Literature DB >> 34345071

Storage and Pre-Neutron Activation Analysis Treatment for Trace Element Analysis in Urine.

Alan J Blotcky1, Edward P Rack2.   

Abstract

The problems regarding storage and pre-neutron activation analysis treatment for the elements aluminum, calcium, vanadium, selenium, copper, iodine, zinc, manganese, and magnesium in a urine matrix are reviewed. The type of collection and storage procedure and pre-neutron activation analysis treatment of mine depend on the specific trace element; that is, its inherent physical and chemical properties. Specifically polyethylene in teflon containers are the most suitable for general determinations. Whether any preservative is added would depend upon the stability of the trace element and its tendency for surface adsorption. Preferably preservatives should contain no radioactivatable elements for maximum efficacy. Freeze drying or packing urine shipments under dry ice needs to be explored on an individual basis. Each pre- or post-neutron activation analysis treatment is specific and optimized for the trace element analyzed.

Entities:  

Keywords:  aluminium; calcium; iodine; magnesium; manganese; neutron activation analysis; pre-NAA treatment; selenium; storage; urine; vanadium; zinc

Year:  1986        PMID: 34345071      PMCID: PMC6658440          DOI: 10.6028/jres.091.015

Source DB:  PubMed          Journal:  J Res Natl Bur Stand (1977)        ISSN: 0160-1741


  10 in total

1.  Neutron activation analysis for bulk and trace elements in urine.

Authors:  R Cornelis; A Speecke; J Hoste
Journal:  Anal Chim Acta       Date:  1975-09       Impact factor: 6.558

2.  Determination of trace aluminum in urine by neutron activation analysis.

Authors:  A J Blotcky; D Hobson; J A Leffler; E P Rack; R R Recker
Journal:  Anal Chem       Date:  1976-06       Impact factor: 6.986

3.  Evidence of aluminum absorption from the gastrointestinal tract and bone deposition by aluminum carbonate ingestion with normal renal function.

Authors:  R R Recker; A J Blotcky; J A Leffler; E P Rack
Journal:  J Lab Clin Med       Date:  1977-11

4.  Determination of iodine in urine by neutron activation analysis. Application of the Szilard-Chalmers effect.

Authors:  A J Blotcky; D M Duven; W M Grauer; E P Rack
Journal:  Anal Chem       Date:  1974-06       Impact factor: 6.986

5.  Rapid and simple continuous radiochemical separation of copper, magnesium, zinc, and manganese in biological materials.

Authors:  K J Hahn; D J Tuma; J L Sullivan
Journal:  Anal Chem       Date:  1968-05       Impact factor: 6.986

6.  Determination of selenium in urine by neutron activation analysis.

Authors:  R Weingarten; Y Shamai; T Schlesinger
Journal:  Int J Appl Radiat Isot       Date:  1979-10

7.  Determination of chlorinated pesticides in urine by molecular neutron activation analysis.

Authors:  L R Opelanio; E P Rack; A J Blotcky; F W Crow
Journal:  Anal Chem       Date:  1983-04       Impact factor: 6.986

8.  Determination of iodoamino acids and thyroid hormones in a urine matrix by neutron activation analysis.

Authors:  M L Firouzbakht; S K Garmestani; E P Rack; A J Blotcky
Journal:  Anal Chem       Date:  1981-10       Impact factor: 6.986

9.  Comparison between neutron activation analysis and graphite furnace atomic absorption spectrometry for trace aluminum determination in biological materials.

Authors:  K Garmestani; A J Blotcky; E P Rack
Journal:  Anal Chem       Date:  1978-01       Impact factor: 6.986

10.  Accurate measurement of stable isotopes 46Ca and 48Ca in human feces, plasma, and urine in relation to human nutrition of calcium.

Authors:  M Janghorbani; A Sundaresan; V R Young
Journal:  Clin Chim Acta       Date:  1981-07-01       Impact factor: 3.786

  10 in total

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