Literature DB >> 33950009

The Hard X-ray Nanoprobe beamline at Diamond Light Source.

Paul D Quinn1, Lucia Alianelli1, Miguel Gomez-Gonzalez1, David Mahoney1, Fernando Cacho-Nerin1, Andrew Peach1, Julia E Parker1.   

Abstract

The Hard X-ray Nanoprobe beamline, I14, at Diamond Light Source is a new facility for nanoscale microscopy. The beamline was designed with an emphasis on multi-modal analysis, providing elemental mapping, speciation mapping by XANES, structural phase mapping using nano-XRD and imaging through differential phase contrast and ptychography. The 185 m-long beamline operates over a 5 keV to 23 keV energy range providing a ≤50 nm beam size for routine user experiments and a flexible scanning system allowing fast acquisition. The beamline achieves robust and stable operation by imaging the source in the vertical direction and implementing horizontally deflecting primary optics and an overfilled secondary source in the horizontal direction. This paper describes the design considerations, optical layout, aspects of the hardware engineering and scanning system in operation as well as some examples illustrating the beamline performance. open access.

Entities:  

Keywords:  Hard X-ray Nanoprobe; multimodal techniques; nano-XANES; nano-XRD; nano-XRF; ptychography; spectro-microscopy

Year:  2021        PMID: 33950009     DOI: 10.1107/S1600577521002502

Source DB:  PubMed          Journal:  J Synchrotron Radiat        ISSN: 0909-0495            Impact factor:   2.616


  6 in total

1.  Local nanoscale phase impurities are degradation sites in halide perovskites.

Authors:  Stuart Macpherson; Tiarnan A S Doherty; Andrew J Winchester; Sofiia Kosar; Duncan N Johnstone; Yu-Hsien Chiang; Krzysztof Galkowski; Miguel Anaya; Kyle Frohna; Affan N Iqbal; Satyawan Nagane; Bart Roose; Zahra Andaji-Garmaroudi; Kieran W P Orr; Julia E Parker; Paul A Midgley; Keshav M Dani; Samuel D Stranks
Journal:  Nature       Date:  2022-05-24       Impact factor: 69.504

2.  Unraveling the varied nature and roles of defects in hybrid halide perovskites with time-resolved photoemission electron microscopy.

Authors:  Sofiia Kosar; Andrew J Winchester; Tiarnan A S Doherty; Stuart Macpherson; Christopher E Petoukhoff; Kyle Frohna; Miguel Anaya; Nicholas S Chan; Julien Madéo; Michael K L Man; Samuel D Stranks; Keshav M Dani
Journal:  Energy Environ Sci       Date:  2021-09-15       Impact factor: 38.532

3.  A cell design for correlative hard X-ray nanoprobe and electron microscopy studies of catalysts under in situ conditions.

Authors:  Julia E Parker; Miguel Gomez-Gonzalez; Yolanda Van Lishout; Husn Islam; Desiree Duran Martin; Dogan Ozkaya; Paul D Quinn; Manfred E Schuster
Journal:  J Synchrotron Radiat       Date:  2022-02-15       Impact factor: 2.616

4.  Design and performance of a dedicated coherent X-ray scanning diffraction instrument at beamline NanoMAX of MAX IV.

Authors:  Dina Carbone; Sebastian Kalbfleisch; Ulf Johansson; Alexander Björling; Maik Kahnt; Simone Sala; Tomas Stankevic; Angel Rodriguez-Fernandez; Björn Bring; Zdenek Matej; Paul Bell; David Erb; Vincent Hardion; Clemens Weninger; Hussein Al-Sallami; Julio Lidon-Simon; Stefan Carlson; Annika Jerrebo; Brian Norsk Jensen; Anders Bjermo; Karl Åhnberg; Linus Roslund
Journal:  J Synchrotron Radiat       Date:  2022-03-16       Impact factor: 2.557

Review 5.  Traceable Characterization of Nanomaterials by X-ray Spectrometry Using Calibrated Instrumentation.

Authors:  Burkhard Beckhoff
Journal:  Nanomaterials (Basel)       Date:  2022-06-30       Impact factor: 5.719

6.  A new Kirkpatrick-Baez-based scanning microscope for the Submicron Resolution X-ray Spectroscopy (SRX) beamline at NSLS-II.

Authors:  E Nazaretski; D S Coburn; W Xu; J Ma; H Xu; R Smith; X Huang; Y Yang; L Huang; M Idir; A Kiss; Y S Chu
Journal:  J Synchrotron Radiat       Date:  2022-07-29       Impact factor: 2.557

  6 in total

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