Literature DB >> 33482467

Differential electron yield imaging with STXM.

William A Hubbard1, Jared J Lodico1, Xin Yi Ling1, Brian T Zutter1, Young-Sang Yu2, David A Shapiro2, B C Regan3.   

Abstract

Total electron yield (TEY) imaging is an established scanning transmission X-ray microscopy (STXM) technique that gives varying contrast based on a sample's geometry, elemental composition, and electrical conductivity. However, the TEY-STXM signal is determined solely by the electrons that the beam ejects from the sample. A related technique, X-ray beam-induced current (XBIC) imaging, is sensitive to electrons and holes independently, but requires electric fields in the sample. Here we report that multi-electrode devices can be wired to produce differential electron yield (DEY) contrast, which is also independently sensitive to electrons and holes, but does not require an electric field. Depending on whether the region illuminated by the focused STXM beam is better connected to one electrode or another, the DEY-STXM contrast changes sign. DEY-STXM images thus provide a vivid map of a device's connectivity landscape, which can be key to understanding device function and failure. To demonstrate an application in the area of failure analysis, we image a 100 nm, lithographically-defined aluminum nanowire that has failed after being stressed with a large current density.
Copyright © 2020 Elsevier B.V. All rights reserved.

Entities:  

Keywords:  Electron yield; Failure analysis; STXM; Scanning transmission X-ray microscopy; TEY; XBIC

Year:  2020        PMID: 33482467      PMCID: PMC8262251          DOI: 10.1016/j.ultramic.2020.113198

Source DB:  PubMed          Journal:  Ultramicroscopy        ISSN: 0304-3991            Impact factor:   2.689


  11 in total

1.  Advanced thin film technology for ultrahigh resolution X-ray microscopy.

Authors:  Joan Vila-Comamala; Konstantins Jefimovs; Jörg Raabe; Tero Pilvi; Rainer H Fink; Mathias Senoner; Andre Maassdorf; Mikko Ritala; Christian David
Journal:  Ultramicroscopy       Date:  2009-07-15       Impact factor: 2.689

2.  A fast, direct x-ray detection charge-coupled device.

Authors:  P Denes; D Doering; H A Padmore; J-P Walder; J Weizeorick
Journal:  Rev Sci Instrum       Date:  2009-08       Impact factor: 1.523

3.  Total-electron-yield current measurements for near-surface extended x-ray-absorption fine structure.

Authors: 
Journal:  Phys Rev B Condens Matter       Date:  1988-02-15

4.  Quantitative analysis of mammalian chromosome by scanning transmission soft X-ray microscopy.

Authors:  K Shinohara; T Ohigashi; S Toné; M Kado; A Ito
Journal:  Ultramicroscopy       Date:  2018-07-05       Impact factor: 2.689

5.  Spectrally resolved x-ray beam induced current in a single InGaP nanowire.

Authors:  Lert Chayanun; Vilgailė Dagytė; Andrea Troian; Damien Salomon; Magnus Borgström; Jesper Wallentin
Journal:  Nanotechnology       Date:  2018-08-23       Impact factor: 3.874

6.  3D chemical mapping: application of scanning transmission (soft) X-ray microscopy (STXM) in combination with angle-scan tomography in bio-, geo-, and environmental sciences.

Authors:  Martin Obst; Gregor Schmid
Journal:  Methods Mol Biol       Date:  2014

7.  Origin and hysteresis of lithium compositional spatiodynamics within battery primary particles.

Authors:  Jongwoo Lim; Yiyang Li; Daan Hein Alsem; Hongyun So; Sang Chul Lee; Peng Bai; Daniel A Cogswell; Xuzhao Liu; Norman Jin; Young-sang Yu; Norman J Salmon; David A Shapiro; Martin Z Bazant; Tolek Tyliszczak; William C Chueh
Journal:  Science       Date:  2016-08-05       Impact factor: 47.728

8.  Electron beam-induced current imaging with two-angstrom resolution.

Authors:  Matthew Mecklenburg; William A Hubbard; Jared J Lodico; B C Regan
Journal:  Ultramicroscopy       Date:  2019-10-01       Impact factor: 2.689

9.  Deactivation of Cu-Exchanged Automotive-Emission NH3 -SCR Catalysts Elucidated with Nanoscale Resolution Using Scanning Transmission X-ray Microscopy.

Authors:  Xinwei Ye; Joel E Schmidt; Ru-Pan Wang; Ilse K van Ravenhorst; Ramon Oord; Tiehong Chen; Frank de Groot; Florian Meirer; Bert M Weckhuysen
Journal:  Angew Chem Int Ed Engl       Date:  2020-02-28       Impact factor: 15.336

10.  An ultrahigh-resolution soft x-ray microscope for quantitative analysis of chemically heterogeneous nanomaterials.

Authors:  David A Shapiro; Sergey Babin; Richard S Celestre; Weilun Chao; Raymond P Conley; Peter Denes; Bjoern Enders; Pablo Enfedaque; Susan James; John M Joseph; Harinarayan Krishnan; Stefano Marchesini; Krishna Muriki; Kasra Nowrouzi; Sharon R Oh; Howard Padmore; Tony Warwick; Lee Yang; Valeriy V Yashchuk; Young-Sang Yu; Jiangtao Zhao
Journal:  Sci Adv       Date:  2020-12-16       Impact factor: 14.136

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