] etc. In the loading process of coal-rock, infrared radiation energy
is a part of dissipated energy, and there is a certain coupling between
them. In view of this feature, some scholars have studied the variation
of infrared radiation energy and its characteristic parameters in
the process of coal-rock’s fracture in recent years, and some
achievements have been made: Xu L. et al.[37] experimentally studied the relationship between
temperature and rock energy and also discussed the relationship between
temperature and granite energy storage capacity (ESC), suggesting
that the increase of temperature reduced the energy storage capacity
of rock, thus promoting the occurrence of rockburst. Li Z.H. et al.[38] analyzed the variation
trend of thermal infrared radiation temperature in the process of
fracture and also defined the concepts of damage precursor point and
critical precursor point. Liu X.X. et al.[39] studied the influence of humidity and water
content in a humid environment on the average temperature of rock
failure, believing that the more water content there is, the faster
is the rock destroyed and the more likely it is to produce an acoustic
emission phenomenon, and temperature can be used as a precursor judgment
indicator. Chen G.Q. et al.[40] studied the thermal precursor information of true triaxial loading
failure of rock and believed that the thermal infrared index should
be introduced in the prediction of rock loading to enhance the accuracy
of judgment. Liu C.Y. et al.[41] divided rockburst into four stages according to carrying capacity
and analyzed the relationship between energy variation trend including
thermal radiation temperature and sample failure. Huang F.R. et al.[42] explained the variation
law of rock and IR under uniaxial compression and believed that there
was a strong linear relationship between temperature and stress. Wang
B.X. et al.[43] conducted
experiments on samples under low-temperature conditions to study the
influence of temperature on mechanical parameters and construct relevant
numerical relationships. It is considered that the dissipated energy
of rock increases linearly with loading and the temperature is related
to the amount of energy accumulation. Although there were some researches
on infrared radiation or temperature associated with infrared radiation
energy, most of them were the fitting and analysis of a single physical
quantity. However, there are few researches on infrared radiation
energy as a form of dissipative energy, let alone the relationship
between them. Therefore, the research in this field is still in its
infancy.As an important internal cause of coal-rock fracture,
the change
of dissipated energy is difficult to measure without contact in the
existing results. In addition, the existing prediction methods based
on energy theory are difficult to apply in practice. However, as one
of the components of dissipative energy, infrared radiation energy
can be measured by a noncontact method, which provides a way to solve
this problem. Based on these, in this paper, the coupling model of
dissipated energy and infrared radiation energy of coal-rock under
a loading condition was established by using thermodynamics, theoretical
mechanics, and statistical theory. Meanwhile, the relationship between
these energies was further verified and analyzed through experiments.
On this basis, the relationship between energy change and the mechanical
state of composite coal-rock during the loading process was established,
and the law of energy transformation in coal-rock was deeply analyzed.
This makes it possible to judge the stress state of coal-rock without
contact and provides a new idea for preventing coal-rock dynamic disaster.
Theory and Method
Microphysical Mechanism
Analysis of Coal-Rock
under Loading
According to a large number of previous experiments
and results, the external force continued to act on the coal-rock
during the loading process, and the measured surface temperature and
external infrared radiation intensity of samples would increase in
this process. According to the first law of thermodynamics, under
ideal adiabatic conditions, all mechanical energy generated by work
done by force is converted into internal energy, which will cause
the internal energy of the object to increase. On this basis and in
refs (44) and (45), it can be seen that in
the loading process of composite coal-rock, the increment of internal
energy will eventually be expressed in the form of elastic strain
energy and dissipated energy. The elastic strain energy is reflected
by the elastic deformation of the object, and other energies that
are not reflected by elastic deformation can be regarded as one of
the components of the dissipated energy.[44,45] Although infrared radiation energy is related to the temperature
of the object, it is essentially a kind of electromagnetic radiation
energy. Therefore, infrared radiation and temperature are two completely
different physical quantities. At the same time, infrared radiant
energy can also be regarded as one of the components of dissipative
energy. To sum up, the balance between mechanical energy generated
by the work done by external forces and various energies is shown
in eq .where Wm is mechanical energy of work done by an external force
(J), Wi is the increased internal energy
(J), We is the elastic strain energy transformed
from
mechanical energy (J), Wd is the dissipated
energy converted from mechanical energy (J), Eh is the infrared radiation energy converted in the process
(J), and WΔ is the energy form of
dissipated energy except infrared radiation energy (J).Composite
coal-rock is a kind of rock and soil material whose internal structure
arrangement is loose, and there are some tiny cracks in the original
state. These provide the physical basis for the energy transformation
of coal-rock under load. From the microscopic point of view, the temperature
rise of coal-rock is related to the molecular thermal movement. During
loading, dislocation movement is easy to occur between the two contact
surfaces of the original tiny crack inside so that the friction does
work, which leads to local heating inside the sample and the overall
internal energy enhancement. With the advance of coal-rock loading,
the high-speed molecules moving disorderedly on the surface of the
microcrack constantly collide with the low-speed molecules located
deep in the interior, which allow low-speed molecules to get some
or all of their kinetic energy from the high-speed ones. This can
be regarded as the process in which the energy generated by the external
work flows into the samples. The longer the loading time is, the more
intense is the process, resulting in more frequent and disorderly
molecular movements in coal-rock. In this process, the average kinetic
energy of the internal whole increases, while the disorder and intensity
of molecular motion are significantly enhanced. According to thermodynamic
laws and experiments in ref (46), the average surface temperature of composite coal-rock
continues to rise in this process.Figure shows the
variation trend of molecular motion in coal-rock during loading, where
the shade of color indicates the temperature and the length of the
arrow indicates how fast the molecules are moving. As can be seen
from Figure , at the
initial stage, most of the molecules in the composite coal-rock move
at a low speed. At this time, coal-rock is in a steady state of energy
balance. When an external force is applied to the coal-rock, the external
force makes the original microcracks in coal-rock closely contact
and increases the possibility of sliding friction movement between
crack contact surfaces. This makes most of the external mechanical
energy Wm convert into the kinetic energy
of the molecules located on the surface of the fracture and further
intensifies the molecular movement at the fracture. This process promotes
the continuous transformation of external mechanical energy into internal
energy of coal-rock and also causes the formation of multiple micro
heat sources in the cracks of composite coal-rock. These heat sources
increase the temperature in the cracks inside coal-rock and continuously
release heat outward, finally increasing the temperature of the whole.
Combined with the above analysis, under ideal adiabatic conditions,
the coal-rock’s increment of internal energy Wi is equal to external mechanical energy Wm. As can be seen in Figure , at the beginning, the color of cracks is
orange and the color outside is blue, and then the orange part gradually
spreads out, indicating heat transfer during loading. At this time,
the surface temperature of coal-rock Tout is obviously lower than the internal temperature Tin. With loading advancing, the probability of high-speed
molecules hitting low-speed molecules increases, which gradually increases
the kinetic energy of the external molecules and intensifies the overall
molecular thermal motion inside the coal-rock. Therefore, this also
leads to an increase in the external surface temperature Tout. As can be also seen from Figure , because of constant heat transfer from
the inside out, the surface temperature Tout gradually increases and the temperature of the sample gradually
changes from low temperature blue to high temperature orange. This
process completes the transformation of external mechanical energy
into internal energy of coal-rock.
Figure 1
Changes of molecular motion in composite
coal-rock during loading.
Changes of molecular motion in composite
coal-rock during loading.In the above content, the mechanism of temperature rise and the
energy conversion process of coal-rock during loading were mainly
discussed, but the reason for the infrared radiation change caused
by loading was not explained. What follows is an analysis of why this
happens based on quantum theory.In the above process, the thermal
motion of coal-rock internal
microscopic particles is enhanced by energy conversion, thus forming
some internal heat sources and releasing heat continuously. The temperature
increase also causes the particles to be excited from the ground state
to the excited state. To return to stability, particles must transition
from high energy to low. According to Bohr’s theory, internal
particles emit a large number of photons as they transition, which
is called electromagnetic radiation. And because these radiations
are temperature-related, they are also called infrared radiation.
This process is shown in Figure . In this process, part of the internal energy of the
composite coal-rock Wi is transformed
into infrared radiation energy Eh, which
conforms to the description of eq .
Figure 2
Microscopic mechanism of infrared radiation generation.
Microscopic mechanism of infrared radiation generation.
The Theoretical Analysis
of Coupling Relationship
between Dissipated Energy and Infrared Radiation Energy
The Analysis of Stress–Temperature
Coupling Relationship
To reveal the coupling relationship
between various energies in the loading process of composite coal-rock,
it is very important to analyze and characterize the parameters of
energies. The rise of temperature is related to the change of internal
energy. According to the first law of thermodynamics, when work transformation
is not considered, the increment of internal energy only comes from
the absorption of energy, which is in the form of heat transfer. Therefore,
it can be considered that when no work is done, the essence of rising
temperature of objects is the transfer of heat between different objects.[47] Combined with previous analysis, infrared radiation
is generated by the excitation of temperature. As a result, the change
of infrared radiant energy is closely related to temperature; thus,
temperature can be regarded as a characteristic parameter representing
infrared radiant energy. It can be known from the literature that
the dissipated energy is calculated according to the stress–strain
curve, so stress can be considered as the characteristic parameter
of it. To sum up, before studying the coupled relationship between
dissipated energy and infrared radiant energy, the stress–temperature
relationship of coal-rock should be clarified.To facilitate
the analysis of the relationship between stress and temperature, the
composite coal-rock is divided into n unit volume
microelements, and then the No.i element is selected
for analysis, as shown in Figure .
Figure 3
Composite coal-rock unit volume diagram.
Composite coal-rock unit volume diagram.According to ref (48) and the previous analysis, the temperature rise of each
coal-rock’s
micro-unit is related to the change of internal energy, and the reasons
for the change are as follows: (1) heat conduction of other elements
and (2) the work of friction being converted to internal energy. Both
processes increase the internal energy of each unit and thus increase
the temperature. These physical processes both make the thermal motion
of internal molecules more intense, which causes the internal energy
of the No.i block of coal-rock per unit volume Q to increase over time. The process can be
expressed aswhere Qf is the increase in internal
energy by converting work done
by the external force (J) and Qa is the
increase in internal energy by heat conduction (J).According
to the heat conduction theory and relevant literature,[49,50] heat conduction leads to an increase in internal energy, which in
turn leads to an increase in temperature. Combined with refs (51−53), when No.i per unit coal-rock’s
temperature rises ΔT in unit time
dt, the net internal energy obtained by heat conduction
dQa iswhere λ is the thermal
conductivity coefficient of coal-rock. At any time t, No.i coal-rock per unit volume dV obtains the net internal energy through heat conduction Qa iswhere ∇2 is the Laplacian operator, which is (∂2/∂x2 + ∂2/∂y2 + ∂2/∂z2).Although there is adhesion between
mineral particles in composite
coal-rock, there are some original cracks, which can be regarded as
the bud of cracks.[40] When the component
of external resultant force in the direction of fracture development
is greater than its maximum static friction force Ffm during loading, sliding friction will occur on both
sides of the original fracture inside the composite coal-rock. Then
the energy conversion from mechanical energy to internal energy is
realized by the action of friction Ffm, and it is accompanied by the generation of heat,
which makes the composite coal-rock local temperature rise. In addition,
because of the different directions of the original cracks in coal-rock,
these cracks’ effective action time of sliding friction τ
is not the same, but τ can be regarded as a constant only related
to the sample structure. Under different loading conditions, the samples
are subjected to different external forces: Under uniaxial loading,
the combined stress σall at the original crack is
the axial principal stress σ1. The resultant stress
σall under triaxial loading is deviator stress, and
its value is the difference between axial stress and lateral stress
(σ1 – σ3). Sliding friction
occurs only when the combined force component is greater than the
maximum static friction force Ffm. According
to the thermodynamic theorem and the calculation of equivalent velocity,
at any time t, No.i per unit volume’s
internal energy Qf of coal-rock increased
by energy conversion though friction can be written aswhere σall is the combined stress
in the original fracture space of the No.i coal-rock
unit (Pa), dS is unit area
of friction surface (m2), θ is angle between the
resultant force and the direction of the original crack (°),
τi is effective time of sliding friction action of
internal cracks (s), and dm is the unit mass, whose
value is 1 kg.Assuming that the temperature of the No.i coal-rock
unit rises ΔT per unit time dt, its heat source intensity qi iswhere
ρ is the density
of coal-rock (kg/m3), c is the specific
heat capacity of coal-rock [J/(kg·K)], and dxdydz = dV is the
unit volume (m3).Then, the internal energy increased
by the unit volume of the No.i coal-rock Q at any time t isSo the temperature of No.i coal-rock unit T at any time t iswhere T0 is the initial temperature of coal-rock (K).By
combining eqs , 4, and 5, it can be
deduced that No.i coal-rock unit temperature T at any time t isEquation is a partial
differential equation. (ΔTi·t) can be solved by writing boundary value conditions for
coal-rock units, and the unitary function model of temperature Ti combined stress σall can
be obtained. The model has some theoretical significance for analyzing
the development of fracture from the microscopic point of view. According
to eq , the average
temperature Tave of macroscopic composite
coal-rock isThe first
two terms of eq refer
to the temperature rise caused by heat resulting from
the conversion of external mechanical energy into internal energy,
and the last term refers to the temperature rise caused by heat conduction.
Under ideal conditions, there is no external heat exchange in the
loading process of coal-rock, so the value of the last term of eq is 0. It can be seen
that the temperature rise of coal-rock is only caused by energy conversion.
Then, Tave can be obtained as follows:where m is
the overall mass of composite coal-rock (kg); a is
the average action constant of the crack angle and τ is the
effective time of sliding friction (s), both of which are related
to material properties; and k and b are thermal constants of composite coal-rock loading, and their
values are only related to material property parameters.Equation is the
temperature–stress coupling model of composite coal-rock, from
which it can be seen that the composite stress σall has a linear relationship with the average body temperature Tave under loading. In eq , there are no external parameters representing
loading rate, initial confining pressure, and so on for k and b, so it can be seen that the change of external
parameters will not affect the stress–temperature linear relationship.
Analysis of Dissipative Energy–Infrared
Radiation Energy Relationship
As mentioned above, all objects
higher than absolute zero will emit infrared radiation, whose radiation
intensity is closely related to material properties and temperature
state. During the loading process, the composite coal-rock is heated
up due to the work of the external force, some atoms or molecules
inside are into excited states by heating, and externally detectable
infrared radiation intensity changes. Based on this, the temperature
state of coal-rock can be obtained by noncontact measurement of infrared
radiation intensity, then the dissipated energy of infrared radiation
can be calculated, and finally the state of coal-rock also can be
obtained.The composite coal-rock can be regarded as a kind
of gray body material.[54] According to thermodynamics,
modern quantum mechanics, and the above analysis, it can be known
that the radiation capacity of the composite coal-rock follows the
Stefan–Boltzmann law. According to refs (55) and (56), the source of infrared
radiant energy is emitted photon energy, and the relation between
its radiation capacity Eh and average
temperature Tave iswhere C is
the radiation coefficient of gray body (W/(m2·K4)); ε is the blackness of composite coal-rock, which
is only related to the property of the material itself, ε = Eh/Eb ≈ 0.96; Eb is the radiation capacity of the black body
at the same temperature (W/m2); and C0 is the black body radiation coefficient, C0 = 5.67 W/(m2·K4).By
combining eq with eq , coal-rock’s
numerical relationship between stress and infrared radiation energy
can be obtained, as follows:According to eq , the relation between infrared radiation energy and
resultant stress
σall is a unary quartic function. For triaxial loading,
the resultant stress σall is deviatoric (σ1 – σ3).If the composite coal-rock
is in an ideal heat insulation environment
(there is no external energy exchange), it can be seen from eq that the external mechanical
energy Wm will all transform into the
internal energy Wi and then finally transform
into elastic strain energy Wd or dissipated
energy Wd. According to ref (57), the strain energy density U of the coal-rock is calculated by eq , as follows:where σ (i = 1, 2, 3) is the triaxial principal
stress (Pa); ε (i = 1, 2, 3) is the triaxial strain; Ud is the unit dissipated energy, which consists of heat energy, kinetic
energy, infrared radiation energy, electromagnetic radiation energy,
etc. (J/m3); and Ue is unit
elastic strain energy (J/m3).When the composite
coal-rock is under triaxial loading, the principal
stress in x and y directions is
equal (σ2 = σ3). Combined with refs (57−59), the unit elastic strain energy Ue can be calculated as follows:where E is
the elastic modulus of loading at the elastic stage and υ is
Poisson’s ratio. Therefore, the calculation formula of unit
dissipation energy Ud under triaxial loading
is as follows:By combining eq and eq , the numerical
relationship between infrared radiant energy and dissipation energy
can be obtained as follows:It can be seen from eq that there is a numerical relationship between the infrared
radiant energy Eh and the dissipated energy Ud in the loading process, but it cannot be expressed
by a simple linear function, which is different from the relationship
between the physical quantity in eq . After substituting equations ①, ③,
and ④ in eq into ②, there is no parameter of time t or
rate v. Therefore, when the initial confining pressure
σ3 is constant, there is a one-to-one correspondence
between the dissipated energy Ud and the
infrared radiant energy Eh. So, the confining
pressure should be kept constant during the loading test.
Sample Preparation and Experimental Methods
To analyze the coupling law between dissipated energy and infrared
radiation energy in the loading process of composite coal-rock mentioned
above and to explore the law between energy and fracture, uniaxial
and triaxial loading experiments were used to study self-made composite
coal-rock. The experimental sample making method and experimental
plan are described below.
Sample Making Method
and Industrial Analysis
of Coal
According to previous research and experience, the
samples selected in the experiment should be a ″rock-coal-rock″
three-layer combination structure. According to the requirements of
the International Society of Rock Mechanics for the experiment, the
overall sample is processed into a standard cylinder specimen with
a diameter of 50 mm and a combined ratio of 100 mm to 1:1:1. The sample
structure is shown in Figure .
Figure 4
Test sample and size.
Test sample and size.As can be seen from Figure , the experimental
samples are composed of roof rock, coal,
and floor rock. The roof rock and floor rock of the test sample are
sandstone, and coal seam is taken from a deep coal seam in a mine
in Nei Mongol. The source address of experimental coal samples is
shown in Figure .
Figure 5
Source
address of experimental coal samples.
Source
address of experimental coal samples.The 5E-MACIII infrared fast coal quality analyzer was used to measure
the industrial analysis indexes of three coal seam samples that were
identical with the experimental samples. The determination results
are shown in Table , and M, A, V,
and FC in it, respectively, represent moisture, ash, volatile matter,
and fixed carbon.
Table 1
Industrial Analysis of Coal Seams
no.
M (%)
A (%)
V (%)
FC (%)
1
5.25
12.74
15.67
66.34
2
5.67
12.58
16.23
65.52
3
5.88
11.96
16.08
66.08
average
5.60
12.43
15.99
65.98
Experimental Conditions
and Methods
The uniaxial and triaxial experimental sites
are shown in Figure , and the structures
of the two experimental systems are shown in Figure . It can be seen from Figures and 7 that there
is little difference between the two experimental scenes. The TAW-2000
triaxial test system was adopted in both of them, which was mainly
composed of a computer, power cabinet, rock loading system, and strain
sensor. All data during the experiment were timely sent to the computer
for storage, which is convenient for subsequent analysis.
The experiment
site. (a) Uniaxial loading scenario. (b) Triaxial
loading scenario.Laboratory equipment.The ThermoView TM Pi20 infrared thermal imager
was selected for
the uniaxial experiment to detect infrared thermal imaging on the
surface of the sample during loading, with a sensitivity of 0.03 °C.
During the triaxial experiment, the infrared thermal imager cannot
detect infrared thermal imaging on the sample surface because of the
enclosed pressure cylinder. Infrared radiation is a kind of electromagnetic
signal in nature, which also follows the law of electromagnetic propagation.
According to the electromagnetic theory and previous studies,[60,61] the electrical conductivity of pressurized oil is extremely low,
so it can be known that the infrared radiation propagates in silicone
oil with a small energy loss. Therefore, an oil-resistant high-precision
infrared probe can be installed in the cylinder to collect the changes
of infrared radiation on the sample surface during loading, and its
sensitivity is 0.02 °C. Because the temperature changes weakly
during loading, the liquid flow in the constant pressure cylinder
may cause temperature loss, thus interfering with the data results.
To solve this problem, the following two solutions can be adopted:
on the one hand, the infrared probe should be installed as close to
the sample as possible; on the other hand, after the confining pressure
loading is completed, it should be static for a period of time to
make the system relatively stable before the test. In the process
of data acquisition, the original data signal must be preprocessed
and digital–analog converted by the signal acquisition system
so as to facilitate further data analysis and calculation of the computer.To ensure the universality of experimental results, multiple control
groups were set up in each experiment. In the uniaxial loading experiment,
nine identical composite coal-rock samples were set up, labeled as
D1–D9, and then divided into three groups
on average. The uniaxial test was carried out according to normal
speed, high speed, and fast speed in each group. The uniaxial loading
rates of D1–D3 were 0.1 mm/min, those
of D4–D6 were 0.3 mm/min, and those of
D7–D9 were 1 mm/min. In the triaxial
loading experiment, nine identical samples were set up, labeled as
S1–S9, and divided into three groups.
The three groups were subjected to constant triaxial loading according
to the three confining pressures of low pressure, medium pressure,
and high pressure. The confining pressures of S1–S3 were 10 MPa, those of S4–6 were
15 MPa, and those of S7–S9 were 20 MPa.To determine the coupling relationship between various energies
of composite coal-rock under different loading conditions, the study
designed two groups of experiments under triaxial and uniaxial loading.
In the uniaxial loading experiments, three loading speeds of 0.1,
0.3, and 1 mm/min were set. The same confining pressure was atmospheric
pressure in each uniaxial experiment, ensuring a single variable.
Under the triaxial loading experiment, three initial confining pressures
of 10, 15, and 20 MPa were set. The loading rate of each experiment
was 0.1 mm/min, which ensured the single variable of the experiment.The experimental steps of uniaxial loading are as follows:(1) The composite coal-rock samples were glued between layers with
adhesive tape, and the strain sensor was installed and then fixed
on the test machine. The infrared thermal imager was aimed at the
center of samples to measure the trend of average surface temperature
during loading.(2) Before starting the experiment, close the
equipment unrelated
to the experiment, close the laboratory doors, and windows, and stop
unnecessary walking.(3) Power on the experiment and set the
loading rate of each group
to 0.1, 0.3, and 1 mm/min, respectively. Start the infrared thermal
imager first, and then start the press after the indicator becomes
stable. Meanwhile, record the surface temperature, stress, and strain
in the loading process.(4) Observe the experimental data until
the axial stress exceeds
the stress peak and the sample is destroyed. The experiment ends and
the data are saved for subsequent processing.Triaxial loading
experiment steps are as follows:(1) The composite coal-rock
samples are glued to each layer with
adhesive tape, and strain sensors are installed. Put it into the pressure
cylinder, push the pressure cylinder into the tester, and open the
oil valve.(2) Switch on the power supply. First turn on the
infrared probe
to record the temperature, and then turn on the press after it is
stabilized. The triaxial stress σ1–σ3 is applied to the predetermined confining pressure value
(10, 15, and 20 MPa).(3) The confining pressure σ3 is kept constant,
and the loading rate is 0.1 mm/min by the displacement control method.
Meanwhile, the surface temperature, stress, and strain during the
loading process are recorded.(4) Observe the axial stress in
real time. When the axial stress
exceeds the stress peak, stop the experiment and save the data for
subsequent processing.After the completion of the above six
groups of experiments, physical
parameters such as stress, strain, and temperature were converted
into total energy, dissipated energy, elastic strain energy, and infrared
radiation energy according to eqs –16, and then further
analysis was conducted. Because the sample components are basically
the same and the experimental conditions are the same, the sample
data with the most obvious characteristics are selected from the three
samples’ data in each group for analysis. If the three samples’
data in a certain group have high dispersion, it must be supplemented
to carry out the experiment under the same loading conditions.
Results and Discussion
Experimental
Results and Fracture State of
Samples
Through the uniaxial and triaxial compression experiments
mentioned above, energy characteristic parameters of composite coal-rock
samples under different loading conditions were obtained, such as
stress, strain, sample surface temperature, and so on. Table shows the sizes and experimental
results of D1–D9, and Table shows S1–S9.
Table 2
Uniaxial Specimen Size and Experimental
Results
no.
high (mm)
diameter
(mm)
loading rate
(mm·min–1)
compressive
strength (MPa)
D1
101.32
49.64
0.10
29.61
D2
98.68
49.78
0.10
28.35
D3
100.24
49.12
0.10
30.47
D4
101.58
49.84
0.30
23.12
D5
101.10
50.12
0.30
25.63
D6
100.74
50.04
0.30
28.47
D7
98.24
49.78
1.00
31.04
D8
97.78
49.94
1.00
32.72
D9
99.64
50.24
1.00
29.33
Table 3
Triaxial Specimen Size and Experimental
Results
no.
high (mm)
diameter
(mm)
confining
pressure (MPa)
compressive
strength (MPa)
deviatoric
stress peak (MPa)
S1
101.64
49.54
10
46.07
36.07
S2
101.24
49.54
10
45.50
35.50
S3
101.10
50.12
10
47.57
37.57
S4
101.32
49.60
15
68.26
53.26
S5
100.98
49.58
15
63.12
48.12
S6
100.74
50.04
15
65.56
50.56
S7
101.52
49.64
20
76.54
56.54
S8
101.84
49.82
20
79.37
59.37
S9
101.62
50.12
20
80.12
60.12
The results show that the failure
trend of nine uniaxial and nine
triaxial samples was similar. Therefore, this paper presents only
one failure diagram of uniaxial sample and one failure diagram of
triaxial sample. The results are shown in Figure . As can be seen from Figure , in both uniaxial or triaxial tests, only
the coal layer had a penetrating fracture, and the rock was slightly
fractured but no obvious fracture was observed. It can be seen that
the coal layer of composite coal-rock is more fragile. In addition,
the preliminary research results also show that the temperature change
of coal is more significant than that of rock during the loading process.
To specifically analyze the reasons for the fracture of coal-rock
and study the coupling relationship between dissipated energy and
infrared radiation energy in the loading process, this paper only
measured the average temperature of the coal surface but did not measure
the temperature of rock.
Figure 8
Experimental sample. (a) Result of uniaxial
experiment. (b) Result
of triaxial experiment.
Experimental sample. (a) Result of uniaxial
experiment. (b) Result
of triaxial experiment.
External
Factors’ Influence on the
Relationship between Characteristic Parameters of Energies
Analysis of the Influence of Loading Rate
on the Correlation of Each Energy Characteristic Parameter
As the experimental results of nine samples in three groups showed
the same trend in the uniaxial experiment, only the stress–strain
curves and temperature change curves of D1, D4, and D8 are shown in Figure . According to previous research results[35] and uniaxial experimental results, all results have the same trend
under different loading rates. There are four obvious stages of compaction,
elasticity, elastic–plastic stage, and fracture on stress–strain
curves of each group under uniaxial loading, and the variation trend
of temperature under different loading rates is basically the same.
Figure 9
Uniaxial
loading experimental result curve. (a) The experimental
result of D1 uniaxial loading at 0.1 mm/min. (b) The experimental
result of D4 uniaxial loading at 0.3 mm/min. (c) The experimental
result of D8 uniaxial loading at 0.3 mm/min.
Uniaxial
loading experimental result curve. (a) The experimental
result of D1 uniaxial loading at 0.1 mm/min. (b) The experimental
result of D4 uniaxial loading at 0.3 mm/min. (c) The experimental
result of D8 uniaxial loading at 0.3 mm/min.The loading experiment result curve of conventional speed
loading
D1 was taken as an example (Figure a) for analysis: In the compaction stage,
the temperature of the internal crack closure fluctuated slightly,
ranging from 0.01 to 0.03 °C, which was still stable, and infrared
radiation energy did not change much. After entering the elastic stage,
the temperature began to fluctuate and rise until it entered the elastic–plastic
stage. In this process, the temperature rise range was between 0.08
and 0.12 °C, which was significantly larger than that of the
previous stage, and infrared radiation energy increased. In elastic–plastic
stage, the temperature fluctuated violently between 0.01 and 0.03
°C, the average surface temperature was obviously higher than
that in the compaction stage, and the infrared radiation energy had
little change. In the fracture stage, the temperature dropped rapidly
to the average temperature in the compaction stage, and infrared radiation
energy decreased.It can be seen from Figure that the average surface temperature of
coal-rock fluctuates
seriously in the loading process, so it is inappropriate to directly
merge it with axial stress. Therefore, in this study, the original
temperature data were smoothed according to its variation trend before
the fitting analysis. And during the loading process, 10–13
strains were selected as intermediate variables to get corresponding
temperature and axial stress data. (Each stage should have a certain
number of strain sampling points.) Then, linear fitting was carried
out for the sampled surface average temperature and axial stress data,
and the fitting results are shown in Figure and Table . It can be seen from Figure and Table that the surface average temperature of samples under
different loading conditions are in a first-order function relationship
with stress, and the correlation coefficients of the two are between
0.93 and 0.97. Therefore, it can be seen that there is a strong correlation
between temperature and stress, and the loading rate does not affect
the correlation trend, which is consistent with the form of eq above.
Table 4
Fitting Results and Correlation Coefficients
no.
fitting relation
correlation
coefficient
D1
Tave = 0.00242σ1 + 20.6529
0.9360
D4
Tave = 0.00519σ1 + 21.6314
0.9678
D8
Tave = 0.00321σ1 + 19.6618
0.9433
Figure 10
Stress–temperature
correlation curve. (a) The fitting results
of D1 uniaxial loading at 0.1 mm/min. (b) The fitting results
of D4 uniaxial loading at 0.3 mm/min. (c) The fitting results
of D8 uniaxial loading at 0.3 mm/min.
Stress–temperature
correlation curve. (a) The fitting results
of D1 uniaxial loading at 0.1 mm/min. (b) The fitting results
of D4 uniaxial loading at 0.3 mm/min. (c) The fitting results
of D8 uniaxial loading at 0.3 mm/min.
Analysis
of the Influence of Initial Confining
Pressure on the Correlation of Each Energy Characteristic Parameter
As the loading conditions of each triaxial test group are the same
and the trend is consistent, only the experimental results of S2, S4, and S7 are shown in Figure . As can be seen
from the experimental results and Figure , the surface temperature and deviatoric
stress changed in a consistent trend under different loading confining
pressures. Because the triaxial test must start from the state of
stress balance, there was no compaction stage similar to the uniaxial
test, but there were still four stages of elasticity, elastic–plastic
stage, yield, and fracture, which also had strong stage characteristics.
Figure 11
Triaxial
loading experimental results curve. (a) The experimental
result of S2 triaxial loading at 10 MPa. (b) The experimental
result of S4 triaxial loading at 15 MPa. (c) The experimental
result of S7 triaxial loading at 15 MPa.
Triaxial
loading experimental results curve. (a) The experimental
result of S2 triaxial loading at 10 MPa. (b) The experimental
result of S4 triaxial loading at 15 MPa. (c) The experimental
result of S7 triaxial loading at 15 MPa.As can be seen from Figure , changes of surface temperature at different mechanical
stages had stage characteristics: At the elastic stage, the temperature
fluctuated between 0.10 and 0.15 °C, which was more violent than
that of uniaxial loading, and the overall trend was relatively stable.
In the elastic–plastic stage, because the sample was a composite
material, the increase rate of deviational stress was larger than
that in the previous stage.[15] In this stage,
the temperature fluctuated rapidly and rose sharply in the early stage,
the average temperature was obviously higher than that in the elastic
stage, and an obvious peak of temperature appeared before the yield
stage. The duration of the yield stage was very short. In this stage,
the temperature of the sample surface still kept a rising trend for
a period of time, but it was not violent, and at the later stage,
it showed a rapid downward trend.According to the comparison
of Figures and 11, the variation
trend of surface average temperature of composite coal-rock during
triaxial loading was similar to that of uniaxial loading, and the
temperature peak was slightly earlier than the stress peak. In addition,
there was a high similarity between the deviatoric stress and temperature.
The fitting curves of Figure were obtained from the numerical fitting of axial stress
and temperature in Figure . And the data processing method before fitting is similar
to that in Figure . The fitting results are shown in Table . It can be seen from Figure and Table that the surface average temperature of samples under
different initial confining pressures are in a first-order function
relationship with stress, and the correlation coefficients of the
two are between 0.94 and 0.95. It can be seen that the initial confining
pressure does not affect the first-order function relation of correlation,
which is consistent with eq .
Figure 12
Stress–surface average temperature correlation curve. (a)
The fitting results of S2 triaxial loading at 10 MPa. (b)
The fitting results of S4 triaxial loading at 15 MPa. (c)
The fitting results of S7 triaxial loading at 15 MPa.
Table 5
Fitting Results and Correlation Coefficients
no.
fitting relation
correlation
coefficient
S2
Tave = 0.02179(σ1–σ3) + 19.6697
0.9414
S4
Tave = 0.01651(σ1–σ3) + 19.6482
0.9512
S7
Tave = 0.01774(σ1–σ3) + 19.2048
0.9463
Stress–surface average temperature correlation curve. (a)
The fitting results of S2 triaxial loading at 10 MPa. (b)
The fitting results of S4 triaxial loading at 15 MPa. (c)
The fitting results of S7 triaxial loading at 15 MPa.Based on the above experimental
analysis, it can be seen that there
is basically a linear relationship between the composite coal-rock
stress and the average surface temperature under different loading
conditions, and the fitting degree is higher than 0.93, which is consistent
with the description of eq in Section . Based on the derivation of eq in Section , it can be seen that the rationality of eq is based on the establishment
of eqs , 12, and 16. And the rationality
of eqs and 16 has been verified in other existing literatures.
On the basis of and in combination with the experimental analysis
in this section, the correctness of eq is similarly verified. Thus, the rationality of eq has been verified indirectly.
Establishment of the Composite Coal-Rock Energy
Coupling Mechanism during the Loading Process
Analysis
of Total Energy Conversion Trend
in the Loading Process
The deformation of composite coal-rock
under load is closely related to the energy conversion. As shown in eq , in the absence of other
exchanges, all the work done by the external environment is transformed
into elastic strain energy and dissipation energy. Figure a–c shows the variation
curves of total energy, dissipated energy, elastic strain energy,
and strain of D1, D4, and D8 at uniaxial
loading rates of 0.1, 0.3, and 1 mm/min, respectively, as well as
stress–strain curves. It can be seen from Figure a–c that the total
energy of composite coal-rock under the uniaxial condition was transformed
into various energies in different mechanical stages according to
different laws, and the loading rate did not affect the energy transformation
trend at each stage.
Figure 13
Energy change curve in the loading process. (a) The energy
change
curve with a uniaxial loading rate of 0.1 mm/min. (b) The energy change
curve with a uniaxial loading rate of 0.3 mm/min. (c) The energy change
curve with a uniaxial loading rate of 1 mm/min. (d) The energy change
curve of the initial confining pressure of 10 MPa under triaxial loading.
(e) The energy change curve of the initial confining pressure of 15
MPa under triaxial loading. (f) The energy change curve of the initial
confining pressure of 20 MPa under triaxial loading.
Energy change curve in the loading process. (a) The energy
change
curve with a uniaxial loading rate of 0.1 mm/min. (b) The energy change
curve with a uniaxial loading rate of 0.3 mm/min. (c) The energy change
curve with a uniaxial loading rate of 1 mm/min. (d) The energy change
curve of the initial confining pressure of 10 MPa under triaxial loading.
(e) The energy change curve of the initial confining pressure of 15
MPa under triaxial loading. (f) The energy change curve of the initial
confining pressure of 20 MPa under triaxial loading.As the trend of all curves was consistent, only Figure a was used for
specific analysis
below: In the compaction stage, more than 99% of the total energy
was converted to elastic strain energy; however, the part that was
converted into dissipated energy was very little. The total energy
increased slowly, which was similar to the change trend of stress.
In this stage, the energy was mostly elastic deformation, and the
total energy density reached 4.757 mJ/mm3 at the end. At
the elastic stage, the total energy increased rapidly, and the growth
rate reached 24.3738 mJ/mm3 later. At this stage, most
of the total energy was still converted into elastic strain energy,
but the growth rate was significantly lower than that of the total
energy, and the conversion rate gradually decreased, while the conversion
dissipation energy increased significantly, but the total energy did
not exceed the elastic strain energy. At the end of this stage, the
energy density of both was 12.788 mJ/mm3. At this time,
the external work was still mostly used for elastic deformation, but
due to the complex internal structure of materials, some areas had
reached the elastic limit. As the loading process progresses, the
inelastic proportion area of samples increased, and part of the total
energy was converted into dissipated energy to be consumed. In the
elastic–plastic stage, the total energy kept increasing at
a high rate. In the early part of this stage, the elastic strain energy
and dissipation energy increased almost at the same rate, with a growth
rate of 6931.394 mJ/mm3, which was significantly higher
than that in the previous stages. In addition, the conversion ratio
of the two energies was the same until the strain reached 0.013. At
this point, the elastic strain energy reached the energy peak, and
its value was 19.575 mJ/mm3. It can be seen that there
was an energy crossing point at which the elastic strain energy and
dissipated energy had the same value and appeared earlier than the
stress peak. The total energy conversion trend changed after this
point. At this time, the elastic strain energy decreased rapidly,
while the dissipated energy density increased, with the growth rate
being 23976.865 mJ/mm3. The total energy and excess elastic
strain energy were almost all converted to dissipative energy. And
the energy density of elastic strain energy was stable at 11.352 mJ/mm3 before coal-rock fracture. It can be seen that although the
specimen was still mainly elastic deformation in the early elastic–plastic
stage, it would eventually reach a limit. The inelastic region continued
to increase with the loading and eventually became dominant, which
led to the release of most of the remaining energy into dissipative
energy. At this time, the sample had a tendency to partially rupture
and the sound of rupture could be heard outside. When entering the
fracture stage, the elastic strain energy of the sample remained stable,
and the total energy almost changed to dissipative energy, which still
kept a high growth rate. Finally, the dissipated energy reached the
energy peak of 68.046 mJ/mm3, the sample broke, and the
dissipated energy was released.Figure d,e shows
the variation curves of total energy, dissipated energy, elastic strain
energy, and strain of samples S2, S4, and S7 under triaxial loading at confining pressures of 10, 15,
and 20 MPa, respectively, as well as the deviant stress–strain
curves. It can be seen from Figure d,e that the relationship between stress state and
energy of composite coal-rock under triaxial loading is similar to
that under uniaxial shown in Figure a-c, and the total energy is transformed into different
energy trends at different mechanical stages. The total energy transformation
rule of the triaxial is similar to that of the uniaxial. Because the
triaxial stress balance needs to be loaded before the triaxial loading,
there is no compaction stage in Figure d,e. Figure e is taken as an example for specific analysis
below: At the elastic stage, the total energy increased at the rate
of 2118.563 mJ/mm3, and almost all the external work was
converted to elastic strain energy, while the dissipation energy could
be ignored because of the low conversion rate. At this moment, the
elastic deformation of the sample could be seen externally. In the
elastic–plastic stage, the total energy increased rapidly and
the rate increased to 3513.290 mJ/mm3. Meanwhile, elastic
strain energy kept increasing slowly but the growth rate decreased
and it gradually approached the energy peak of 24.319 mJ/mm3. In this stage, the total energy was transformed into dissipated
energy at a faster speed, which was similar to the early elastic–plastic
stage of uniaxial. However, the elastic strain energy still existed
in a large amount inside the specimen, so the outer part of the specimen
was still elastic deformation, but the inner part had a plastic deformation
trend. At the initial stage of yield, the total energy conversion
dissipation energy kept increasing, the elastic strain energy was
almost stable at 7.558 mJ/mm3, and the energy density was
25.402 mJ/mm3 when the strain was 0.0056, which was earlier
than that of stress. Since then, almost all the total energy was converted
to dissipative energy, and part of elastic strain energy was also
converted to it, which led to the rapid growth of dissipative energy
until rupture. This stage was the same as the later stage of the uniaxial
loading elastic–plastic stage. The plastic deformation trend
of the sample was gradually greater than the elastic, and finally,
the specimen cracked because the plastic deformation reached the load
strength. To sum up, under triaxial loading, there is a corresponding
relationship between energy transformation trend and stress. Before
the rupture, it has the same characteristics as the uniaxial one;
that is, the dissipated energy increases significantly and the elastic
strain energy remains stable. Therefore, it is feasible to predict
the trend of coal-rock rupture by using energy characteristics.
Trend Analysis of Infrared Radiant Energy
and Establishment of Its Coupling Mechanism with Dissipative Energy
According to the above analysis, the change of energy state of
composite coal-rock during loading can be expressed by eq , and infrared radiant energy is
one of the components of dissipated energy. According to eq , the dissipated energy can be expressed
as infrared radiant energy Eh and dissipated
energy excluding infrared radiant energy WΔ. Thus, eq can be
processed to obtain the relation of eq , as follows:where Eh is infrared radiant
energy (J); Uh is infrared radiant energy
density, which is proportional to the
infrared radiant energy under the same volume (J/m3); and UΔ is the energy density of dissipated
energy excluding infrared radiant energy (J/m3).According to eq ,
when the sample volume is certain, the infrared radiation energy of
the object is proportional to the infrared radiation energy density,
and the variation trend of the infrared radiation energy Eh is consistent with that of the infrared radiation energy
density Uh. Therefore, the variation law
of energy density can be obtained by analyzing the variation of infrared
radiation energy, which is helpful for the in-depth analysis of the
relationship between infrared radiation energy, dissipated energy,
and total energy. The infrared radiation energy of composite coal-rock
under uniaxial and triaxial loading can be obtained by calculation
using eq . Since each
sample has the same variation trend under the same loading condition,
only uniaxial D1, D4, and D8 and
triaxial S2, S4, and S7 were analyzed. Figure shows the curves
of energy density and infrared radiation energy of the six samples
changing with strain.
Figure 14
The curve of infrared radiation energy in loading. (a–c)
The variation trend of energy density, infrared radiation energy,
and strain of composite coal-rock under uniaxial loading rates of
0.1, 0.3, and 1 mm/min, respectively. (d–f) The variation trends
of energy density, infrared radiation energy, and strain of the samples
under confining pressures of 10, 15, and 20 MPa, respectively.
The curve of infrared radiation energy in loading. (a–c)
The variation trend of energy density, infrared radiation energy,
and strain of composite coal-rock under uniaxial loading rates of
0.1, 0.3, and 1 mm/min, respectively. (d–f) The variation trends
of energy density, infrared radiation energy, and strain of the samples
under confining pressures of 10, 15, and 20 MPa, respectively.According to the analysis of Figures and 11 above, it
can be seen that the trend of temperature on the sample surface corresponds
to each mechanical stage. In addition, it can be seen from Figure that the variation
trend of infrared radiation energy and temperature of coal-rock under
uniaxial or triaxial loading is basically consistent, which has similar
characteristics in various mechanical stages under uniaxial or triaxial
loading. To summarize the variation characteristics of various mechanical
stages of infrared radiation energy in the loading process, the stress
increase process in the early uniaxial elastic–plastic stage
is referred to as the elastic–plastic stage, and the transient
stress fluctuation in the later stage is referred to as the yield
stage. Although coal-rock fracture is a way of releasing dissipative
energy, it is very unlikely to directly measure it. As one of the
forms of dissipative energy, infrared radiation energy can be measured
without contact, which is helpful to judge the state of samples.It can be seen from Figure that infrared radiation energy was correlated with
the variation trend of dissipated energy. Figure a under the uniaxial condition and Figure e under the triaxial
condition were taken as examples for analysis. In the compaction and
elastic stages, the total energy was mainly elastic deformation energy.
Although the dissipative energy increased slowly, there was no obvious
increase trend in general. Meanwhile, the infrared radiation energy
changed steadily. At this stage, two energies remained stable at 9.869
and 8.521 mJ, respectively. At the later stage, the dissipated energy
began to rise, and the infrared radiation energy increased slowly
in accordance with it. At the early stage of the elastic–plastic
phase, the dissipative energy began to increase significantly, and
the growth rate under uniaxial and triaxial loading was 5826.818 and
3772.337 mJ/mm3, respectively. At this time, the infrared
radiation energy increased significantly and obvious stages appeared,
consistent with the change of dissipative energy. Near the intersection
point of elastic strain energy and dissipative energy, the dissipative
energy increased rapidly and nearly linearly, the infrared radiation
energy increased to a high energy value (9.996 mJ under the uniaxial
condition and 9.796 mJ under the triaxial condition), and the infrared
radiation energy peak appeared. According to the law of energy conservation
and the curve change in Figure , the infrared radiation energy at this time came from
two parts, mainly from the dissipated energy converted and the transformation
of elastic strain energy, which resulted in the sharp increase and
high energy peak of infrared radiation energy. In the yield stage,
the total energy was mainly transformed into dissipative energy release
rather than elastic strain energy. Although the infrared radiation
energy still kept the high energy value fluctuation at the early part
of this stage, the drop occurred significantly earlier than the stress
peak and fracture stage. Combined with the analysis of eq , when the proportion of the infrared
radiation energy of the dissipated energy begins to decline significantly,
the proportion of dissipated energy excluding infrared radiant energy UΔ (i.e., kinetic energy, plastic deformation
energy, etc.) will rise significantly, and the composite coal-rock
will begin to enter the fracture deformation stage. At this time,
the fracture sound of the sample could be heard externally and cracks
could be produced until the penetrating cracks occurred. Therefore,
in the late yield and fracture stage, the dissipation energy realization
form changed, and the infrared radiation energy was no longer dominant,
which fluctuated stably with a low energy value without an increasing
trend. At this time, the dissipated energy excluding infrared radiant
energy was dominant, leading to fracture.To sum up, infrared
radiant energy is closely related to dissipated
energy in the loading process. It also can be seen that the change
trend of dissipated energy can be obtained by analyzing the change
of infrared radiation energy, and the stress state of composite coal-rock
samples can be further obtained. Finally, noncontact prediction of
coal-rock state can be achieved by monitoring infrared radiation energy.
The method to judge the state of composite coal-rock by using the
coupling mechanism of dissipated energy and infrared radiation energy
is shown in Figure . The thickness of the shear head represents the amount of energy
obtained by the conversion.
Figure 15
A method to judge the state of coal-rock by
the coupling relation
of dissipated energy and infrared radiation energy.
A method to judge the state of coal-rock by
the coupling relation
of dissipated energy and infrared radiation energy.As can be seen from Figure , in the loading process, the internal energy of composite
coal-rock will increase due to the action of external mechanical energy.
And the increased internal energy will be further transformed into
elastic deformation energy and dissipation energy. However, the trend
of coal-rock internal energy transformation is different in each loading
stage. In the early loading stage, the increment of internal energy Wi is mostly converted to elastic strain energy We but rarely to dissipated energy Wd. However, from the elastic–plastic stage, the
elastic strain energy We of coal-rock
basically reaches the upper limit, which leads to the residual internal
energy increment Wi and part of elastic
strain energy We conversion into dissipated
energy Wd. It also can be seen from Figure that the change
of dissipated energy Wd has an obvious
corresponding relationship with the state of composite coal-rock.
When the dissipated energy Wd increases
rapidly, the fracture process of coal-rock accelerates obviously.According to eq and Figure , dissipative energy
can be considered in two forms, one of which is infrared radiant energy
and the other is other energy, and at different stress stages, the
main forms of dissipated energy are different. Before the elastic–plastic
stage, the main form of dissipated energy is infrared radiation energy,
and the growth trend of it is almost the same as that of dissipated
energy. At this time, based on the above analysis, the composite coal-rock
mainly has elastic deformation, the fracture trend is not obvious,
and there is no obvious crack outside. After this stage, the form
of dissipation energy changes: the proportion of infrared radiation
energy decreases, while the other forms of energy increases. Although
the infrared radiation energy still keeps increasing in a short time,
it tends to saturate obviously. In addition, the performance of other
forms of energy is more obvious, and the coal-rock begins the plastic
deformation and the production of visible cracks. Finally, before
the fracture, the infrared radiation energy decreases rapidly, but
the dissipation energy increases rapidly, and other forms of energy
increase obviously, which lead to the fracture of the sample.It can be seen that there is an obvious coupling relationship between
infrared radiation energy and dissipated energy, and the dissipated
energy state that is difficult to be measured directly can be understood
by analyzing the infrared radiation energy state. On this basis, the
stress state of coal-rock can be obtained by using this relationship.At present, contact detection is still the main method to predict
the fracture trend of composite coal-rock. Although some studies have
used energy theory to predict the failure state, most of them are
based on the analysis of elastic strain energy and dissipated energy
and rarely involve the analysis of the specific expression form of
dissipated energy. So, the relationship between infrared radiant energy
and dissipated energy constructed in Figure can provide new ideas for the research
in this field and is conducive to further research on noncontact coal-rock
fracture state prediction technology.
Conclusions
(1) This paper analyzes the transformation mechanism
of various
energies and the generation mechanism of infrared radiation energy
in the loading process of composite coal-rock from a microscopic perspective.
Based on the theory of friction heat generation and heat conduction,
the mathematical model of energy characteristic parameters is established
by using the method of micro element analysis. On this basis, the
coupling model of dissipated energy and infrared radiation energy
is further deduced and established based on the thermodynamics theory
and Stefan–Boltzmann law.(2) The variation of dissipated
energy in the loading process of
composite coal-rock has stages. In the early stages of loading, the
dissipation energy obtained by energy conversion is small, but it
increases rapidly in the late stages, which causes the rupture of
the coal-rock. And the components of dissipated energy are different
at different stages, which are closely related to the deformation
state of coal-rock.(3) There is correlation between the variation
of infrared radiation
energy and dissipation energy. In the early stage, the trend of the
two is basically the same, but in the late stage, the infrared radiation
energy does not increase significantly, which is different from the
trend of dissipation energy. In addition, the infrared radiation energy
drops obviously earlier than coal-rock fracture, which has a certain
precursor. Based on this, the relationship between infrared radiation
energy and dissipated energy is established, and the change rule of
coal-rock state based on energy transformation is further obtained.
It will provide a new method to prevent coal-rock dynamic disaster.
Authors: Rob F M van Doremalen; Jaap J van Netten; Jeff G van Baal; Miriam M R Vollenbroek-Hutten; Ferdinand van der Heijden Journal: J Diabetes Sci Technol Date: 2019-06-14