Literature DB >> 30778496

C-H 18F-fluorination of 8-methylquinolines with Ag[18F]F.

So Jeong Lee1, Allen F Brooks, Naoko Ichiishi, Katarina J Makaravage, Andrew V Mossine, Melanie S Sanford, Peter J H Scott.   

Abstract

This report describes a Pd-mediated C-H radiofluorination of 8-methylquinoline derivatives with no-carrier-added Ag[18F]F. To achieve this transformation, a new method was developed for the generation of Ag[18F]F using a sep-pak cartridge. The C-H radiofluorination was then optimized and applied to a series of substituted <span class="Chemical">8-methylquinoline derivatives. Finally, this method was fully automated using a radiochemistry synthesis module.

Entities:  

Year:  2019        PMID： 30778496      PMCID： PMC6556205          DOI： 10.1039/c9cc00641a

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  22 in total

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Review 2.  18F labeling of arenes.

Authors:  Matthew Tredwell; Véronique Gouverneur
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3.  Semiautomated synthesis of a novel [18F] amine fluorocyanoborane for PET imaging studies. Radiosynthesis and in vivo characterization in rats.

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Journal:  Appl Radiat Isot       Date:  2006-10-24       Impact factor: 1.513

4.  Copper-mediated fluorination of aryl iodides.

Authors:  Patrick S Fier; John F Hartwig
Journal:  J Am Chem Soc       Date:  2012-06-22       Impact factor: 15.419

5.  Palladium-catalyzed asymmetric synthesis of allylic fluorides.

Authors:  Matthew H Katcher; Abigail G Doyle
Journal:  J Am Chem Soc       Date:  2010-11-18       Impact factor: 15.419

6.  Pd-catalyzed C-H fluorination with nucleophilic fluoride.

Authors:  Kate B McMurtrey; Joy M Racowski; Melanie S Sanford
Journal:  Org Lett       Date:  2012-07-30       Impact factor: 6.005

7.  Oxidative aliphatic C-H fluorination with fluoride ion catalyzed by a manganese porphyrin.

Authors:  Wei Liu; Xiongyi Huang; Mu-Jeng Cheng; Robert J Nielsen; William A Goddard; John T Groves
Journal:  Science       Date:  2012-09-14       Impact factor: 47.728

8.  Palladium-catalyzed intramolecular aminofluorination of unactivated alkenes.

Authors:  Tao Wu; Guoyin Yin; Guosheng Liu
Journal:  J Am Chem Soc       Date:  2009-11-18       Impact factor: 15.419

9.  Copper-catalyzed, directing group-assisted fluorination of arene and heteroarene C-H bonds.

Authors:  Thanh Truong; Kristine Klimovica; Olafs Daugulis
Journal:  J Am Chem Soc       Date:  2013-06-12       Impact factor: 15.419

10.  Review of F-FDG Synthesis and Quality Control.

Authors:  S Yu
Journal:  Biomed Imaging Interv J       Date:  2006-10-01
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  3 in total

1.  Synthesis of [18F]-γ-fluoro-α,β,-unsaturated esters and ketones via vinylogous 18F-fluorination of α-diazoacetates with [18F]AgF.

Authors:  Stephen Thompson; So Jeong Lee; Isaac M Jackson; Naoko Ichiishi; Allen F Brooks; Melanie S Sanford; Peter J H Scott
Journal:  Synthesis (Stuttg)       Date:  2019-12       Impact factor: 3.157

2.  Copper-Mediated Late-stage Radiofluorination: Five Years of Impact on Pre-clinical and Clinical PET Imaging.

Authors:  Jay S Wright; Tanpreet Kaur; Sean Preshlock; Sean S Tanzey; Wade P Winton; Liam S Sharninghausen; Nicholas Wiesner; Allen F Brooks; Melanie S Sanford; Peter J H Scott
Journal:  Clin Transl Imaging       Date:  2020-05-26

Review 3.  Recent advances in transition-metal-catalyzed incorporation of fluorine-containing groups.

Authors:  Xiaowei Li; Xiaolin Shi; Xiangqian Li; Dayong Shi
Journal:  Beilstein J Org Chem       Date:  2019-09-23       Impact factor: 2.883
  3 in total

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