Literature DB >> 29858560

Efficient Synthesis of Five Types of Heterocyclic Compounds via Intramolecular Elimination Using Ultrasound-Static Heating Technique.

Hongfei Jiang1, Xueyang Dong1, Xin Jin1, Danyang Zhu1, Ruijuan Yin1,2, Rilei Yu1,2, Shengbiao Wan1, Lijuan Zhang3, Tao Jiang1,2.   

Abstract

An experimental technique, ultrasound-static heating, has been developed for the efficient synthesis of heterocyclic compounds. The technique involves ultrasonic irradiation and static heating processes. First, the ultrasonic irradiation process is performed to form an intermediate of the heterocyclic compound under mild conditions and the subsequent static heating process (heating the intermediate under solvent-free conditions without stirring) produces the target heterocyclic compounds via intramolecular elimination.
© 2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

Keywords:  heterocyclic compounds; non-stirred reaction; solvent-free synthesis; static heating; ultrasound

Year:  2018        PMID: 29858560     DOI: 10.1002/asia.201800682

Source DB:  PubMed          Journal:  Chem Asian J        ISSN: 1861-471X


  1 in total

1.  Facile synthesis of 3-substituted imidazo[1,2-a]pyridines through formimidamide chemistry.

Authors:  Rasapalli Sivappa; Vamshikrishna Reddy Sammeta; Yanchang Huang; James A Golen; Sergey N Savinov
Journal:  RSC Adv       Date:  2019-09-19       Impact factor: 4.036

  1 in total

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