Literature DB >> 30032035

A cryogen-consumption-free system for dynamic nuclear polarization at 9.4 T.

Mathieu Baudin1, Basile Vuichoud2, Aurélien Bornet3, Geoffrey Bodenhausen4, Sami Jannin2.   

Abstract

A novel system for dissolution dynamic nuclear polarization based on a cost-effective "cryogen-free" magnet that can generate fields up to 9.4 T with a sample space that can reach temperatures below 1.4 K in a continuous and stable manner. Polarization levels up to P(1H) = 60 ± 5% can be reached with TEMPOL in about 20 min, and P(13C) = 50 ± 5% can be achieved using adiabatic cross polarization.
Copyright © 2018 Elsevier Inc. All rights reserved.

Entities:  

Keywords:  Adiabatic cross polarization; Cryogen-consumption-free magnets; Dissolution DNP; Dynamic nuclear polarization (DNP)

Year:  2018        PMID： 30032035     DOI： 10.1016/j.jmr.2018.07.001

Source DB:  PubMed          Journal:  J Magn Reson        ISSN： 1090-7807            Impact factor:   2.229


  9 in total

1.  A multisample 7 T dynamic nuclear polarization polarizer for preclinical hyperpolarized MR.

Authors:  Tian Cheng; Adam P Gaunt; Irene Marco-Rius; Marcel Gehrung; Albert P Chen; Jacques J van der Klink; Arnaud Comment
Journal:  NMR Biomed       Date:  2020-01-30       Impact factor: 4.044

2.  Performance and reproducibility of 13C and 15N hyperpolarization using a cryogen-free DNP polarizer.

Authors:  Arianna Ferrari; Josh Peters; Mariia Anikeeva; Andrey Pravdivtsev; Frowin Ellermann; Kolja Them; Olga Will; Eva Peschke; Hikari Yoshihara; Olav Jansen; Jan-Bernd Hövener
Journal:  Sci Rep       Date:  2022-07-08       Impact factor: 4.996

Review 3.  Hyperpolarized water as universal sensitivity booster in biomolecular NMR.

Authors:  Christian Hilty; Dennis Kurzbach; Lucio Frydman
Journal:  Nat Protoc       Date:  2022-05-11       Impact factor: 17.021

Review 4.  Application and methodology of dissolution dynamic nuclear polarization in physical, chemical and biological contexts.

Authors:  Sami Jannin; Jean-Nicolas Dumez; Patrick Giraudeau; Dennis Kurzbach
Journal:  J Magn Reson       Date:  2019-06-04       Impact factor: 2.229

5.  Scalable dissolution-dynamic nuclear polarization with rapid transfer of a polarized solid.

Authors:  Karel Kouřil; Hana Kouřilová; Samuel Bartram; Malcolm H Levitt; Benno Meier
Journal:  Nat Commun       Date:  2019-04-15       Impact factor: 14.919

6.  Hyperpolarized NMR Metabolomics at Natural 13C Abundance.

Authors:  Arnab Dey; Benoît Charrier; Estelle Martineau; Catherine Deborde; Elodie Gandriau; Annick Moing; Daniel Jacob; Dmitry Eshchenko; Marc Schnell; Roberto Melzi; Dennis Kurzbach; Morgan Ceillier; Quentin Chappuis; Samuel F Cousin; James G Kempf; Sami Jannin; Jean-Nicolas Dumez; Patrick Giraudeau
Journal:  Anal Chem       Date:  2020-11-02       Impact factor: 6.986

7.  Direct observation of hyperpolarization breaking through the spin diffusion barrier.

Authors:  Quentin Stern; Samuel François Cousin; Frédéric Mentink-Vigier; Arthur César Pinon; Stuart James Elliott; Olivier Cala; Sami Jannin
Journal:  Sci Adv       Date:  2021-04-30       Impact factor: 14.136

8.  Toward protein NMR at physiological concentrations by hyperpolarized water-Finding and mapping uncharted conformational spaces.

Authors:  Ludovica M Epasto; Kateryna Che; Fanny Kozak; Albina Selimovic; Pavel Kadeřávek; Dennis Kurzbach
Journal:  Sci Adv       Date:  2022-08-05       Impact factor: 14.957

9.  Porous functionalized polymers enable generating and transporting hyperpolarized mixtures of metabolites.

Authors:  Théo El Daraï; Samuel F Cousin; Quentin Stern; Morgan Ceillier; James Kempf; Dmitry Eshchenko; Roberto Melzi; Marc Schnell; Laurent Gremillard; Aurélien Bornet; Jonas Milani; Basile Vuichoud; Olivier Cala; Damien Montarnal; Sami Jannin
Journal:  Nat Commun       Date:  2021-08-04       Impact factor: 14.919
  9 in total

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