Literature DB >> 29451569

Metal-free NaI/TBHP-mediated sulfonylation of thiols with sulfonyl hydrazides.

Qian Chen1, Yulin Huang, Xiaofeng Wang, Jiawei Wu, Guodian Yu.   

Abstract

A highly efficient sulfonylation of thiols has been achieved through the metal-free NaI/TBHP-mediated cross-coupling of sulfonyl hydrazides and thiols at room temperature. This method provides a convenient and practical route to thiosulfonates in 84-99% yields (39 examples) with wide functional group compatibility.

Entities:  

Year:  2018        PMID: 29451569     DOI: 10.1039/c8ob00244d

Source DB:  PubMed          Journal:  Org Biomol Chem        ISSN: 1477-0520            Impact factor:   3.876


  2 in total

1.  Highly efficient and tunable visible-light-catalytic synthesis of 2,5-diformylfuran using HBr and molecular oxygen.

Authors:  Wenwei Hu; Jialuo She; Zaihui Fu; Bo Yang; Huanhuan Zhang; Dabo Jiang
Journal:  RSC Adv       Date:  2021-07-02       Impact factor: 4.036

2.  A straightforward and convenient synthesis of functionalized allyl thiosulfonates and allyl disulfanes.

Authors:  Raju Jannapu Reddy; Md Waheed; Jangam Jagadesh Kumar
Journal:  RSC Adv       Date:  2018-12-04       Impact factor: 4.036

  2 in total

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