Literature DB >> 33017511

Alkali-Metal Mediation: Diversity of Applications in Main-Group Organometallic Chemistry.

Thomas X Gentner1, Robert E Mulvey1.   

Abstract

Organolithium compounds have been at the forefront of synthetic chemistry for over a century, as they mediate the synthesis of myriads of compounds that are utilised worldwide in academic and industrin class="Chemical">al settings. For that reason, lithium has always been the most important alkali metal in organometallic chemistry. Today, that importance is being seriously challenged by sodium and potassium, as the alkali-metal mediation of organic reactions in general has started branching off in several new directions. Recent examples covering main-group homogeneous catalysis, stoichiometric organic synthesis, low-valent main-group metal chemistry, polymerization, and green chemistry are showcased in this Review. Since alkali-metal compounds are often not the end products of these applications, their roles are rarely given top billing. Thus, this Review has been written to alert the community to this rising unifying phenomenon of "alkali-metal mediation".
© 2020 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH.

Entities:  

Keywords:  alkali metals; catalysis; metallation; organolithium compounds; π-arene interactions

Year:  2020        PMID: 33017511     DOI: 10.1002/anie.202010963

Source DB:  PubMed          Journal:  Angew Chem Int Ed Engl        ISSN: 1433-7851            Impact factor:   15.336


  14 in total

1.  t BuOLi-Promoted Hydroboration of Esters and Epoxides.

Authors:  Yinyin Shi; Yue Wang; Zhefan Huang; Fangjun Zhang; Yinlin Shao
Journal:  ACS Omega       Date:  2022-05-25

2.  Lithium achieves sequence selective ring-opening terpolymerisation (ROTERP) of ternary monomer mixtures.

Authors:  Susanne Rupf; Patrick Pröhm; Alex J Plajer
Journal:  Chem Sci       Date:  2022-05-05       Impact factor: 9.969

3.  (2-Ethylhexyl)sodium: A Hexane-Soluble Reagent for Br/Na-Exchanges and Directed Metalations in Continuous Flow.

Authors:  Johannes H Harenberg; Niels Weidmann; Alexander J Wiegand; Carla A Hoefer; Rajasekar Reddy Annapureddy; Paul Knochel
Journal:  Angew Chem Int Ed Engl       Date:  2021-05-03       Impact factor: 15.336

4.  THF-solvated Heavy Alkali Metal Benzyl Compounds (Na, Rb, Cs): Defined Deprotonation Reagents for Alkali Metal Mediation Chemistry.

Authors:  Lukas Brieger; Christian Unkelbach; Carsten Strohmann
Journal:  Chemistry       Date:  2021-10-25       Impact factor: 5.020

5.  Heterotrimetallic Carbon Dioxide Copolymerization and Switchable Catalysts: Sodium is the Key to High Activity and Unusual Selectivity.

Authors:  Alex J Plajer; Charlotte K Williams
Journal:  Angew Chem Int Ed Engl       Date:  2021-05-10       Impact factor: 15.336

6.  Synthesis, Crystal and Electronic Structures of a Thiophosphinoyl- and Amino-Substituted Metallated Ylide.

Authors:  Mike Jörges; Alexander Kroll; Leif Kelling; Richard Gauld; Bert Mallick; Stefan M Huber; Viktoria H Gessner
Journal:  ChemistryOpen       Date:  2021-09-27       Impact factor: 2.630

7.  Reductive Dimerization of CO by a Na/Mg(I) Diamide.

Authors:  Han-Ying Liu; Ryan J Schwamm; Samuel E Neale; Michael S Hill; Claire L McMullin; Mary F Mahon
Journal:  J Am Chem Soc       Date:  2021-10-15       Impact factor: 15.419

8.  Metallation of sensitive fluoroarenes using a potassium TMP-zincate supported by a silyl(bis)amido ligand.

Authors:  Pasquale Mastropierro; Alan R Kennedy; Eva Hevia
Journal:  Chem Commun (Camb)       Date:  2022-04-26       Impact factor: 6.065

9.  Prospective Evaluation of an Amide-Based Zinc Scaffold as an Anti-Alzheimer Agent: In Vitro, In Vivo, and Computational Studies.

Authors:  Wajeeha Waseem; Fareeha Anwar; Uzma Saleem; Bashir Ahmad; Rehman Zafar; Asifa Anwar; Muhammad Saeed Jan; Umer Rashid; Abdul Sadiq; Tariq Ismail
Journal:  ACS Omega       Date:  2022-07-19

10.  Ring-Opening Polymerization of L-Lactide Catalyzed by Potassium-Based Complexes: Mechanistic Studies.

Authors:  Christian Rentero; Jesús Damián; Asier Medel; María Fernández-Millán; Yolanda Rusconi; Giovanni Talarico; Tomás Cuenca; Valentina Sessini; Marta E G Mosquera
Journal:  Polymers (Basel)       Date:  2022-07-23       Impact factor: 4.967

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