Literature DB >> 34198184

High fidelity triangular sweep of the magnetic field for millisecond scan EPR imaging.

Denis A Komarov1, Alexandre Samouilov1, Hiroshi Hirata2, Jay L Zweier3.   

Abstract

Linearity of the magnetic field sweep is important for high resolution continuous wave EPR imaging. Driving the field with triangular wave function is the most efficient way to scan EPR projections. However, the magnetic field sweep profile can be significantly distorted during fast millisecond projection scan. In this work, we introduce a method to generate highly linear and properly symmetrical triangular sweeps of the magnetic field using calibrated harmonics of the triangular wave function. First, the frequency response function of the EPR magnet and its power circuitry was obtained. For this, the field sweeping coil was driven with sinusoidal signals of different frequencies and the actual magnetic field inside the magnet was recorded. To cover wide range of frequencies, the measurements were carried out independently using gaussmeter, Hall-effect linear sensor integrated circuit, and an inductance coil. For each frequency, the system gain and the phase delay were determined. These data were used to adjust the amplitudes and the phases of individual harmonics of the triangular wave function. After the calibration, the maximum deviation of the magnetic field from the linear function was 0.05% of sweep width for 4 ms scan. The maximum discrepancy between the forward and the reverse scan was less than 0.04%. Sweep overhead time for changing the scan direction was 5%. The proposed approach allows generation of high fidelity triangular magnetic field sweeps with accuracy better than 0.1% for the range of the magnetic field sweep widths up to 48 G and scan duration from 10 s down to 1 ms.
Copyright © 2021 Elsevier Inc. All rights reserved.

Entities:  

Keywords:  Continuous wave; EPR imaging; Electron paramagnetic resonance; Fast scan; Frequency response function; High resolution; Linear time-invariant system; Magnetic field; Sweep linearity

Mesh:

Year:  2021        PMID: 34198184      PMCID: PMC8316393          DOI: 10.1016/j.jmr.2021.107024

Source DB:  PubMed          Journal:  J Magn Reson        ISSN: 1090-7807            Impact factor:   2.734


  28 in total

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Journal:  J Magn Reson       Date:  2016-12-31       Impact factor: 2.229

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Authors:  Sankaran Subramanian; Nallathamby Devasahayam; Alan McMillan; Shingo Matsumoto; Jeeva P Munasinghe; Keita Saito; James B Mitchell; Gadisetti V R Chandramouli; Murali C Krishna
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7.  Detection of undistorted continuous wave (CW) electron paramagnetic resonance (EPR) spectra with non-adiabatic rapid sweep (NARS) of the magnetic field.

Authors:  Aaron W Kittell; Theodore G Camenisch; Joseph J Ratke; Jason W Sidabras; James S Hyde
Journal:  J Magn Reson       Date:  2011-06-13       Impact factor: 2.229

8.  A Linear Magnetic Field Scan Driver.

Authors:  Richard W Quine; Tomasz Czechowski; Gareth R Eaton
Journal:  Concepts Magn Reson Part B Magn Reson Eng       Date:  2009-02-01       Impact factor: 1.176

9.  Algebraic reconstruction of 3D spatial EPR images from high numbers of noisy projections: An improved image reconstruction technique for high resolution fast scan EPR imaging.

Authors:  Denis A Komarov; Alexandre Samouilov; Rizwan Ahmad; Jay L Zweier
Journal:  J Magn Reson       Date:  2020-08-25       Impact factor: 2.229

10.  Non-invasive mapping of glutathione levels in mouse brains by in vivo electron paramagnetic resonance (EPR) imaging: Applied to a kindling mouse model.

Authors:  Miho C Emoto; Hideo Sato-Akaba; Yuta Matsuoka; Ken-Ichi Yamada; Hirotada G Fujii
Journal:  Neurosci Lett       Date:  2018-10-02       Impact factor: 3.046

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