| Literature DB >> 34118030 |
Francesca Ceccacci1, Simona Sennato2, Edoardo Rossi3, Raffaele Proroga3, Stefano Sarti4, Marco Diociaiuti5, Stefano Casciardi6, Valentina Mussi7, Alessia Ciogli8, Federico Bordi4, Giovanna Mancini9, Cecilia Bombelli10.
Abstract
In this chapter we describe: (1) the procedure for the synthesis of four single chain bolaamphiphiles, displaying chains of 12, 16, 20 and 30 methylene units and triphenylphosphonium moieties as headgroups (TPP1-TPP4); (2) the methods used to characterize TPP1-TPP4 spontaneous aggregation in aqueous solution. We illustrate the determination of Krafft point and cac by conductivity measurements and the procedures used to investigate dimensions, morphology, and stability by dynamic and dielectrophoretic laser light scattering, dialysis, transmission electron microscopy, and Raman spectroscopy measurements.Entities:
Keywords: Equilibrium systems; Kinetic traps; Kolbe electrolysis; Thermomorphic electrolytic solution; Triphenylphosphonium bolaamphiphiles; U-shaped/extended conformation
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Year: 2021 PMID： 34118030 DOI： 10.1007/978-1-0716-1262-0_3
Source DB: PubMed Journal: Methods Mol Biol ISSN： 1064-3745