Literature DB >> 34662572

Determination of proteinaceous free amino acids by gas chromatography.

Ken'ichi Ichihara1, Chihiro Kohsaka2, Yoshihiro Yamamoto2.   

Abstract

A method was developed for determination of proteinaceous free amino acids by gas chromatography-mass spectrometry (GC-MS). The guanidino group of arginine in amino acid samples was modified with 1,2-cyclohexanedione at room temperature under basic conditions, and all amino acids were directly derivatized with isobutyl chloroformate. The amino acid derivatives formed were analyzed by GC-MS. The method developed was applied successfully for the determination of amino acids in the Japanese alcoholic beverage, sake.
Copyright © 2021 Elsevier Inc. All rights reserved.

Entities:  

Keywords:  1,2-Cyclohexanedione; Arginine; Gas chromatography; Guanidino group; Sake

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Year:  2021        PMID： 34662572     DOI： 10.1016/j.ab.2021.114423

Source DB:  PubMed          Journal:  Anal Biochem        ISSN： 0003-2697            Impact factor:   3.365


  2 in total

1.  Qualitative and quantitative analyses of chemical components of Citri Sarcodactylis Fructus from different origins based on UPLC-Q-Exactive Orbitrap-MS and GC-MS.

Authors:  Jinrong Ning; Kanghui Wang; Wanling Yang; Mengshi Liu; Jingyuan Tian; Minyan Wei; Guodong Zheng
Journal:  Food Sci Nutr       Date:  2022-03-14       Impact factor: 3.553

2.  Development of a Simple, Underivatized Method for Rapid Determination of Free Amino Acids in Honey Using Dilute-and-Shoot Strategy and Liquid Chromatography-Tandem Mass Spectrometry.

Authors:  Wen Ma; Bingxin Yang; Jun Li; Xianjiang Li
Journal:  Molecules       Date:  2022-02-04       Impact factor: 4.411
  2 in total

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