Literature DB >> 30350663

Electrochemical Formation of 3,5-Diimido-1,2-dithiolanes by Dehydrogenative Coupling.

Valentina M Breising1, Tile Gieshoff1,2, Anton Kehl1, Vincent Kilian1, Dieter Schollmeyer1, Siegfried R Waldvogel1,2.   

Abstract

A synthetic approach to the cyclic disulfide moiety of 3,5-diimido-1,2-dithiolane derivatives starting with readily available precursors including the electrochemical coupling of dithioanilides is developed. The electrochemical key step provides sustainable synthetic access in high yields, using a very simple electrolysis setup.

Entities:  

Year:  2018        PMID： 30350663     DOI： 10.1021/acs.orglett.8b02904

Source DB:  PubMed          Journal:  Org Lett        ISSN： 1523-7052            Impact factor:   6.005


  3 in total

1.  N,N'-Diphenyldithiomalonodiamide: Structural Features, Acidic Properties, and In Silico Estimation of Biological Activity.

Authors:  A E Sinotsko; A V Bespalov; N V Pashchevskaya; V V Dotsenko; N A Aksenov; I V Aksenova
Journal:  Russ J Gen Chem       Date:  2021-12-17       Impact factor: 0.868

Review 2.  Photochemical and Electrochemical Applications of Proton-Coupled Electron Transfer in Organic Synthesis.

Authors:  Philip R D Murray; James H Cox; Nicholas D Chiappini; Casey B Roos; Elizabeth A McLoughlin; Benjamin G Hejna; Suong T Nguyen; Hunter H Ripberger; Jacob M Ganley; Elaine Tsui; Nick Y Shin; Brian Koronkiewicz; Guanqi Qiu; Robert R Knowles
Journal:  Chem Rev       Date:  2021-11-23       Impact factor: 60.622

3.  Electrochemical Synthesis of Fluorinated Orthoesters from 1,3-Benzodioxoles.

Authors:  Johannes L Röckl; Adrian V Hauck; Dieter Schollmeyer; Siegfried R Waldvogel
Journal:  ChemistryOpen       Date:  2019-05-14       Impact factor: 2.911
  3 in total

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