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Literature DB >> 31932829

Facile synthesis of novel lithium β-diketonate glyme adducts: the effect of molecular engineering on the thermal properties.

Nishant Peddagopu¹, Patrizia Rossi², Carmela Bonaccorso³, Ausrine Bartasyte⁴, Paola Paoli², Graziella Malandrino¹.

Abstract

Novel adducts of lithium hexafluoroacetylacetonato {Li(hfa)} with polyethers (monoglyme = {CH3OCH2CH2OCH3}, diglyme = {CH3O(CH2CH2O)2CH3}, triglyme = {CH3O(CH2CH2O)3CH3} and tetraglyme {CH3O(CH2CH2O)4CH3} have been synthesized through a single step reaction and characterized by FT-IR spectroscopy, 1H, and 13C NMR, single crystal X-ray diffraction studies along with thermal analysis.

Entities: Chemical

Year: 2020 PMID： 31932829 DOI： 10.1039/c9dt04732h

Source DB: PubMed Journal: Dalton Trans ISSN： 1477-9226 Impact factor: 4.390

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Cited

1 in total

1. Sodium β-Diketonate Glyme Adducts as Precursors for Fluoride Phases: Synthesis, Characterization and Functional Validation.

Authors: Nishant Peddagopu; Anna L Pellegrino; Carmela Bonaccorso; Patrizia Rossi; Paola Paoli; Graziella Malandrino
Journal: Molecules Date: 2022-09-23 Impact factor: 4.927

1 in total