Literature DB >> 30443995

Enhancing signal-to-noise ratio and resolution in low-field NMR relaxation measurements using post-acquisition digital filters.

Tatiana Monaretto1, Andre Souza2, Tiago Bueno Moraes3, Victor Bertucci-Neto4, Corinne Rondeau-Mouro5, Luiz Alberto Colnago4.   

Abstract

The traditional way to enhance signal-to-noise ratio (SNR) of nuclear magnetic resonance (NMR) signals is to increase the number of scans. However, this procedure increases the measuring time that can be prohibitive for some applications. Therefore, we have tested the use of several post-acquisition digital filters to enhance SNR up to one order of magnitude in time domain NMR (TD-NMR) relaxation measurements. The procedures were studied using continuous wave free precession (CWFP-T1 ) signals, acquired with very low flip angles that contain six times more noise than the Carr-Purcell-Meiboom-Gill (CPMG) signal of the same sample and experimental time. Linear (LI) and logarithmic (LO) data compression, low-pass infinity impulse response (LP), Savitzky-Golay (SG), and wavelet transform (WA) post-acquisition filters enhanced the SNR of the CWFP-T1 signals by at least six times. The best filters were LO, SG, and WA that have high enhancement in SNR without significant distortions in the ILT relaxation distribution data. Therefore, it was demonstrated that these post-acquisition digital filters could be a useful way to denoise CWFP-T1 , as well as CPMG noisy signals, and consequently reducing the experimental time. It was also demonstrated that filtered CWFP-T1 method has the potential to be a rapid and nondestructive method to measure fat content in beef and certainly in other meat samples.
© 2018 John Wiley & Sons, Ltd.

Keywords:  CPMG; CWFP; Savitzky-Golay filter; data compression; low-field NMR; post-acquisition filter; wavelet transform

Year:  2018        PMID: 30443995     DOI: 10.1002/mrc.4806

Source DB:  PubMed          Journal:  Magn Reson Chem        ISSN: 0749-1581            Impact factor:   2.447


  2 in total

Review 1.  Recent 1D and 2D TD-NMR Pulse Sequences for Plant Science.

Authors:  Tatiana Monaretto; Tiago Bueno Moraes; Luiz Alberto Colnago
Journal:  Plants (Basel)       Date:  2021-04-21

2.  Non-Invasive Method to Predict the Composition of Requeijão Cremoso Directly in Commercial Packages Using Time Domain NMR Relaxometry and Chemometrics.

Authors:  G de Oliveira Machado; Gustavo Galastri Teixeira; Rodrigo Henrique Dos Santos Garcia; Tiago Bueno Moraes; Evandro Bona; Poliana M Santos; Luiz Alberto Colnago
Journal:  Molecules       Date:  2022-07-11       Impact factor: 4.927

  2 in total

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