Literature DB >> 33731976

2-Azadienes as Enamine Umpolung Synthons for the Preparation of Chiral Amines.

Steven J Malcolmson1, Kangnan Li1, Xinxin Shao1.   

Abstract

The development of new strategies for the preparation of chiral amines is an important objective in organic synthesis. In this Synpacts, we summarize our approach for catalytically accessing nucleophilic n class="Chemical">aminoalkyl metal species from 2-azadienes, and its application in generating a number of important but elusive chiral amine scaffolds. Reductive couplings with ketones and imines afford 1,2-amino tertiary alcohols and 1,2-diamines, respectively, whereas fluoroarylations of gem-difluoro-2-azadienes deliver α-trifluoromethylated benzylic amines.

Entities:  

Keywords:  2-azadienes; amino alcohols; cross-coupling; diamines; fluoroarylation; reductive coupling

Year:  2019        PMID: 33731976      PMCID: PMC7963344          DOI: 10.1055/s-0037-1611770

Source DB:  PubMed          Journal:  Synlett        ISSN: 0936-5214            Impact factor:   2.454


  137 in total

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9.  Enantioselective CuH-Catalyzed Hydroallylation of Vinylarenes.

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1.  A Diastereodivergent and Enantioselective Approach to syn- and anti-Diamines: Development of 2-Azatrienes for Cu-Catalyzed Reductive Couplings with Imines That Furnish Allylic Amines.

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  1 in total

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