Literature DB >> 33776141

Feasibility of Laboratory-Based EXAFS Spectroscopy with Cryogenic Detectors.

Simon J George1, Matthew H Carpenter1, Stephan Friedrich2, Robin Cantor1.   

Abstract

Extended X-ray Absorption Fine Structure (EXAFS) spectroscopy is a powerful technique that gives element-specific information about the structure of molecules. The development of a laboratory EXAFS spectrometer capable of measuring transmission spectra would be a significant advance as the technique is currently only available at synchrotron radiation lightsources. Here, we explore the potential of cryogenic detectors as the energy resolving component of a laboratory transmission EXAFS instrument. We examine the energy resolution, count-rate, and detector stability needed for good EXAFS spectra and compare these to the properties of cryogenic detectors and conventional X-ray optics. We find that superconducting tunnel junction (STJ) detectors are well-suited for this application.

Entities:  

Keywords:  Cryogenic Detectors; EXAFS; STJ Detectors; XAS

Year:  2020        PMID: 33776141      PMCID: PMC7990010          DOI: 10.1007/s10909-020-02474-7

Source DB:  PubMed          Journal:  J Low Temp Phys        ISSN: 0022-2291            Impact factor:   1.570


  8 in total

1.  Iron carbonyl sulfides, formaldehyde, and amines condense to give the proposed azadithiolate cofactor of the Fe-only hydrogenases.

Authors:  Hongxiang Li; Thomas B Rauchfuss
Journal:  J Am Chem Soc       Date:  2002-02-06       Impact factor: 15.419

2.  Applications of extended X-ray absorption fine-structure spectroscopy to studies of bimetallic nanoparticle catalysts.

Authors:  Anatoly I Frenkel
Journal:  Chem Soc Rev       Date:  2012-12-21       Impact factor: 54.564

3.  Table-top ultrafast x-ray microcalorimeter spectrometry for molecular structure.

Authors:  J Uhlig; W Fullagar; J N Ullom; W B Doriese; J W Fowler; D S Swetz; N Gador; S E Canton; K Kinnunen; I J Maasilta; C D Reintsema; D A Bennett; L R Vale; G C Hilton; K D Irwin; D R Schmidt; V Sundström
Journal:  Phys Rev Lett       Date:  2013-03-26       Impact factor: 9.161

4.  Parameter-free calculations of X-ray spectra with FEFF9.

Authors:  John J Rehr; Joshua J Kas; Fernando D Vila; Micah P Prange; Kevin Jorissen
Journal:  Phys Chem Chem Phys       Date:  2010-05-06       Impact factor: 3.676

5.  The solution structure of the copper clioquinol complex.

Authors:  M Jake Pushie; Kurt H Nienaber; Kelly L Summers; Julien J H Cotelesage; Olena Ponomarenko; Helen K Nichol; Ingrid J Pickering; Graham N George
Journal:  J Inorg Biochem       Date:  2014-01-16       Impact factor: 4.155

6.  An improved laboratory-based x-ray absorption fine structure and x-ray emission spectrometer for analytical applications in materials chemistry research.

Authors:  Evan P Jahrman; William M Holden; Alexander S Ditter; Devon R Mortensen; Gerald T Seidler; Timothy T Fister; Stosh A Kozimor; Louis F J Piper; Jatinkumar Rana; Neil C Hyatt; Martin C Stennett
Journal:  Rev Sci Instrum       Date:  2019-02       Impact factor: 1.523

7.  Soft X-ray spectroscopy with transition-edge sensors at Stanford Synchrotron Radiation Lightsource beamline 10-1.

Authors:  Sang-Jun Lee; Charles J Titus; Roberto Alonso Mori; Michael L Baker; Douglas A Bennett; Hsiao-Mei Cho; William B Doriese; Joseph W Fowler; Kelly J Gaffney; Alessandro Gallo; Johnathon D Gard; Gene C Hilton; Hoyoung Jang; Young Il Joe; Christopher J Kenney; Jason Knight; Thomas Kroll; Jun-Sik Lee; Dale Li; Donghui Lu; Ronald Marks; Michael P Minitti; Kelsey M Morgan; Hirohito Ogasawara; Galen C O'Neil; Carl D Reintsema; Daniel R Schmidt; Dimosthenis Sokaras; Joel N Ullom; Tsu-Chien Weng; Christopher Williams; Betty A Young; Daniel S Swetz; Kent D Irwin; Dennis Nordlund
Journal:  Rev Sci Instrum       Date:  2019-11-01       Impact factor: 1.523

8.  Collecting data in the home laboratory: evolution of X-ray sources, detectors and working practices.

Authors:  Tadeusz Skarzynski
Journal:  Acta Crystallogr D Biol Crystallogr       Date:  2013-06-18
  8 in total

北京卡尤迪生物科技股份有限公司 © 2022-2023.