Literature DB >> 33566018

A helium mini-cryostat for the nanoprobe beamline ID16B at ESRF: characteristics and performance.

Ricardo G Steinmann1, Gema Martinez-Criado1, Damien Salomon1, Hugo Vitoux1, Remi Tucoulou1, Julie Villanova1, Sylvain Laboure1, Joel Eymery2, Jaime Segura-Ruiz1.   

Abstract

A helium mini-cryostat has been developed for the hard X-ray nanoprobe ID16B of the European Synchrotron to collect X-ray excited optical luminescence and X-ray fluorescence at low temperature (<10 K). The mini-cryostat has been specifically designed to fit within the strong space restrictions and high-demanding mechanical constraints imposed by the beamline to provide vibration-free operation and maximal thermal stability. This paper reports the detailed design, architecture and technical requirements of the mini-cryostat, and presents the first experimental data measured using the cryogenic equipment. The resulting cryo-system features ultimate thermal stability, fast cool-down and ultra-low vibrations. The simultaneous X-ray fluorescence and X-ray excited optical luminescence data acquired from bulk GaN and core/shell InGaN/GaN multi-quantum wells validated the excellent performance of the cryostat with ultimate resolution, stability and sensitivity.

Entities:  

Keywords:  X-ray nanoprobes; XEOL; XRF; cryostat

Year:  2020        PMID: 33566018     DOI: 10.1107/S1600577520007110

Source DB:  PubMed          Journal:  J Synchrotron Radiat        ISSN: 0909-0495            Impact factor:   2.616


  2 in total

Review 1.  Traceable Characterization of Nanomaterials by X-ray Spectrometry Using Calibrated Instrumentation.

Authors:  Burkhard Beckhoff
Journal:  Nanomaterials (Basel)       Date:  2022-06-30       Impact factor: 5.719

2.  High-resolution XEOL spectroscopy setup at the X-ray absorption spectroscopy beamline P65 of PETRA III.

Authors:  S Levcenko; R Biller; T Pfeiffelmann; K Ritter; H H Falk; T Wang; S Siebentritt; E Welter; C S Schnohr
Journal:  J Synchrotron Radiat       Date:  2022-08-11       Impact factor: 2.557

  2 in total

北京卡尤迪生物科技股份有限公司 © 2022-2023.