Literature DB >> 34298526

When X-rays alter the course of your experiments.

Wim Bras1, Dean Myles1, Roberto Felici2.   

Abstract

The continuing increase in the brilliance of synchrotron radiation beamlines allows for many new and exciting experiments that were impossible before the present generation of synchrotron radiation sources came on line. However, the exposure to such intense beams also tests the limits of what samples can endure. Whilst the effects of radiation induced damage in a static experiment often can easily be recognized by changes in the diffraction or spectroscopy curves, the influence of radiation on chemical or physical processes, where one expects curves to change, is less often recognized and can be misinterpreted as a 'real' result instead of as a 'radiation influenced result'. This is especially a concern in time-resolved materials science experiments using techniques as Powder Diffraction, Small Angle Scattering and X-ray Absorption Spectroscopy. Here, the effects of radiation (5 - 50 keV) on some time-resolved processes in different types of materials and in different physical states are discussed. We show that such effects are not limited to soft matter and biology but rather can be found across the whole spectrum of materials research, over a large range of radiation doses and is not limited to very high brilliance beamlines.
© 2021 IOP Publishing Ltd.

Keywords:  material science; radiation interactions; synchrotron radiation; time-resolved experiments

Year:  2021        PMID: 34298526     DOI: 10.1088/1361-648X/ac1767

Source DB:  PubMed          Journal:  J Phys Condens Matter        ISSN: 0953-8984            Impact factor:   2.333


  2 in total

1.  Data Mining of Polymer Phase Transitions upon Temperature Changes by Small and Wide-Angle X-ray Scattering Combined with Raman Spectroscopy.

Authors:  Sarah Saidi; Giuseppe Portale; Wim Bras; Alessandro Longo; José Manuel Amigo; David Chapron; Patrice Bourson; Daniel Hermida-Merino
Journal:  Polymers (Basel)       Date:  2021-11-30       Impact factor: 4.329

2.  Radiolysis-Driven Evolution of Gold Nanostructures - Model Verification by Scale Bridging In Situ Liquid-Phase Transmission Electron Microscopy and X-Ray Diffraction.

Authors:  Birk Fritsch; Tobias S Zech; Mark P Bruns; Andreas Körner; Saba Khadivianazar; Mingjian Wu; Neda Zargar Talebi; Sannakaisa Virtanen; Tobias Unruh; Michael P M Jank; Erdmann Spiecker; Andreas Hutzler
Journal:  Adv Sci (Weinh)       Date:  2022-07-03       Impact factor: 17.521

  2 in total

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