Literature DB >> 35221667

Efficient Synthesis of 6,6´-Diamido-2,2´-dipicolylamine Ligands for Potential Phosphate Anion Sensing.

Shuai Wang1,2, Lichong Gong3, Georges El Fakhri1, Junfeng Wang1.   

Abstract

We report here the efficient synthesis of 6,6´-diamido-2,2´-dipicolylamines (DA-DPAs) which could be applied to phosphate anion sensing via pre-formed metal complexes. The design was based on the retrosynthetic analysis. This strategy enabled us to achieve the functionalized DA-DPAs in satisfactory yields with high purity using the Boekelheide rearrangement. Meanwhile, all the intermediates could be easily purified by silica gel column chromatography.

Entities:  

Year:  2021        PMID： 35221667      PMCID： PMC8865135          DOI： 10.1039/d1nj03030b

Source DB:  PubMed          Journal:  New J Chem        ISSN： 1144-0546            Impact factor:   3.925


  54 in total

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4.  Novel asymmetrically functionalized bis-dipicolylamine metal complexes: peripheral decoration of a potent anion recognition scaffold.

Authors:  Joel A Drewry; Steven Fletcher; Haider Hassan; Patrick T Gunning
Journal:  Org Biomol Chem       Date:  2009-10-12       Impact factor: 3.876

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Authors:  John H Conway; Dorothea Fiedler
Journal:  Angew Chem Int Ed Engl       Date:  2015-02-04       Impact factor: 15.336

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7.  Electrocatalytic Hydrogen Production by a Nickel(II) Complex with a Phosphinopyridyl Ligand.

Authors:  Ryo Tatematsu; Tomohiko Inomata; Tomohiro Ozawa; Hideki Masuda
Journal:  Angew Chem Int Ed Engl       Date:  2016-03-16       Impact factor: 15.336

8.  Fluorenone based fluorescent probe for selective "turn-on" detection of pyrophosphate and alanine.

Authors:  Daniel Thangadurai T; Nithya I; Manjubaashini N; Bhuvanesh N; Bharathi G; Nandhakumar R; Nataraj D
Journal:  Spectrochim Acta A Mol Biomol Spectrosc       Date:  2017-11-06       Impact factor: 4.098

9.  Phosphorescent sensor for phosphorylated peptides based on an iridium complex.

Authors:  Jung Hyun Kang; Hee Jin Kim; Tae-Hyuk Kwon; Jong-In Hong
Journal:  J Org Chem       Date:  2014-06-20       Impact factor: 4.354

10.  Manganese-Based Contrast Agents for Magnetic Resonance Imaging of Liver Tumors: Structure-Activity Relationships and Lead Candidate Evaluation.

Authors:  Junfeng Wang; Huan Wang; Ian A Ramsay; Derek J Erstad; Bryan C Fuchs; Kenneth K Tanabe; Peter Caravan; Eric M Gale
Journal:  J Med Chem       Date:  2018-09-25       Impact factor: 7.446
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