Literature DB >> 3372812

Determination of phylloquinone and menaquinone in human milk using high performance liquid chromatography.

H Isshiki1, Y Suzuki, A Yonekubo, H Hasegawa, Y Yamamoto.   

Abstract

A high performance liquid chromatographic method for measuring vitamin K in human milk and cow milk is described. The K vitamins were extracted with n-pentane from enzymatic hydrolysate of milk, purified by semipreparative HPLC, and then analyzed by reversed-phase HPLC equipped with a dual electrochemical detector. The amount of phylloquinone and menaquinone-4 in human milk was 2.1 +/- .9 and 1.3 +/- 1 microgram/L, respectively (n = 23). A small amount of menaquinone-6 was detected in both human and cow milk.

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Year:  1988        PMID: 3372812     DOI: 10.3168/jds.S0022-0302(88)79600-9

Source DB:  PubMed          Journal:  J Dairy Sci        ISSN: 0022-0302            Impact factor:   4.034


  3 in total

1.  Determination of phylloquinone (vitamin K(1)) by high performance liquid chromatography with UV detection and with particle beam-mass spectrometry.

Authors:  M Careri; A Mangia; P Manini; N Taboni
Journal:  Anal Bioanal Chem       Date:  1996-04       Impact factor: 4.142

2.  Quantitation of vitamin K in human milk.

Authors:  L M Canfield; J M Hopkinson; A F Lima; G S Martin; K Sugimoto; J Burr; L Clark; D L McGee
Journal:  Lipids       Date:  1990-07       Impact factor: 1.880

Review 3.  Micronutrients in Human Milk: Analytical Methods.

Authors:  Daniela Hampel; Daphna K Dror; Lindsay H Allen
Journal:  Adv Nutr       Date:  2018-05-01       Impact factor: 8.701

  3 in total

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