Shutong Li1,2, Xianyang Liu3, Xiuqin Deng3, Xiao Hui3, Ruiliang Guo1,2,4, Junlin Chen1,2,5, Jiaqiang Zhang1,2,5. 1. Northwest Institute of Eco-Environment and Resources, Chinese Academy of Sciences, Lanzhou 730030, China. 2. Key Laboratory of Petroleum Resources, Lanzhou 730000, Gansu, China. 3. PetroChina Changqing Oil Field Company, Xi'an 710018, China. 4. School of Earth Sciences and Engineering; Shaanxi Key Laboratory of Petroleum Accumulation Geology, Xi'an Shiyou University, Xi'an 710065, China. 5. University of Chinese Academy of Sciences, Beijing 100049, China.
Abstract
Exploring the tightness mechanism through a quantitative analysis of the pore evolution process is the research hotspot of tight oil reservoirs. The physical characteristics of Chang 6 (Ch-6) sandstones in the western Jiyuan area have the typical features of a tight oil reservoir. Based on the reservoir physical property, lithological characteristics, diagenetic types and sequence, and burial and thermal evolution history, this study analyzes the factors leading to reservoir tightness and establishes the model of the pore evolution process. The results show that the sedimentary microfacies type controls the reservoir detrital material and further affects its physical properties. The high content of feldspar and rock fragments and the fine grain size are the material cause for the reservoir tightness. The sandstones of the main underwater distributary channel are the dominant sedimentary bodies for the development of a high-quality reservoir. In terms of diagenesis, compaction is the primary cause for reservoir tightness, and the porosity reduction by cementation is weaker than that by compaction. Meanwhile, the quantitative calculation results indicate that the porosity losses by compaction, carbonate cementation, kaolinite cementation, chlorite coatings, and siliceous cementation are 23.5, 3.1, 3.8, 3.0, and 0.8%, respectively. In addition, dissolution is significant to improve the reservoir physical property, and the increase of dissolved porosity is around 3.2%. More significantly, this study uses a detailed and systematic method for analyzing the tightness mechanism and the pore evolution process of the Ch-6 sandstones in the western Jiyuan area, Ordos Basin, China.
Exploring the tightness mechanism through a quantitative analysis of the pore evolution process is the research hotspot of tight oil reservoirs. The physical characteristics of Chang 6 (Ch-6) sandstones in the western Jiyuan area have the typical features of a tight oil reservoir. Based on the reservoir physical property, lithological characteristics, diagenetic types and sequence, and burial and thermal evolution history, this study analyzes the factors leading to reservoir tightness and establishes the model of the pore evolution process. The results show that the sedimentary microfacies type controls the reservoir detrital material and further affects its physical properties. The high content of feldspar and rock fragments and the fine grain size are the material cause for the reservoir tightness. The sandstones of the main underwater distributary channel are the dominant sedimentary bodies for the development of a high-quality reservoir. In terms of diagenesis, compaction is the primary cause for reservoir tightness, and the porosity reduction by cementation is weaker than that by compaction. Meanwhile, the quantitative calculation results indicate that the porosity losses by compaction, carbonate cementation, kaolinite cementation, chlorite coatings, and siliceous cementation are 23.5, 3.1, 3.8, 3.0, and 0.8%, respectively. In addition, dissolution is significant to improve the reservoir physical property, and the increase of dissolved porosity is around 3.2%. More significantly, this study uses a detailed and systematic method for analyzing the tightness mechanism and the pore evolution process of the Ch-6 sandstones in the western Jiyuan area, Ordos Basin, China.
Unconventional oil and
gas are important components of hydrocarbon
resources, including shale gas, shale oil, tight sandstone oil, natural
gas hydrates, etc.[1−5] Tight sandstone oil comes from sandstone reservoirs with porosity
less than 10%, air permeability less than 1 mD, or in situ matrix
permeability less than 0.1 mD.[6] The sandstones
of the Upper Triassic Yanchang formation in the Ordos basin are characterized
by low porosity, ultralow permeability, and abundant oil resources.[7−10] In the Yanchang formation, Chang 6 (Ch-6) has huge potential for
exploration and development of tight oil, with reserves of more than
100 million tons in the Jiyuan, Xifeng, and Huaqing areas.[11−15]At present, quantitative analysis of the reservoir pore evolution
is the research hotspot in the study of reservoir and diagenesis.
In 1987, David firstly established the calculation method of porosity
evolution using thin-section analysis data and achieved good results
in the calculation of the compaction porosity loss of Jurassic feldspathic
quartz sandstones in Utah and Ordovician quartz sandstones in Oklahoma.[16] Later, Ehrenberg demonstrated the quantitative
simulation method of porosity evolution and proposed the useful supplements
of the compaction porosity loss calculation method, statistical method
of thin sections, effects of particle solution on compaction porosity
loss, and repeatability of the calculated results.[17] In addition, the studies on the Ventura Basin in California
by Wilson and that on the Bermejo Basin in Argentina by Damanti have
achieved effective applications.[18,19] In terms of
Chinese research studies, many scholars have done many works in the
quantitative analysis of the reservoir pore evolution and obtained
productive results in the Ordos Basin, Bohai Bay Basin, Junggar Basin,
and Songliao Basin.[20−25]Previous studies focused more on the overall effect of compaction
and cementation but ignored the individual effects of various types
of cementation and the “specific process” of reservoir
tightness.[25−27] At the same time, from the simulation method of pore
evolution based on thin-section data, it is difficult to accurately
evaluate the dissolved contents of each component and the variation
of rock skeleton volume in the diagenetic process. Such statistical
errors need to be inhibited through the method of sample screening
and data processing.[24]Above all,
this paper uses a detailed and systematic method for
studying the reservoir tightness mechanism via the analysis of the
porosity evolution process of the Ch-6 reservoir in the western Jiyuan
(WJY) area, hoping that it could provide a scientific basis for the
relative studies of tight oil reservoirs in other areas.
Geological Setting
The Ordos Basin is a polycyclic craton
margin basin in North China,
which is characterized by stable subsidence and multiple migrations
of depocenters, and it is composed of the Precambrian basement and
Phanerozoic sediments.[28,29] The oil and gas resources of
the Ordos Basin are abundant, and the petroleum geology conditions
are relatively simple.[30,31] The internal structure of the
basin is relatively simple, and the strata are relatively gentle with
a dip angle of less than 1°, but faults and thrust structures
abundantly exist in the western margin due to the later influences
of the Yanshan movement.[14] According to
the nature of the basin basement, the structure form, and characteristics,
it can be divided into six first-level tectonic units: the Yimeng
uplift, the Weibei uplift, the west margin thrust belt, the Jinxi
flexure belt, the Tianhuan depression, and the Shanbei slop.[32] The western Jiyuan (WJY) area, which is located
in the western area of the Ordos Basin, spans the Tianhuan depression
(Figure a,b) and presents
a gentle monoclinal structure sloping westward. In the sedimentary
period of Yanchang formation, the basin is a half-graben-like sag,
extending along the south and north directions, with a steep and narrow
western flank and a moderate eastern flank.[8] A complete continental river–delta–lake depositional
system is developed in the Triassic Yanchang formation of the Ordos
Basin, which continuously and stably presents the three stages of
lake-transgression to lake-flooding to lake regression. Accordingly,
the Yanchang formation records the whole process of the formation,
development, prosperity, decline, and extinction of the lake basin
with a 12 Ma time span, which can be subdivided into 10 areas represented
as Ch-1 (at the top) to Ch-10 (at the bottom).[32] Ch-6 is the regressive deposit after the heyday of the
Ch-7 lake basin, which develops the deep lake, semideep lake, and
delta facies from the basin center to the margin. The thickness of
the Ch-6 formation is 80–110 m (Figure ), which is comfortably in contact with the
Ch-7 formation; the typical delta deposits are mainly composed of
gray sandstone, dark mudstone, and thin coal seam.[33] In the WJY area, the underwater distributary channels are
well developed in the delta front and the distributary channels are
partly developed in the delta plain, which are controlled by the provenance
of northwestern Alxa ancient land.[34]
Figure 1
(a) Ordos Basin
tectonic units and location of the study area.
(b) Map showing the distribution of CH-61 sand bodies in
the WJY area.
Figure 2
Lithology section and depositional environment
of the Upper Triassic
Yanchang formation in the Ordos Basin, China.
(a) Ordos Basin
tectonic units and location of the study area.
(b) Map showing the distribution of CH-61 sand bodies in
the WJY area.Lithology section and depositional environment
of the Upper Triassic
Yanchang formation in the Ordos Basin, China.
Materials and Methods
All kinds of data used in this
study were collected from the core
samples of the Ch-6 sandstone reservoirs in the WJY area. First, the
data on porosity, permeability, grain size, and the mercury pressure
test were collected from the Changqing Oilfield Company. Based on
the data on the physical properties of 414 samples and the mercury
pressure data of 12 samples, this study analyzed the pore structure
and pore-throat features of the Ch-6 tight oil reservoirs. At the
same time, data on the grain size obtained from nine samples were
utilized to assess particle sizes and calculate the sorting coefficient
(S0) as well as the initial porosity of
the Ch-6 reservoirs according to the method published by Scherer.[35]In addition, 62 samples were collected
from 43 Wells for microscopic
petrology and pore-throat identification in the Key Laboratory of
Petroleum Resources Research, Institute of Geology and Geophysics,
Chinese Academy of Sciences. By observing 152 thin sections, the statistical
analysis was performed, which includes mineral type and content, the
degree of sorting and roundness, pore type, current thin porosity,
the content of dissolved pores, the content of original intergranular
pores, and cements content. The thin sections were impregnated with
red and blue epoxy resin to highlight the pore spaces, and some of
them were stained with Alizarin Red S and K-ferricyanide for carbonate
mineral identification. The mineral composition and pore space were
observed with Axioskop 40 polarizing microscope manufactured by Zeiss.
An optical collection system was used to quantify thin-section porosity
and diagenetic cements content by counting at least 350 points of
each thin section. The method of point counting and proportion counting
was mainly utilized in the quantitative calculation of detrital components
and all kinds of pore content.[16,17] Moreover, 11 freshly
broken chips of reservoir samples were prepared, and the MERLIN field
emission scanning electron microscope (FE-SEM) equipped with the energy-dispersive
X-ray (EDS) system manufactured by Zeiss was used to carry out a more
detailed observation on the morphology of authigenic clay minerals
and intergranular cement. On the basis of thin-section observation,
the diagenetic stages of Ch-6 in the WJY area were identified according
to the China Petroleum Standard of the Division of Diagenetic Stage
in Clastic Rocks (SY/T 5477-2003). At last, mathematical statistics
were used in the quantitative calculation of porosity in different
diagenetic stages following the methods published by Lai et al.[36]The carbon and oxygen isotopes of 45 sandstone
samples were measured
in the Key Laboratory of Petroleum Resources Research, Institute of
Geology and Geophysics, Chinese Academy of Sciences. The specific
process is to carry out the accurate measurement of carbon and oxygen
stable isotopes of CO2 that were released from the dissolution
of carbonate materials by H3PO4 with a MAT-252
isotope mass spectrometer. The measurement accuracy is less than 0.5‰,
and all isotope data were calibrated with standard samples including
NBS-18, GBW04405, and GBW04406. Ultimately, the data were presented
relative to the Vienna PeeDee Belemnite (V-PDB) and in the δ
notation.
Results
Reservoir Lithology
Through observation
and statistical analysis of more than 150 thin sections, the Ch-6
reservoirs in the WJY area were found to be mainly composed of lithic
arkose, feldspathic litharenite, and a small amount of arkose according
to Folk’s classification scheme[37] (Figure a). The
detrital compositions of reservoir sandstones are dominated by quartz,
ranging from 11.29 to 46.67% with an average of 29.83%, feldspar,
ranging from 7.17 to 55.17% with an average of 35.17%, and rock fragments,
ranging from 1.3 to 34.2% with an average of 10.81%. On comparing
the fraction of rock fragments from a different origin, the content
of metamorphic rock fragments was found to be the highest (from 1.13
to 15.7% with an average of 5.97%), followed by sedimentary and volcanic
rock fragments (from 0 to 9.47% with an average of 2.47%, from 0.17
to 9.03% with an average of 2.37%, respectively) (Figure b). In terms of grain size,
the Ch-6 reservoir sandstones are mainly composed of fine sandstone
and siltstone (Figure a). In addition, the shape of grains is mainly subrounded to subangular
with moderately sorted composition (Figure b).
Figure 3
Rock compositions of the Ch-6 sandstones in
the WJY area, Ordos
Basin. (a) Ternary diagram showing framework grain compositions. (b)
Histogram displaying the compositions of rock fragments. Q, Quartz;
F, feldspar; R, rock fragments; I, quartz arenite; II, subarkose;
III, sublitharenite; IV, arkose; V, lithic arkose; VI, feldspathic
litharenite; and VII, litharenite.
Figure 4
Histograms
of (a) grain size and (b) sorting characteristics of
Ch-6 in the WJY area, Ordos Basin.
Rock compositions of the Ch-6 sandstones in
the WJY area, Ordos
Basin. (a) Ternary diagram showing framework grain compositions. (b)
Histogram displaying the compositions of rock fragments. Q, Quartz;
F, feldspar; R, rock fragments; I, quartz arenite; II, subarkose;
III, sublitharenite; IV, arkose; V, lithic arkose; VI, feldspathic
litharenite; and VII, litharenite.Histograms
of (a) grain size and (b) sorting characteristics of
Ch-6 in the WJY area, Ordos Basin.
Reservoir Properties
Porosity
and Permeability
The porosity
of the Ch-6 sandstones in the WJY area mainly ranges from 6 to 12%
with an average of 8.59% and the permeability mainly ranges from 0.1
to 0.5 mD with an average of 0.32 mD (Figure ). Therefore, these sandstones have the typical
characteristics of low porosity and permeability, which belong to
the category of tight oil reservoirs defined by Zou et al., Yao et
al., and Kuang et al.[3,7,38] Moreover,
there is a roughly exponential correlation (R2 = 0.4686) between porosity and permeability, which shows
that the permeability is mainly controlled by the development of the
connected pores (Figure ).
Figure 5
Distribution of (a) porosity and (b) permeability of the Ch-6 reservoirs
in the WJY area, Ordos Basin.
Figure 6
Relationship
between the porosity and permeability of the Ch-6
reservoirs in the WJY area, Ordos Basin.
Distribution of (a) porosity and (b) permeability of the Ch-6 reservoirs
in the WJY area, Ordos Basin.Relationship
between the porosity and permeability of the Ch-6
reservoirs in the WJY area, Ordos Basin.
Pore Types and Pore-Throat Characteristics
Porosity determines the reservoir capacity, and permeability is
an important factor for reservoir productivity.[39,40] The pore types of the Ch-6 reservoirs in the WJY area are mainly
original intergranular pores, feldspar dissolved pores, rock fragments
dissolved pores, intercrystalline pores, and microcracks, the thin-section
porosity of which are 1.60, 0.84, 0.16, 0.09, and 0.03% (Figure a), respectively.
Therefore, the original intergranular pore and dissolved pores account
for 95.58% of the total thin-section porosity (Figure b).
Figure 7
Pore type distribution diagram of the Ch-6 reservoir
in the WJY
area, Ordos Basin. (a) Diagram showing the percentages of various
pore types. (b) Diagram showing the total thin-section porosity and
the different types of porosities.
Pore type distribution diagram of the Ch-6 reservoir
in the WJY
area, Ordos Basin. (a) Diagram showing the percentages of various
pore types. (b) Diagram showing the total thin-section porosity and
the different types of porosities.Mercury injection analysis is an important method to study the
reservoir pore structure, which can quantitatively reflect the microstructure
characteristics of the reservoir pore throat. Based on the analysis
and calculation of typical capillary pressure curves and pore-throat
radius value distribution of the Ch-6 reservoir (Figure ), it could be found that the
mean displacement pressure ranges from 0.21 to 2.53 MPa with an average
of 1.22 MPa, the median throat radius value ranges from 0.06 to 0.51
μm with an average of 0.24 μm, the measured porosity ranges
from 6.4 to 16.3% with an average of 9.94%, and the measured permeability
ranges from 0.06 to 0.68 mD with an average of 0.24 mD. It is found
by further analysis that the measured porosity and permeability are
positively correlated with the median throat radius values and negatively
correlated with the mean displacement pressure. However, it must be
pointed out that due to the limitations of experimental methods, mercury
injection analysis could only characterize the characteristics of
the partial pore system but could not characterize the full-scale
pore-throat structure of sandstones.[41,42] Hence, the
experimental data here mainly describe the pore structure features
above the mesopores in sandstones.
Figure 8
Typical capillary pressure curves and
pore-throat radius distribution
of the Ch-6 reservoirs in the WJY area, Ordos Basin. (A) Well C193,
2242.72 m; (B) Well Y60, 2549.81 m; (C) Well Y27, 2348.40 m; and (D)
Well Y94, 2739.48 m.
Typical capillary pressure curves and
pore-throat radius distribution
of the Ch-6 reservoirs in the WJY area, Ordos Basin. (A) Well C193,
2242.72 m; (B) Well Y60, 2549.81 m; (C) Well Y27, 2348.40 m; and (D)
Well Y94, 2739.48 m.
Diagenetic
Types
Compaction
Compaction is one of
the significant factors leading to the tightness of the Ch-6 reservoirs
in the WJY area and could be divided into two types: mechanical compaction
and chemical compaction. By observing the thin sections, it could
be seen that the contact relation between the particles is mainly
a linear contact, which preserves the original intergranular pores
(Figure a) at the
early stage of burial. As the burial depth increases and the paleogeotemperature
exceeds 70 °C,[43] chemical compaction
starts and the contact relation between the particles tends to a linear-suture
contact (Figure b);
also some mica particles undergo a plastic deformation (Figure c), where the original intergranular
pores are relatively less.
Figure 9
Microscopic characteristics of the Ch-6 sandstones
in the WJY area,
Ordos Basin. (a) Original intergranular pores (yellow arrow); the
brown chlorite coatings on the surface of the grains after being soaked
by oil (green arrow); Well F11, 2368.33 m, plane-polarized light (PPL).
(b) Grains exhibit a linear contact due to compaction (blue arrow),
and some of them have microcracks (yellow arrow); Well Y83, 2492.42
m, PPL. (c) Plastic deformation of mica fragments due to compaction,
which are in close contact with the rigid grains (yellow arrow); Well
H35, 2515.63 m, PPL. (d) Intergranular pores (green arrow) and feldspar
dissolved pores (blue arrow) are cemented by ferrocalcite; Well H307,
2736.84 m, PPL; (e) Intergranular pores are cemented by ferrocalcite
(yellow arrow); Well H315, 2580.75 m, PPL. (f) Secondary growth on
the surface of terrigenous quartz grains (yellow arrow); Well H306,
2739.40 m, PPL. (g) Authigenic quartz with a good crystal morphology
in dissolution pores (yellow arrow); Well Y76, 2379.90 m, SEM. (h)
Microcrystalline chlorites, which grow vertically on the surface of
the grains in the intergranular pore, form coatings on the surface
of the grains (yellow arrow); Well F11, 2369.17 m, PPL. (i) Chlorite
with the crystalline morphology of a petaline shape on the surface
of the grains (yellow arrow); Well Y28, 2423.00 m, SEM. (j) Kaolinite
in feldspar dissolved pores (yellow arrow); Well C335, 2303.36 m,
PPL. (k) Authigenic kaolinite grains with accordion morphologies occur
in pore spaces (yellow arrow); Well Y28, 2442.78 m, SEM. (l) Illite
occurs as pore bridges with the crystalline morphology of a needlelike
and hairy structure (yellow arrow); Well Y76, 2385.80 m, SEM. (m)
Feldspar dissolved pores (yellow arrow) and moldic pores (red arrow);
Well Y76, 2338.63 m, PPL. (n) Intergranular pores (green arrow) and
debris dissolved pores (yellow arrow); Well C335, 2303.36 m, PPL.
(o) Feldspar grains are dissolved (yellow arrow) and authigenic kaolinite
is developed in the dissolved pores (red arrow); Well Y28, 2448.23
m, SEM.
Microscopic characteristics of the Ch-6 sandstones
in the WJY area,
Ordos Basin. (a) Original intergranular pores (yellow arrow); the
brown chlorite coatings on the surface of the grains after being soaked
by oil (green arrow); Well F11, 2368.33 m, plane-polarized light (PPL).
(b) Grains exhibit a linear contact due to compaction (blue arrow),
and some of them have microcracks (yellow arrow); Well Y83, 2492.42
m, PPL. (c) Plastic deformation of mica fragments due to compaction,
which are in close contact with the rigid grains (yellow arrow); Well
H35, 2515.63 m, PPL. (d) Intergranular pores (green arrow) and feldspar
dissolved pores (blue arrow) are cemented by ferrocalcite; Well H307,
2736.84 m, PPL; (e) Intergranular pores are cemented by ferrocalcite
(yellow arrow); Well H315, 2580.75 m, PPL. (f) Secondary growth on
the surface of terrigenous quartz grains (yellow arrow); Well H306,
2739.40 m, PPL. (g) Authigenic quartz with a good crystal morphology
in dissolution pores (yellow arrow); Well Y76, 2379.90 m, SEM. (h)
Microcrystalline chlorites, which grow vertically on the surface of
the grains in the intergranular pore, form coatings on the surface
of the grains (yellow arrow); Well F11, 2369.17 m, PPL. (i) Chlorite
with the crystalline morphology of a petaline shape on the surface
of the grains (yellow arrow); Well Y28, 2423.00 m, SEM. (j) Kaolinite
in feldspar dissolved pores (yellow arrow); Well C335, 2303.36 m,
PPL. (k) Authigenickaolinite grains with accordion morphologies occur
in pore spaces (yellow arrow); Well Y28, 2442.78 m, SEM. (l) Illite
occurs as pore bridges with the crystalline morphology of a needlelike
and hairy structure (yellow arrow); Well Y76, 2385.80 m, SEM. (m)
Feldspar dissolved pores (yellow arrow) and moldic pores (red arrow);
Well Y76, 2338.63 m, PPL. (n) Intergranular pores (green arrow) and
debris dissolved pores (yellow arrow); Well C335, 2303.36 m, PPL.
(o) Feldspar grains are dissolved (yellow arrow) and authigenickaolinite
is developed in the dissolved pores (red arrow); Well Y28, 2448.23
m, SEM.
Cementation
Cementation is an important
consolidation diagenesis due to the precipitation of authigenic minerals
in the pores, which lasts throughout the diagenesis process except
for compaction. By observing the thin sections, it was seen that the
main types of cementation of the Ch-6 reservoirs are composed of carbonate
cementation, siliceous cementation, and clay minerals cementation.
Carbonate Cementation
Carbonate
cement is one of the most common authigenic minerals in clastic rock
reservoirs that are continuously superimposed in the vertical direction
with multiple argillaceous interlayers. By observing the thin sections
of the Ch-6 reservoir sandstones in the WJY area, it was seen that
the carbonate cements are dominated by ferrocalcite (Figure d,e) with an average content
of 4.10%. They are mainly distributed in the intergranular pores and/or
the intragranular dissolution pores of feldspar and show up as deep
red after being stained. These features indicate that the later dissolution
of feldspars is likely to provide the necessary calcium ions for their
precipitation.
Siliceous Cementation
Compared
with carbonate cement, siliceous cement is limited and its average
content is 1.1%, which is characterized by terrigenous quartz overgrowth
and authigenic quartz crystals in dissolved pores (Figure f,g).
Clay Cementation
The authigenic
clay minerals of the Ch-6 reservoir sandstones in the WJY area are
primarily composed of chlorite, kaolinite, and illite. Chlorites primarily
appear as a grain coating, and this form of pore-filling cement is
rare; the average content of chlorite is around 4.9%. Authigenickaolinite
fills the pores in the form of interstitial material (Figure j) and exhibits accordion morphologies
(Figure k), and the
average content of kaolinite is around 3.9%. Illite occurs as pore
bridges with the crystalline morphology of a needlelike and hairy
structure according to the SEM observation (Figure l), and the average content of illite is
less than 1%.
Dissolution
The main dissolved
grains are detrital feldspars and rock fragments, usually along the
grain edges and cleavage fractures to form intragranular and intergranular
dissolved pores and little moldic pores (Figure m–o). However, the dissolution of
pore-filling carbonate cements is relatively rare. Meanwhile, the
reservoir property would be improved effectively when the dissolved
matters are moved out of the pore or throat. However, the permeability
of the reservoir would be greatly reduced when these matters precipitate
in the intergranular pore in the form of authigenic clay minerals.
The results in this study suggest that dissolution is the most significant
factor to improve the physical properties of the Ch-6 reservoirs in
the WJY area, and the average content of the dissolved pores is about
4.2%.
Discussion
Diagenetic Stage and Sequence
On
the basis of the aforementioned sedimentary characteristics and predecessor
research results,[44] the sedimentary environment
of Ch-6 formation in the WJY area is identified as a fresh-brackish
inland lake basin. The dividing standard of the diagenetic stage and
sequence is according to the China Petroleum Standard of the Division
of Diagenetic Stage in Clastic Rocks (SY/T 5477-2003).The maximum
buried depth of the Ch-6 reservoirs in the WJY area ranges from 2500
to 2700 m, corresponding to the maximum paleotemperature ranging from
100 to 125 °C with an ancient land surface temperature of 15
°C and a paleogeothermal gradient of about 3.5–4.0 °C/100
m.[44] The vitrinite reflectance (Ro) of the Ch-6 mudstone mainly ranges from 0.5
to 0.9% and a small number of samples exceed to 1.2%. The smectite
content of mixed layer I/S is under 15%; the homogenization temperature
of fluid inclusions in the margin of quartz secondary enlargement
and the microcracks ranges from 70 to 170 °C, which holds two
distinct temperature peak areas of 80 to 100 and 120 to 130 °C.[10] These data indicate that the Ch-6 tight oil
reservoir is at the mesogenetic A stage. Furthermore, the petrographic
characteristics of the Ch-6 tight oil reservoirs (e.g., point to linear
contact between grains, the types of dissolved minerals, which are
mainly composed of feldspar and detritus, etc.) also indicate that
they belong to the mesogenetic A stage (Figure ).
Figure 10
Classification symbols of the CH-6 diagenetic
evolution stage in
the WJY area, Ordos Basin.
Classification symbols of the CH-6 diagenetic
evolution stage in
the WJY area, Ordos Basin.Additionally, the δ18O value of carbonate cements
is usually used to calculate the paleotemperature and as a geological
thermometer for determining the ambient temperatures, which can evaluate
the environmental conditions and the diagenetic stages of cementation.
In this study, the mature theoretical equation for geological thermometers
proposed by Shackleton et al. is used to calculate the paleotemperature
(T).[45] The paleotemperature
is actually the forming temperature of carbonate cements and it is
calculated using the following equation.where the δ18O uses
the PDB
standard; δ18Ow is the oxygen isotope
values of geological fluids medium at the time carbonate cements formation,
and the value of δ18Ow is selected as
−2.5‰ according to the overall geological environment
at the time of the Ch-6 diagenesis period.The calculation results
show that the paleotemperature of carbonate
cements in the Ch-6 reservoirs ranges from 95 to 110 °C (Table ), which corresponds
to the mesogenetic A stage.
Table 1
Carbon and Oxygen
Isotopic Data of
Ch-6 Carbonate Cements in the WJY Area
no.
well name
depth (m)
δ13CPDB (‰)
δ18OPDB (‰)
value of Z
paleotemperature
(°C)
1
C118
2266.5
–1.913
–21.547
112.65
101.78
2
C18
2153.9
–0.788
–20.972
115.24
97.62
3
C18
2145.5
1.09
–15.022
122.05
58.47
4
C18
2184.86
–0.449
–20.594
116.12
94.92
5
F10
2216.9
–0.763
–22.221
114.67
106.74
6
H132
2336.15
–1.909
–19.55
113.65
87.62
7
H132
2368.25
1.361
–20.877
119.69
96.94
8
H269
2385.8
–1.05
–18.512
115.93
80.58
9
H269
2396.3
0.325
–21.48
117.27
101.29
10
H269
2366
–0.989
–22.307
114.17
107.38
11
H269
2408.7
–0.289
–23.109
115.2
113.41
12
H269
2419.27
0.204
–20.341
117.59
93.13
13
H48
2480.1
–0.84
–21.819
114.71
103.77
14
H83
2455.7
–1.674
–20.687
113.57
95.58
15
H83
2662
–8.742
–21.48
98.7
101.29
16
Y114
2273.6
–2.202
–21.161
112.25
98.98
17
Y115
2298.3
0.184
–14.506
120.45
55.41
18
Y115
2313.8
0.399
–14.511
120.89
55.44
19
Y115
2382.05
–2.428
–18.963
112.88
83.61
20
Y117
2349.4
–1.751
–19.647
113.93
88.29
21
Y117
2351.2
–1.348
–14.11
117.51
53.1
22
Y117
2353.7
–1.422
–17.021
115.91
70.83
23
Y123
2376.1
–3.806
–21.038
109.03
98.09
24
Y28
2440.8
–1.995
–21.482
112.52
101.3
25
Y28
2443.1
–1.262
–22.351
113.58
107.7
26
Y28
2448.28
–2.138
–21.219
112.35
99.4
27
Y41
2506.8
–1.787
–17.555
114.9
74.27
28
Y41
2508.3
–0.473
–15.095
118.81
58.91
29
Y41
2547.7
–4.491
–21.982
107.16
104.97
30
Y41
2556.65
–3.48
–21.208
109.61
99.32
31
Y41
2571.4
–2.566
–22.008
111.08
105.16
32
Y71
2370.1
–1.67
–19.746
114.05
88.97
33
Y71
2415.9
–0.157
–20.799
116.62
96.38
34
Y73
2375.3
0.056
–20.652
117.13
95.33
35
Y76
2345.7
–0.27
–25.53
114.03
132.4
36
Y76
2337.7
–0.312
–23.855
114.78
119.13
37
Y76
2339.7
–0.141
–24.115
115
121.16
38
Y76
2385.62
2.317
–24.793
119.7
126.49
39
Y76
2385.62
–1.218
–20.397
114.65
93.53
40
Y76
2378.95
–0.224
–21.617
116.08
102.29
41
Y76
2372.6
2.127
–24.298
119.56
122.59
42
Y76
2378.95
2.031
–24.221
119.4
121.98
43
Y76
2379.9
0.147
–20.962
117.16
97.55
44
Y76
2385.8
–0.769
–21.365
115.09
100.45
45
Y76
2393.6
–3.002
–19.711
111.34
88.73
Comprehending the observation of diagenesis and textural
relationships
of authigenic minerals with the results of the diagenetic stage analysis
and isotopic data, the diagenetic evolution sequence of the Ch-6 reservoirs
in the WJY area is as follows: mechanical compaction, formation of
chlorite coating, formation of quartz overgrowth, feldspar dissolution,
formation of authigenickaolinite, formation of authigenic quartz,
conversion of kaolinite to illite, precipitation of ferrocalcite,
and, finally, hydrocarbon emplacement.
Controlling
Factors of Reservoir Quality
Sedimentary Conditions
Determine the Material
Basis of the Reservoir
Sedimentary conditions control the
reservoir material basis. Fundamentally, sedimentary facies control
the microscopic distribution of reservoirs and affect the basic physical
properties of the reservoir. In this study, the physical parameters
of sand bodies of different sedimentary microfacies were calculated.
The results show that the average porosity and permeability of the
main channel sandstones in the delta plain are 6.61% and 0.08 mD,
respectively; the average porosity and permeability of the channel
margin sandstones in the delta plain are 5.04% and 0.05 mD, respectively;
the average porosity and permeability of the main channel sandstones
in the delta front are 9.53% and 0.32 mD, respectively; the average
porosity and permeability of the channel margin sandstones in the
delta front are 4.93% and 0.13 mD, respectively; the average porosity
and permeability of interdistributary bay sands is 3.48%, 0.05 mD,
respectively (Table ). In consequence, the main channel sandstone of the underwater distributary
channel in the delta front is the dominant sedimentary body for the
relatively high-quality reservoir development.
Table 2
Physical Parameters of Sand Bodies
with Different Sedimentary Microfacies
distributary
channel
underwater distributary
channel
physical
parameter
main channel
sandstones
channel margin
sandstones
main channel
sandstones
channel margin
sandstones
interdistributary
bay sandstones
porosity (%)
6.61
5.04
9.53
4.93
3.48
permeability (mD)
0.08
0.05
0.32
0.13
0.05
Moreover, petrological characteristics (e.g., lithology,
composition,
grain size, sorting, and roundness) also affect reservoir physical
properties, while the detailed impact mechanism is comprehensive and
multifactorial.[46,47] Therefore, it is difficult to
find the correlation between a single factor and reservoir physical
characteristics. This study attempts to use the mathematical statistics
methods and pick several influence factors that are well correlated
with reservoir physical properties (Figure and 12). The result
shows that the average particle size is positively associated with
thin-section porosity (Figure ). Quartz content is positively associated with intergranular
pore content. The total content of feldspar and rock fragment is positively
associated with the thin-section porosity of dissolved pores (Figure ). Further, according
to the lithologic characteristics of the reservoir, the high content
of feldspar and rock fragment as well as the fine particle size are
the material causes for the weak compaction capability of the reservoirs
and partly the reasons for the reservoir tightness.
Figure 11
Correlation between
intergranular pore content and quartz content;
the correlation between thin-section porosity of dissolved pores and
the total content of feldspar and rock fragments.
Figure 12
Correlation
between thin-section porosity and the average particle
size.
Correlation between
intergranular pore content and quartz content;
the correlation between thin-section porosity of dissolved pores and
the total content of feldspar and rock fragments.Correlation
between thin-section porosity and the average particle
size.
Reservoir
Transformation due to Diagenesis
As mentioned above, sedimentary
conditions control the petrologic
basis and spatial distribution of reservoirs. Furthermore, after deposition,
as the burial depth increases, the diagenetic conditions (temperature,
pressure, pH, and fluid solubility) change, and the diagenetic features
show obvious diversity in each diagenetic stage. Accordingly, the
diagenesis diversity can affect the pore evolution and physical characteristics
of the reservoirs.To assess the relative importance of compaction
and cementation in the ultimate reservoir quality, the diagram of
Houseknecht et al. is applied in the study[16] (Figure ). The
diagram shows that more data points cluster in the lower-left portion
of the diagram, which indicates that the reservoirs are mainly controlled
by compaction in the process of tightness and the effect of cementation
is relatively weak.
Figure 13
Intergranular volume vs cements volume for the Ch-6 sandstones
in the WJY area, Ordos Basin.
Intergranular volume vs cements volume for the Ch-6 sandstones
in the WJY area, Ordos Basin.In addition, the effects of different diageneses on reservoir properties
are studied through correlation analysis. The result suggests that
the content of carbonate cements, kaolinite fillings, chlorite coatings,
and siliceous cements are all negatively associated with the measured
porosity (Figure ), which indicates that multiple cementations are an important cause
of reservoir densification.
Figure 14
Correlation between different cements with
measured porosity.
Correlation between different cements with
measured porosity.
Quantitative
Analysis of the Pore Evolution
Process
According to research requirements, original porosity
(OP) is obtained as follows. The original porosity (OP) could be calculated
with eq , where particle
diameters of P25 and P75 represent the corresponding
cumulative volume fraction of 25 and 75%, respectively. The Trask
sorting coefficient (S0) can be calculated
with eq . The calculated
results show that S0 is 1.32 and the original
porosity (OP) of the Ch-6 reservoirs in the WJY area is 38.2%.In addition, it is significantly
necessary
to analyze the quantitative influence of various diagenesis on reservoirs.
Based on the burial history, paleogeothermal history[44] (Figure ), porosity evolution progress, and the aforementioned diagenetic
evolution sequence of Ch-6 in the WJY area, analyzing the reservoir
changes due to the various diagenesis types, this study established
the quantitative progress of pores evolution and divided the progress
into seven main stages (Figure ).
Figure 15
Burial and paleogeothermal history of the Ch-6 reservoir
in the
WJY area, Ordos Basin.
Figure 16
Model diagram of the
Ch-6 reservoir tightness process and pore
evolution in the WJY area, Ordos Basin.
Burial and paleogeothermal history of the Ch-6 reservoir
in the
WJY area, Ordos Basin.Model diagram of the
Ch-6 reservoir tightness process and pore
evolution in the WJY area, Ordos Basin.First, in the early stages of burial and diagenesis, various diagenesis
had not yet begun to transform the reservoirs. The reservoir space
was mainly composed of primary intergranular pores and the contact
type between particles was point-contact. As calculated above, the
optional porosity was 38.2%.Second, in the compaction porosity
loss stage, the burial depth
and paleogeotemperature increased to around 1500 m and 65 °C,
respectively. Under the gravitational pressure of overlying sediments
and tectonic stress, the grains rearranged and intergranular water
was discharged, and the contact type between the grains changed to
a point-linear contact and the porosity was gradually lost. In fact,
compaction occurs throughout the diagenesis process and it is not
a specific diagenetic action at a certain diagenetic stage. Therefore,
to reflect the changing degree of the reservoir by compaction, this
study considers it as an influencing parameter for quantitative analysis.
The observation and statistic results of thin sections show that the
intergranular volume (IGV) is about 19.2%. Based on the calculation
of eq , the compaction
porosity loss (COPL) is 23.5%. In addition, when the burial depth
was around 1500 m and the paleogeotemperature was 65 °C, a small
amount of early carbonate cements and clay membrane of chlorite were
developed in the reservoirs. However, these two types of diagenesis
have little effect on the reservoir in the early diagenetic stage,
and the study does not conduct the quantitative analysis. Therefore,
under the transformation of compaction, the reservoir pore type was
residual primary intergranular pore and the residual porosity was
about 14.7%.Third, in the dissolved porosity increase
stage, the burial depth and paleogeotemperature increased to around
1700 m and 85 °C, respectively. The soluble components were dissolved
due to the change of the diagenetic environment. Similar to compaction,
dissolution also occurred throughout the diagenesis process and the
study considers it as an influencing parameter for quantitative analysis.
The results of the analysis indicate that the dissolution minerals
are mainly unstable minerals such as early carbonate cementation,
feldspar, and rock fragments. The pore types are residual primary
intergranular pores and intergranular dissolved pores during this
stage. In addition, with the increase of compaction, the contact relation
between grains changes from point to point-line. The observation and
statistic results of thin sections show that the dissolved porosity
(DP) is about 4.2%. Based on the calculation as in eq , the dissolved porosity increase
(DPI) was around 3.2% and the residual porosity of the reservoir was
17.9%.Fourth, in the chlorite cementation porosity
loss stage, the burial depth and paleogeotemperature increased to
around 1900 m and 100 °C, respectively. The authigenic chlorite
of the Ch-6 reservoirs is mainly developed in the form of a grain
coating. The observation and statistic results of the thin sections
show that the content of chlorite cements (CHCEM) is about 4.9%. Based
on the calculation as in eq , chlorite cementation porosity loss (CHCEPL) was around 3.8%
and the residual porosity of the reservoir was 14.1%.Fifth, in the kaolinite cementation porosity
loss stage, the burial depth and paleogeotemperature increased to
around 2250 m and 125 °C, respectively. Authigenickaolinite
is one of the common authigenic clay minerals in the Ch-6 reservoir
of the WJY area, which is mainly filled in the dissolved pores of
feldspar and residual original intergranular pores and closely related
to the unstable aluminosilicate minerals (such as feldspar). The observation
and statistic results of the thin sections show that the content of
kaolinite cements (KCEM) is about 3.9%. Based on the calculation as
in eq , the kaolinite
cementation porosity loss (KCEPL) was 3.0% and the residual porosity
of the reservoir was 11.1%.Finally, in the carbonate cementation porosity
loss and siliceous cementation porosity loss stage, the burial depth
of the Ch-6 reservoir increased to the maximum burial depth of about
2700 m, and then the stratum was continually uplifted to the present
burial depth of about 2100 m. The medium-term carbonate cements are
mainly sparry calcite or ferrocalcite, but the late carbonate cements
are mainly ankerite and to a lesser extent ferrocalcite in the Ch-6
reservoirs of the WJY area. The early carbonate cements are scarcely
observed due to the dissolution. The observation and statistic results
of the thin sections show that the content of carbonate cements (CACEM)
is about 4.1%. Based on the calculation as in eq , the carbonate cementation porosity loss
(CACEPL) was 3.1% and the residual porosity was around 8.0% after
the carbonate cementation. In addition, the main types of siliceous
cements in the Ch-6 reservoirs of the WJY area are terrigenous quartz
overgrowth and authigenic quartz crystals in dissolved pores. The
observation and statistic results of the thin sections show that the
content of siliceous cements (SCEM) is about 1.1%. Based on the calculation
as in eq , the siliceous
cementation porosity loss (SCEPL) was 0.8% and the residual porosity
of the reservoir was about 7.2%. Inescapably, the illite was rarely
developed in the reservoirs in this stage and had little effect on
the reservoir. Therefore, the study ignores it as an influencing parameter
and does not conduct a quantitative analysis of illite cementation.Above all, on account of the quantitative
analysis of porosity evolution, compaction is the primary cause leading
to reservoir tightness. The other diagenetic factors leading to reservoir
tightness are cementation of chlorite, carbonate, kaolinite, silica,
and illite, ranked from a strong to a weak degree of influence on
reservoir tightness. In addition, dissolution is the key factor to
improve the physical property of the reservoir. The tightness process
and pore evolution model of the Ch-6 reservoir in the WJY area are
shown in Figure (Table ).
Table 3
Meaning of the Abbreviations in the
Above Equations
OP
original porosity: the porosity
before all kinds of diagenesis
COPL
compaction porosity loss:
the percentage of the pore volume reduced after compaction in the
apparent original rock volume
IGV
intergranular volume: the
porosity that has undergone compaction but without dissolution
DPI
dissolved porosity increase:
the percentage of pore volume resulting from dissolution in the apparent
volume before all kinds of diagenesis
DP
dissolved porosity: the
percentage of pore volume resulting from dissolution in the apparent
volume at present
CHEPL
chlorite cementation porosity
loss: the percentage of reduced pore volume due to chlorite cementation
in the apparent volume before all kinds of diagenesis
CHCEM
chlorite cements content:
the percentage of chlorite cements content in the rock volume
KCEPL
kaolinite cementation porosity
loss: the percentage of reduced pore volume due to kaolinite cementation
in the apparent volume before all kinds of diagenesis
KCEM
kaolinite cements content:
the percentage of kaolinite cements content in the rock volume
CACEPL
carbonate cementation porosity
loss: the percentage of reduced pore volume due to carbonate cementation
in the apparent volume before all kinds of diagenesis
CACEM
carbonate cements content:
the percentage of carbonate cements content in the rock volume
SCEPL
silica cementation porosity
loss: the percentage of reduced pore volume due to silica cementation
in the apparent volume before all kinds of diagenesis
SCEM
silica cements content:
the percentage of silica cements content in the rock volume
Conclusions
Sedimentary facies types primarily controlled the material basis
of the Ch-6 reservoirs in the WJY area and further affected their
physical properties. The high content of feldspar and rock fragments
and the fine grain size are the material causes for the reservoir
tightness. The main channel sandstone of the underwater distributary
channel is the dominant sedimentary facies type for the high-quality
reservoir development.The diagenetic stage of the reservoir
Ch-6 in the WJY area is identified
as the late stage of eodiagenesis A to the early stage of mesodiagenesis
B. The main diagenetic factors that lead to the reservoir tightness
include compaction and the cementation of carbonate, chlorite kaolinite,
and silica, the porosity loss of which are 23.5, 3.1, 3.8, 3.0, and
0.8%, respectively. The dissolved porosity increase is around 3.2%.
Therefore, compaction and the cementation of chlorite, kaolinite,
and carbonate are the key factors to damage the physical property
of the reservoir. The dissolution is the most significant factor to
improve reservoir physical property.