Literature DB >> 32009020

High-throughput, Multi-batch System for the Efficient Microwave Digestion of Biological Samples.

Davide Spanu1, Laura Butti1, Ginevra Boldrocchi2, Roberta Bettinetti2, Damiano Monticelli1.   

Abstract

In this paper, we proposed a high-throughput microwave digestion system based on multi-batch reactors (three quartz test tubes inside commercial PTFE vessels). This original configuration was validated by ICP-MS analysis of several elements in biological certified reference materials (fish tissues and plankton). The proposed system was proved to be free from contamination showing very low LODs. The improved hardware configuration is therefore highly beneficial for the detection of trace elements in microsamples from the marine food web.

Keywords:  High-throughput microwave digestion; biological samples; marine food web; microsamples; trace elements

Year:  2020        PMID: 32009020     DOI: 10.2116/analsci.19A004

Source DB:  PubMed          Journal:  Anal Sci        ISSN: 0910-6340            Impact factor:   2.081


  2 in total

1.  Simple Acid Digestion Procedure for the Determination of Total Mercury in Plankton by Cold Vapor Atomic Fluorescence Spectroscopy.

Authors:  João Pereira Santos; Lirie Mehmeti; Vera I Slaveykova
Journal:  Methods Protoc       Date:  2022-03-25

2.  How to Clean and Safely Remove HF from Acid Digestion Solutions for Ultra-Trace Analysis: A Microwave-Assisted Vessel-Inside-Vessel Protocol.

Authors:  Marco Pinna; Arianna Signorelli; Gilberto Binda; Carlo Dossi; Laura Rampazzi; Davide Spanu; Sandro Recchia
Journal:  Methods Protoc       Date:  2022-04-03
  2 in total

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